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急求钛酸钾盐的XRD衍射的标准卡片数据
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| 急求K2Ti2O5、 K2Ti3O7、 K2Ti4O9、 K2Ti5O11、 K2Ti6O13、 K2Ti8O17和TiO2-B的XRD衍射的标准卡片数据,用于标定衍射峰,应助者鄙人沉重感谢,奖励金币20。 |
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2楼2007-10-08 18:52:09
3楼2007-10-08 19:20:12
4楼2007-10-09 10:28:32
纳米镍粉
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Name and formula Reference code: 00-013-0447 PDF index name: Potassium Titanium Oxide Empirical formula: K2O9Ti4 Chemical formula: K2Ti4O9 Crystallographic parameters Crystal system: Unknown RIR: - Status, subfiles and quality Status: Marked as deleted by ICDD Subfiles: Inorganic Quality: Doubtful (O) Comments Deleted by: Deleted by 27-447. References Primary reference: Berry et al., J. Inorg. Nucl. Chem., 14, 231, (1960) Peak list No. h k l d [A] 2Theta[deg] I [%] 1 8.66000 10.206 100.0 2 6.15000 14.391 45.0 3 3.93000 22.607 12.0 4 3.74000 23.772 14.0 5 3.67000 24.232 10.0 6 3.17000 28.127 45.0 7 2.94000 30.378 50.0 8 2.87000 31.138 45.0 9 2.79000 32.054 10.0 10 2.71000 33.027 25.0 11 2.65000 33.797 40.0 12 2.19000 41.187 30.0 13 2.09000 43.254 30.0 14 1.89000 48.104 30.0 Stick Pattern |

5楼2007-10-09 17:50:16
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Name and formula Reference code: 00-013-0448 PDF index name: Potassium Titanium Oxide Empirical formula: K2O5Ti2 Chemical formula: K2Ti2O5 Crystallographic parameters Crystal system: Unknown RIR: - Status, subfiles and quality Status: Marked as deleted by ICDD Subfiles: Inorganic Corrosion Quality: Doubtful (O) Comments Deleted by: Deleted by 51-1890, indexed, single phase, LRB 11/00. References Primary reference: Berry et al., J. Inorg. Nucl. Chem., 14, 231, (1960) Peak list No. h k l d [A] 2Theta[deg] I [%] 1 6.65000 13.304 100.0 2 4.72000 18.785 6.0 3 3.29000 27.081 35.0 4 3.10000 28.776 12.0 5 3.08000 28.967 20.0 6 2.82000 31.704 12.0 7 2.76000 32.412 2.0 8 2.66000 33.666 6.0 9 2.64000 33.929 10.0 10 2.59000 34.605 4.0 11 2.44000 36.806 4.0 12 2.38000 37.768 2.0 13 2.18000 41.385 50.0 14 1.92000 47.306 8.0 15 1.89000 48.104 6.0 16 1.76000 51.911 2.0 17 1.63500 56.216 16.0 18 1.61000 57.168 2.0 19 1.59000 57.955 4.0 20 1.57000 58.765 2.0 21 1.56000 59.179 4.0 22 1.53000 60.459 8.0 23 1.35000 69.583 2.0 24 1.32000 71.403 4.0 25 1.31000 72.033 4.0 26 1.23000 77.549 4.0 27 1.21000 79.079 2.0 28 1.19000 80.678 2.0 29 1.17000 82.352 2.0 30 1.10000 88.898 2.0 31 1.06000 93.221 2.0 Stick Pattern |

