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[求助]
急急，求微谱数据，麻烦多发些
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化合物1：MeOD δ 149.13, 104.25, 87.60, 79.19, 73.58, 71.58, 70.75, 64.11, 56.51, 22.71, 14.16, 11.69. 化合物2：MeOD δ 154.59, 148.91, 147.40, 138.84, 131.48, 122.18, 115.73, 112.19, 104.38, 87.39, 86.61, 83.95, 79.62, 74.02, 73.20, 64.57, 61.74, 57.29, 56.75, 56.49, 55.77 化合物3：MeOD δ 151.61, 148.65, 148.41, 146.72, 133.77, 132.73, 131.17, 128.18, 120.73, 120.36, 118.57, 115.35, 111.54, 111.03, 85.90, 79.19, 73.80, 63.47, 61.92, 56.20, 56.02, |
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lifeliuyan
至尊木虫 (职业作家)
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【答案】应助回帖
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查询结果：共查到1164个化合物(查询结果仅供参考) -------------------------------------------------------------------------------- 1 . threo-3,3'-dimethoxy-4,8'-oxyneoligna-9,4',7',9'-tetraol-7(8)-ene C20H24O7 相似度:95% Chemistry of Natural Compounds 2009 45 424-426 LIGNANS FROM Gnetum montanum Markgr. f. megalocarpua Li Qin Wang, You Xing Zhao,Lu Zhou and Jun Zhou Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 2 . erythroguaiacylglycerol-β-O-4'-coniferyl ether 相似度:95% Chinese Traditional and Herbal Drugs 2012 43 649-652 Chemical constituents from barks of Ailanthus altissima WANG Yan; ZHANG Hai-ning; WANG Wen-jing; ZHANG Sheng-yuan; ZHANG Xiao-qi; YE Wen-cai Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 3 . erythroguaiacylglycerol-8-O-4'-(coniferyl alcohol) ether 相似度:95% China Journal of Chinese Materia Medica 2012 37 1241-1244 Non-alkaloid chemical constituents from Coptis chinensis CHEN Liang; WANG Lei; ZHANG Qingwen; ZHANG Shengyuan; YE Wencai Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 4 . GGCE 相似度:95% Journal of Wood Science 2005 51 370-378 Stereochemistry and biosynthesis of 8-O-4 neolignans in Eucommia ulmoides: diastereoselective formation of guaiacylglycerol-8-O-4 -(sinapyl alcohol) ether Nattaya Lourith, Takeshi Katayama, Toshisada Suzuki Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 5 . (-)-threo-guaiacylglycerol-8-O-4'-(coniferyl alcohol) ether 相似度:90% Bioorganic & Medicinal Chemistry 2012 20 4164-4171 Natural products as a gold mine for selective matrix metalloproteinases inhibitors Liyan Wang, Xi Li, Shoude Zhang, Weiqiang Lu, Sha Liao, Xiaofeng Liu, Lei Shan, Xu Shen, Hualiang Jiang, Weidong Zhang, Jin Huang, Honglin Li Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 6 . threo-guaiacylglycerol-8-O-4'-(coniferyl alcohol) ether 相似度:90% China Journal of Chinese Materia Medica 2012 37 1241-1244 Non-alkaloid chemical constituents from Coptis chinensis CHEN Liang; WANG Lei; ZHANG Qingwen; ZHANG Shengyuan; YE Wencai Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 7 . GGCE 相似度:90% Journal of Wood Science 2005 51 370-378 Stereochemistry and biosynthesis of 8-O-4 neolignans in Eucommia ulmoides: diastereoselective formation of guaiacylglycerol-8-O-4 -(sinapyl alcohol) ether Nattaya Lourith, Takeshi Katayama, Toshisada Suzuki Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 8 . 1-(4-glucosyl-3-methoxyhenyl)-2-{2,6-dimethoxy-4-[1-(E)-propene-3-ol]-phenoxy}-propan-1,3-diol 相似度:90% Nippon Nōgeikagaku Kaishi 1986 60 593-599 Structure and Physiological Activity of Phenyl Propanoid Glycosides of Hassaku (Citrus hassaku HORT.) and Orange (Citrus sinensis OSBECK.) Peelings Akiyoshi SAWABE, Yoshiharu MATSUBARA, Hiroyasu KUMAMOTO, Yoshitomi IIZUKA, Kozo OKAMOTO Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 9 . (threo) 3, 3'-Dimethoxy-4, 8'-oxyneoligna29, 4', 7', 9'-tetraol-7(8)-ene C20H24O7 相似度:85% Acta Botanica Yunnanica 2004 26(2) 229-233 Lignans from Tsuga dumosa ZHAO You-Xing,LUO Xiao-Dong,ZHOU Jun Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 10 . 