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5Â¥2013-08-16 08:45:12
wangzhipengj
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baiyuefei
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yaolan123: ½ð±Ò+2, ¸ÐлӦÖú£¬½±ÀøÒ»Ï 2013-06-23 21:27:55
oven1986: ¼ìË÷EPI+1, ¸ÐлӦÖú¡£ 2013-08-16 11:06:15
yaolan123: ½ð±Ò+2, ¸ÐлӦÖú£¬½±ÀøÒ»Ï 2013-06-23 21:27:55
oven1986: ¼ìË÷EPI+1, ¸ÐлӦÖú¡£ 2013-08-16 11:06:15
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ÓÃÍøÂç°æµÄCA²éѯ¼´¿É£¬¾Í¿ÉµÃÖª¾ßÌåÊÇʲôÎÄÏ׵쬲éѯ½á¹ûÈçÏ£¬1»ò2£¬²»ÖªÄĸöÊÇÄãÐèÒªµÄ£¬×Ô¼ºÑ¡ÔñÏ塃 1. A rapid determination of total pinenes in a mixture of terpenes By: Bardyshev, I. I.; Chernyaeva, O. I.; Litvinova, A. N. The method is based on changes of temp. owing to the isomerization, polymerization, and partial esterification of ¦Á- and ¦Â-pinenes (I) with AcOH and H2SO4 under standardized exptl. conditions avoiding the reaction of other turpentine constituents. The app. consisted of a thermostat, a Dewar flask, two 10-cc. pipets (with siphoned lower parts which made it possible to keep them inserted in the thermostat), two thermometers (one inside the Dewar flask, the other outside), and a hand stirrer. The temp. was kept at 25 ¡À 0.1¡ã. The reagent was prepd. by mixing 100% AcOH and 50% H2SO4 in vol. proportions 10:1. ¦Á-Pinene (b. 155-6¡ã, nD20 1.4653-1.4656, d420 0.8578-0.8582) was used as the standard. A plot of the temp. differences, ¦¤t, against the contents of ¦Á-pinene in the mixt. gave a straight line. Since at low concns. of I it took around 30 min. to reach the max. temp. a mixt. of pure ¦Á-pinene and the substance being analyzed was prepd. in the ratio 1:1. The amt. of I in this case was calcd.: x = 2 (a - 50), where a represented ¦Á-pinene in the mixt. In the presence of larger quantities of ¦Â-pinene 1.5% was subtracted from a. Smaller quantities of camphene did not interfere. This method is superior to the fractionation method. Gidroliznaya i Lesokhimicheskaya Promyshlennost Volume8 IssueNo. 2 Pages15-17 Journal 1955 CODEN:GLKPA2 ISSN:0016-9706 2. Mixed (lichenoid and macular) cutaneous amyloidoses Toribio J; Quinones P A; Virgil T R; Santa-Cruz C S Between October 1972 and Paril 1974 a total of four patients suffering from lichen amyloidosus were admitted to the wards of the Department of Dermatology, University Hospital, Valladolid. All these patients also showed a macular amyloidosis associated with the lichenoid eruption. The authors emphasize that macular amyloidosis is quite commonly found as an associated and closely related condition in lichen amyloidosus. Acta dermato-venereologica Volume55 Issue3 Pages221-6 Journal; Article; (JOURNAL ARTICLE) 1975 ISSN:0001-5555 Journal Code:0370310 Sweden |
3Â¥2013-06-23 17:49:54
baiyuefei
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4Â¥2013-06-23 17:51:00













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