6楼2007-10-09 17:50:47
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Name and formula Reference code: 00-013-0574 PDF index name: Potassium Titanium Oxide Empirical formula: K2O13Ti6 Chemical formula: K2Ti6O13 Crystallographic parameters Crystal system: Monoclinic a (?): 15.6000 b (?): 3.8000 c (?): 9.1300 Alpha (°): 90.0000 Beta (°): 99.6000 Gamma (°): 90.0000 Volume of cell (10^6 pm^3): 533.65 RIR: - Status, subfiles and quality Status: Marked as deleted by ICDD Subfiles: Inorganic Quality: Indexed (I) Comments Deleted by: Deleted by 40-403. References Primary reference: Plumley, Orr., J. Am. Chem. Soc., 83, 1289, (1961) Peak list No. h k l d [A] 2Theta[deg] I [%] 1 2 0 0 7.74000 11.423 100.0 2 -2 0 1 6.42000 13.782 80.0 3 0 0 2 4.50000 19.713 10.0 4 3 0 1 4.18000 21.239 80.0 5 1 1 0 3.67000 24.232 40.0 6 -4 0 2 3.20000 27.858 10.0 7 -1 0 3 3.03000 29.455 40.0 8 -2 0 3 2.97000 30.064 100.0 9 -1 1 2 2.91000 30.699 10.0 10 1 1 2 2.79000 32.054 40.0 11 4 1 0 2.70000 33.153 60.0 12 -3 1 2 2.66000 33.666 10.0 13 6 0 0 2.57000 34.882 40.0 14 -4 0 4 2.10000 43.038 80.0 15 6 0 2 2.08000 43.473 60.0 16 3 1 3 2.04000 44.370 10.0 17 -5 0 4 1.98000 45.790 10.0 18 0 2 0 1.90000 47.835 80.0 Stick Pattern |

7楼2007-10-09 17:51:57
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Name and formula Reference code: 00-024-0901 PDF index name: Potassium Titanium Oxide Empirical formula: K3O17Ti8 Chemical formula: K3Ti8O17 Crystallographic parameters Crystal system: Monoclinic Space group: C*/* Space group number: 12 a (?): 15.6800 b (?): 3.8090 c (?): 12.0600 Alpha (°): 90.0000 Beta (°): 95.0000 Gamma (°): 90.0000 Calculated density (g/cm^3): 3.57 Volume of cell (10^6 pm^3): 717.54 Z: 2.00 RIR: - Subfiles and Quality Subfiles: Inorganic Corrosion Quality: Indexed (I) Comments Color: Black General comments: Single crystal data taken. Sample preparation: A molten mixture of K2CO3 , TiO2 and Nb2O5 was electrolyzed under argon at 1010 C for 16 hours to yield K3Ti8O17 . Additional pattern: See ICSD 18312 (PDF 01-072-1699). References Primary reference: Watts., J. Solid State Chem., 1, 319, (1970) Peak list No. h k l d [A] 2Theta[deg] I [%] 1 1 1 0 3.70000 24.033 100.0 2 3 1 0 3.07000 29.063 60.0 3 -3 1 1 3.01000 29.655 50.0 4 -2 0 4 2.88800 30.939 60.0 5 1 1 3 2.69000 33.280 10.0 6 3 1 2 2.68100 33.395 80.0 7 -6 0 1 2.59200 34.577 10.0 8 -1 1 4 2.35800 38.134 5.0 9 -4 0 5 2.13000 42.402 20.0 10 0 2 0 1.90500 47.702 50.0 Stick Pattern |