2,2'-dimethoxy-(3-hydroxy-1-propenyl)-4'-(1,2,3-trihydroxypropyl)biphenyl ethers, C20H24O7 相似度:85% Phytochemistry 1992 31 3993-3995 Biphenylneolignans from wood of Eurycoma longifolia Hiroshi Morita, Etsuko Kishi, Koichi Takeya, Hideji Itokawa Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 11 . compound Õ C20H24O7 相似度:85% Chinese Traditional and Herbal Drugs 2009 40 183-186 Chemical constituents of Marsdenia tenacissima MA Ming-fang; DING Ke-yi; DING Li-sheng; WANG Xiao-ling Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 12 . 苏式-愈创木基甘油-β-O-4'-松柏基醚 相似度:85% China Journal of Chinese Materia Medica 2012 37 1968-1972 Lignans from Sinocalamus affinis ZHU Mei; XIONG Liang; WANG Yanan; CHEN Minghua; JIANG Bingya; LIN Sheng; ZHU Chenggen; YANG Yongchun; SHI Jiangong Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 13 . 2,2'-dimethoxy-(3-hydroxy-1-propenyl)-4'-(1,2,3-trihydroxypropyl)biphenyl ethers, C20H24O7 相似度:80% Phytochemistry 1992 31 3993-3995 Biphenylneolignans from wood of Eurycoma longifolia Hiroshi Morita, Etsuko Kishi, Koichi Takeya, Hideji Itokawa Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 14 . (7'R,8'R)-2,2'-Dimethoxy-4-(3-hydroxyl-propenyl)-4'-(1,2,3-trihydroxy-propyl) biphenyl ether 相似度:80% Archives of Pharmacal Research 2007 30 1067-1074 Lignan and terpene constituents from the aerial parts of saussurea pulchella Sang Un Choi, Min Cheol Yang, Kyu Ha Lee, Ki Hyun Kim and Kang Ro Lee Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 15 . debilignanoside C26H34O12 相似度:76% Journal of Asian Natural Products Research 2011 Vol.13,No.9 811-816 Chemical constituents of Equisetum debile Jun-Ming Tan, Yi-Hua Qiu, Xin-Qi Tan, Chang-Heng Tan and Kai Xiao Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 16 . (7R,8S)-1-(3,4-dimethoxyphenyl)-2-[4-(3-hydroxy-1-propenyl)-2-methoxyphenoxy]-propane-1,3-diol C21H26O7 相似度:75% Chemical & Pharmaceutical Bulletin 2009 57 298-301 Two New Stereoisomers of Neolignan and Lignan from the Flower Buds of Magnolia fargesii Jun Lee, Eun-Kyoung Seo, Dae Sik Jang, Tae Joung Ha, Jong-Pyung Kim, Joo-Won Nam, Green Bae, Yun Mi Lee, Min Suk Yang and Jin Sook Kim Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 17 . 赤式-愈创木基甘油-β-O-4'-松柏基醚 相似度:75% China Journal of Chinese Materia Medica 2012 37 1968-1972 Lignans from Sinocalamus affinis ZHU Mei; XIONG Liang; WANG Yanan; CHEN Minghua; JIANG Bingya; LIN Sheng; ZHU Chenggen; YANG Yongchun; SHI Jiangong Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 18 . VGEt 相似度:75% Journal of Wood Science 2004 50 142-150 Isolation of lignin–carbohydrate bonds in wood.Model experiments and preliminary application to pine wood Olov Karlsson, Tsutomu Ikeda, Takao Kishimoto, Kengo Magara, Yuji Matsumoto, Shuji Hosoya Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 19 . chushizisin B C19H22O6 相似度:70% Journal of Natural Products 2009 72 621-625 Antioxidant Lignans from the Fruits of Broussonetia papyrifera Ren-Qiang Mei, Yue-Hu Wang, Guan-Hua Du, Guang-Ming Liu, Li Zhang, and Yong-Xian Cheng Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 20 . chushizisin D C19H24O6 相似度:70% Journal of Natural Products 2009 72 621-625 Antioxidant Lignans from the Fruits of Broussonetia papyrifera Ren-Qiang Mei, Yue-Hu Wang, Guan-Hua Du, Guang-Ming Liu, Li Zhang, and Yong-Xian Cheng Structure 13C NMR 碳谱模拟图 |
7楼2013-11-05 19:25:31
lifeliuyan
至尊木虫 (职业作家)
- PhEPI: 1
- 应助: 3913 (副教授)
- 金币: 48784.8
- 散金: 890
- 红花: 208
- 帖子: 4735
- 在线: 635.4小时
- 虫号: 1141109
- 注册: 2010-11-07
- 性别: MM
- 专业: 中药药效物质
2楼2013-11-05 17:54:55
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上面的发错了。。。。 化合物1：MeOD 11.7,14.2,22.7,56.5,64.1,70.8,71.6,73.6,79.2,87.6,104.3,149.1 化合物2：MeOD 55.8,56.5,56.8,57.3,61.7,64.6,73.2,74.0,79.6,84.0,86.6,87.4,104.4,112.2,115.7,122.2,131.5,138.8,147.4,148.9,154.6 化合物3：MeOD 56.0,56.2,61.9,63.5,73.8,79.2,85.9,111.0,111.5,118.6,120.4,120.7,128.2,131.2,132.7,133.8,146.7,148.4,148.7,151.6 |
3楼2013-11-05 18:56:05
4楼2013-11-05 18:56:45