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[求助]
急急，求微谱数据，麻烦多发些
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化合物1：MeOD δ 149.13, 104.25, 87.60, 79.19, 73.58, 71.58, 70.75, 64.11, 56.51, 22.71, 14.16, 11.69. 化合物2：MeOD δ 154.59, 148.91, 147.40, 138.84, 131.48, 122.18, 115.73, 112.19, 104.38, 87.39, 86.61, 83.95, 79.62, 74.02, 73.20, 64.57, 61.74, 57.29, 56.75, 56.49, 55.77 化合物3：MeOD δ 151.61, 148.65, 148.41, 146.72, 133.77, 132.73, 131.17, 128.18, 120.73, 120.36, 118.57, 115.35, 111.54, 111.03, 85.90, 79.19, 73.80, 63.47, 61.92, 56.20, 56.02, |
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上面的发错了。。。。 化合物1：MeOD 11.7,14.2,22.7,56.5,64.1,70.8,71.6,73.6,79.2,87.6,104.3,149.1 化合物2：MeOD 55.8,56.5,56.8,57.3,61.7,64.6,73.2,74.0,79.6,84.0,86.6,87.4,104.4,112.2,115.7,122.2,131.5,138.8,147.4,148.9,154.6 化合物3：MeOD 56.0,56.2,61.9,63.5,73.8,79.2,85.9,111.0,111.5,118.6,120.4,120.7,128.2,131.2,132.7,133.8,146.7,148.4,148.7,151.6 |
3楼2013-11-05 18:56:05
lifeliuyan
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2楼2013-11-05 17:54:55
4楼2013-11-05 18:56:45
lifeliuyan
至尊木虫 (职业作家)
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【答案】应助回帖
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查询结果：共查到52个化合物(查询结果仅供参考) -------------------------------------------------------------------------------- 1 . 1-O-L-isoleucyl-D-fructose 相似度:58.3% Indian Journal of Chemistry Section B 2007 46B 2026-2044 Enzymatic syntheses of L-valyl,L-leucyl and L-isoleucyl esters of carbohydrates using Candida rugosa lipase Somashekar,Bhandya R; Divakar,Soundar Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 2 . bahiensol C19H40O5 相似度:50% Chemical & Pharmaceutical Bulletin 2003 51(5) 612-613 Bahiensol, a New Glycerolipid from a Cultured Myxomycete Didymium bahiense var. bahiense Yuka MISONO,Masami ISHIBASHI,and Akira ITO Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 3 . rhodiocyanoside D C11H17NO6 相似度:50% Chemical & Pharmaceutical Bulletin 1997 45 1498-1503 Bioactive Constituents of Chinese Natural Medicines. IV. Rhodiolae Radix. (2). : On the Histamine Release Inhibitors from the Underground Part of Rhodiola sacra (PRAIN ex HAMET) S. H. Fu (Crassulaceae) : Chemical Structures of Rhodiocyanoside D and Sacran Masayuki YOSHIKAWA,Hiromi SHIMADA,Sugako HORIKAWA,Toshiyuki MURAKAMI,Hiroshi SHIMODA,Johji YAMAHARA and Hisashi MATSUDA Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 4 . heterosigmaglycolipid II C47H72O10 相似度:50% Chemical & Pharmaceutical Bulletin 1992 40 1404-1410 Marine Natural Products. XXIX. Heterosigma-glycolipids I, II, III, and IV, Four Diacylglyceroglycolipids Possessing ω3-Polyunsaturated Fatty Acid Residues, from the Raphidopycean Dinoflagellate Heterosigma akashiwo Motomasa KOBAYASHI,Kozo HAYASHI,Kazuyoshi KAWAZOE and Isao KITAGAWA Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 5 . compound 3 相似度:50% Chemical & Pharmaceutical Bulletin 1990 38 378-381 Studies on the Constituents of Thladiantha dubia BUNGE. II. : Structures of Dubiosides D, E and F, Neutral Saponins of Quillaic Acid Isolated from the Tuber Tsuneatsu NAGAO,Ryuichiro TANAKA,Hikaru OKABE and Tatsuo YAMAUCHI Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 6 . oleaside C C36H54O12 相似度:50% Chemical & Pharmaceutical Bulletin 1979 27 1604-1610 Oleasides ; Novel Cardenolides with an Unusual Framework in Nerium (Nerium 10) FUMIKO ABE and TATSUO YAMAUCHI Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 7 . SG-A C28H44O8 相似度:50% Chemical & Pharmaceutical Bulletin 1979 27 2304-2309 Studies on the Constituents of Asclepiadaceae Plants. XLVI. Aglycones form Stephanotis japonica MAKINO SUMIO TERADA and HIROSHI MITSUHASHI Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 8 . 6-O-glucopyranosyl-cycloastragenol 相似度:50% Chemical & Pharmaceutical Bulletin 1983 31 716-722 Saponin and Sapogenol. XXXVII. Chemical Constituents of Astragali Radix, the Root of Astragalus membranaceus BUNGE. (4). Astragalosides VII and VIII SAO KITAGAWA,HUIKANG WANG and MASAYUKI YOSHIKAWA Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 9 . compound 10 相似度:50% Chemical & Pharmaceutical Bulletin 1983 31 698-708 Saponin and Sapogenol. XXXV. Chemical Constituents of Astragali Radix, the Root of Astragalus membranaceus BUNGE. (2). Astragalosides I, II and IV, Acetylastragaloside I and Isoastragalosides I and II ISAO KITAGAWA,HUIKANG WANG,MASAYUKI SAITO,AKIRA TAKAGI