8楼2007-10-09 17:53:35
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Name and formula Reference code: 00-027-0447 PDF index name: Potassium Titanium Oxide Empirical formula: K2O9Ti4 Chemical formula: K2Ti4O9 Crystallographic parameters Crystal system: Monoclinic a (?): 12.7400 b (?): 3.7990 c (?): 8.9300 Alpha (°): 90.0000 Beta (°): 104.1000 Gamma (°): 90.0000 Calculated density (g/cm^3): 3.28 Volume of cell (10^6 pm^3): 419.18 Z: 2.00 RIR: - Status, subfiles and quality Status: Marked as deleted by ICDD Subfiles: Inorganic Quality: Blank (B) Comments Deleted by: Deleted by 00-032-0861; McMurdie parcel 7/89. Additional pattern: To replace 00-013-0447. References Primary reference: Easteal, Udy., J. Inorg. Nucl. Chem., 35, 3956, (1973) Peak list No. h k l d [A] 2Theta[deg] I [%] 1 0 0 1 8.80000 10.044 100.0 2 -1 0 1 8.25000 10.715 40.0 3 2 0 0 6.23000 14.205 40.0 4 -2 1 1 3.17200 28.109 50.0 5 4 0 0 3.07100 29.053 30.0 6 2 1 1 2.93900 30.389 50.0 7 -1 1 2 2.87900 31.038 50.0 8 3 1 0 2.78800 32.078 20.0 9 4 0 1 2.71000 33.027 50.0 10 1 0 3 2.66000 33.666 50.0 11 1 1 3 2.17600 41.464 50.0 12 5 1 0 2.08100 43.451 50.0 13 4 0 3 1.89100 48.077 70.0 14 -1 2 1 1.84300 49.412 20.0 15 -1 0 5 1.77500 51.440 20.0 16 0 2 2 1.74200 52.488 30.0 17 -8 0 2 1.57900 58.397 30.0 18 -7 1 3 1.55300 59.472 30.0 19 5 1 3 1.53900 60.069 30.0 20 -4 2 3 1.49600 61.982 30.0 21 -8 1 1 1.46500 63.445 30.0 22 0 2 4 1.42700 65.341 30.0 23 7 1 2 1.40400 66.548 30.0 Stick Pattern |

9楼2007-10-09 17:54:31
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Name and formula Reference code: 00-032-0861 PDF index name: Potassium Titanium Oxide Empirical formula: K2O9Ti4 Chemical formula: K2Ti4O9 Crystallographic parameters Crystal system: Monoclinic Space group: C2/m Space group number: 12 a (?): 18.2500 b (?): 3.7910 c (?): 12.0100 Alpha (°): 90.0000 Beta (°): 106.4000 Gamma (°): 90.0000 Calculated density (g/cm^3): 3.45 Volume of cell (10^6 pm^3): 797.11 Z: 4.00 RIR: - Subfiles and Quality Subfiles: Inorganic Corrosion Quality: Indexed (I) Comments Color: White Sample preparation: Prepared by solid state reaction of KCl on Tl2Ti4O9 at 460 C under 10-2 torr vacuum. Additional pattern: To replace 00-027-0447. References Primary reference: Dion, M., Private Communication, (1981) Unit cell: Dion, M. et al., J. Inorg. Nucl. Chem., 40, 917, (1978) Peak list No. h k l d [A] 2Theta[deg] I [%] 1 2 0 0 8.76000 10.090 100.0 2 2 0 1 6.19000 14.297 35.0 3 0 0 2 5.75000 15.398 2.0 4 -4 0 2 4.09000 21.712 1.0 5 -2 0 3 3.95000 22.491 3.0 6 4 0 1 3.75000 23.707 3.0 7 1 1 0 3.71000 23.967 2.0 8 3 1 0 3.18000 28.037 35.0 9 4 0 2 3.08000 28.967 1.0 10 3 1 1 2.95000 30.273 35.0 11 0 0 4 2.88000 31.027 30.0 12 -4 0 4 2.80000 31.937 1.0 13 -6 0 3 2.72000 32.902 20.0 14 -3 1 3 2.66000 33.666 30.0 15 3 1 2 2.62000 34.196 4.0 16 4 0 3 2.55000 35.165 1.0 17 -1 1 4 2.34400 38.371 3.0 18 -8 0 2 2.27000 39.673 1.0 19 5 1 2 2.18600 41.266 25.0 20 2 0 5 2.08900 43.276 25.0 21 8 0 1 2.04700 44.210 2.0 22 3 1 4 1.98600 45.643 2.0 23 0 2 0 1.89500 47.969 10.0 24 2 2 0 1.85400 49.099 2.0 25 4 0 5 1.83800 49.555 1.0 26 -10 0 2 1.82700 49.874 2.0 27 -9 1 3 1.75200 52.166 2.0 28 3 1 5 1.74400 52.423 8.0 Stick Pattern |

10楼2007-10-09 17:54:49













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