| 查看: 480 | 回复: 1 | |||
zhjie6688木虫 (正式写手)
|
[求助]
单晶问题 已有1人参与
|
|
各位大侠好！文章修改意见回来了，文章修改意见回来了，牵扯以下单晶问题，不知道怎么回答，十万火急，求解答。非常感谢!问题如下： 1.Give standard literature references for SMART, SAINT, SADABS and SHELXTL...in fact, these procedures were only used for the structure of the organic molecule. A complete and accurate description of the data collection strategy, structure solution and refinement for the complexes must be included, and properly referenced. 2.While generally, the crystallographic experiments have been performed poorly and not up to contemporary International standards, that of 3c is extremely poor. Some explanation to justify its inclusion in the paper is required or the entire structure should be removed. I believe the refinement is incorrect as the unit cell contents have not been properly assigned, Z = 4 not Z = 2. 3.Where the residual electron density peaks are greater than 1, e.g. 3a, give their locations in the Experimental section. 4.Figure captions to figures 1, 2 and 3, give the symmetry operation corresponding to "a" in each case. 5. X-ray structure determinations: a reference for SHELXTL should be given. |
回复此楼» 猜你喜欢
有没有化学、材料专业的同学需要调剂 考虑天津高效的可以邮件或者私信
已经有1人回复
-
26年博士招生
已经有16人回复
-
无机化学论文润色/翻译怎么收费?
已经有139人回复
-
江西理工大学功能晶态材料方向刘遂军课题组招收2026年秋季入学博士研究生
已经有11人回复
-
宁夏大学团簇新材料团队招收材料/化学/化工专业博士生
已经有0人回复
-
MIL-101有单晶样品吗
已经有1人回复
-
已删除
已经有3人回复
-
收调剂研究生
已经有2人回复
-
【2026 考研调剂】哈尔滨工程大学核科学与技术学院核化工系 招收调剂生
已经有3人回复
-
武汉纺织大学技术研究院招收化学、化工、生物、材料、纺织等背景专业调剂生
已经有0人回复
-
【2026 考研调剂】哈尔滨工程大学核科学与技术学院核化工系 招收调剂生
已经有1人回复
maomao11259
木虫 (小有名气)
- 应助: 2 (幼儿园)
- 金币: 1955.3
- 散金: 10
- 红花: 2
- 帖子: 294
- 在线: 42.1小时
- 虫号: 289589
- 注册: 2006-10-22
- 专业: 配位化学
【答案】应助回帖
感谢参与，应助指数 +1
|
1.Give standard literature references for SMART, SAINT, SADABS and SHELXTL...in fact, these procedures were only used for the structure of the organic molecule. A complete and accurate description of the data collection strategy, structure solution and refinement for the complexes must be included, and properly referenced. 你的cif里数据收集、解析和精修的描述方式不够准确和详细。 |
2楼2014-03-06 22:46:06