and MASAYUKI YOSHIKAWA Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 10 . compound 1 C12H24O7 相似度:50% Chemistry of Natural Compounds 2001 37 124-126 SYNTHESIS OF D-MANNITE ESTERS OF ALIPHATIC AND AROMATIC ACIDS A. F. Artamonov, F. S. Nigmatullina,M. T. Aldabergenova, and B. Zh. Dzhiembaev Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 11 . C-Glycoside Xiβ 相似度:50% Chemistry of Natural Compounds 1991 27 318-322 13C NMR SPECTRA OF BIOLOGICALLY. ACTIVE COMPOUNDS XI. DIASTEREOMERIC EFFECTS IN C-GLYCOSIDES L. M. Khalilov, A. Yu. Spivak, E. V. Vasil'eva,A. A. Fatykhov, N. A. Prokhorova, and G. A. Tolstikov Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 12 . cyclosieversigenin 相似度:50% Chemistry of Natural Compounds 1990 26 555-558 TRITERPENE GLYCOSIDES OF Astragalus AND THEIR GENINS XXXII. CYCLOCARPOSIDE FROM Astragalus coluteocarpus B. A. Imomnazarov, M. I. Isaev,S. S. Saboiev, and N. K. Abubakirov Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 13 . cyclosieversigenin 6-O-α-L-rhamnopyranoside C36H60O9 相似度:50% Chemistry of Natural Compounds 1990 26 555-558 TRITERPENE GLYCOSIDES OF Astragalus AND THEIR GENINS XXXII. CYCLOCARPOSIDE FROM Astragalus coluteocarpus B. A. Imomnazarov, M. I. Isaev,S. S. Saboiev, and N. K. Abubakirov Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 14 . AF-VIII 相似度:50% Chemistry of Natural Compounds 1989 25 371-372 GLUCOFRUCTANS OF Cousinia polycephala K. Turdumambetov, N. V. Plekhanova, D. A. Rakhimov,and M. R. Yagudaev Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 15 . EF-VII 相似度:50% Chemistry of Natural Compounds 1989 25 371-372 GLUCOFRUCTANS OF Cousinia polycephala K. Turdumambetov, N. V. Plekhanova, D. A. Rakhimov,and M. R. Yagudaev Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 16 . compound 3a 相似度:50% Phytochemistry 1997 45 647-650 Glycolipids from Byrsonima crassifolia Luca Rastrelli, Nunziatina De Tommasi, Ingeborg Berger, Armando Caceres, Amarillis Saravia, Francesco De Simone Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 17 . (Z)-3-Hexenyl-1-O-β-D-glucopyranoside 相似度:50% Natural Product Sciences 2008 14 100-106 Phytochemical Constituents of Schizonepeta tenuifolia Briquet Lee, Il-Kyun; Kim, Min-Ah; Lee, Seung-Young; Hong, Jong-Ki; Lee, Jei-Hyun; Lee, Kang-Ro Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 18 . α-palmityl glycerin ether(鲛肝醇) C19H40O3 相似度:50% Chinese Journal of Marine Drugs 2001 20(2) 12-15 Chemical study on secondary metabolites from ascidian Styela clava(I) LAO Yan-bin, JIANG Ting, LI Jun, FU Hong-zheng, LIN Wen-han Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 19 . 2-甲氧基-十八烷基-α-甘油醚 相似度:50% Chinese Journal of Marine Drugs 2000 19(5) 1-3 STUDIES ON THE CHEMICAL CONSTITUTIONS OF THE SPONGE SUBERITES TYLOBTUSA LEVI Li Wenlin, Mao Shilong, Yi Yanghua Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 20 . sucrose 相似度:50% Phytochemistry 1988 27 1469-1472 Galloylsucroses from rhubarbs Yoshiki Kashiwada,Gen-ichiro Nonaka,Itsuo Nishioka Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 21 . 1-(adenin-9-yl)-3-O-(phosphonomethyl)-β-D-galactofuranose sodium salt C12H18N5O8P 相似度:50% Heterocycles 2010 82 663-687 Synthesis and Anti-HIV Activity of New 3'-O-Phosphonomethyl Nucleosides Michal Cesnek and Piet Herdewijn Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 22 . methoxymethyl 3,4,5-tri-O-benzyl-β-D-fructopyranoside 相似度:50% Heterocycles 2005 66 453-468 Synthesis of Di- and Trisaccharides Comprising D-Fructopyranose with β2 → 1 Glycosidic Linkage Using β-D-fructopyranosyl Fluoride as the Fructosyl Donor Eisuke Kaji,* Emiko Kurimoto, Reiko Saiga, Ayako Matsuura, Kazuho Harada, and Takashi Nishino Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 23 . methyl-β-D-galactopyranoside 4,6-butylboronate 相似度:50% Magnetic Resonance in Chemistry 2003 41 1015-1020 Combined 1H, 13C and 11B NMR and mass spectral assignments of boronate complexes of D-(+)-glucose, D-(+)-mannose, methyl--D-glucopyranoside, methyl-β-D-galactopyranoside and methyl--D-mannopyranoside Reem Smoum, Abraham Rubinstein and Morris Srebnik Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 24 . Gancderan B 相似度:50% Phytochemistry 1986 25 2817-2820 Glycan structures of ganoderans b and c, hypoglycemic glycans of ganoderma lucidum fruit bodies Masashi Tomoda, Ryoko Gonda, Yoshimasa Kasahara, Hiroshi Hikino Structure 13C NMR 碳谱模拟图 |
5楼2013-11-05 19:24:12