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[求助]
微谱求助，急求！！各位帮忙看下，谢谢了啊~
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化合物1氘代氯仿溶剂，C谱数据如下： 14.46,18.37,20.68,23.74,30.76,58.32,61.55 化合物2氘代氯仿溶剂，C谱数据如下： 14.44,18.36,20.86,28.73,30.75,42.01,58.35,61.55,68.06,115.62,120.53,146.13 化合物3氘代氯仿溶剂，C谱数据如下： 29.85,114.33,142.53,159.51,163.57,185.40,213.59 三个化合物的微谱数据 谢谢帮助了！！ |
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yaolan123
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感谢参与，应助指数 +1
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化合物1 查询结果：共查到4个化合物(查询结果仅供参考) -------------------------------------------------------------------------------- 1 . N,N,N-tributyl-N-propanesulfonic acid ammonium hydrogen sulfate 相似度:71.4% Journal of Heterocyclic Chemistry 2010 47 63-67 Synthesis of 4H-benzopyrans catalyzed by acyclic acidic ionic liquids in aqueous media Dong Fang, Hua-Bin Zhang and Zu-Liang Liu Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 2 . N,N,N-tributyl-N-propanesulfonic acid ammonium hydrogen sulfate 相似度:71.4% Journal of Heterocyclic Chemistry 2010 47 509-512 Synthesis of 14-aryl-14H-dibenzo[a,j]xanthenes catalyzed by acyclic acidic ionic liquids Dong Fang and Zu-Liang Liu Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 3 . diethyl tetrahydropyran-2,2-dicarboxylate 相似度:62.5% Organic Magnetic Resonance 1983 21 94-107 Carbon-13 NMR spectra of saturated heterocycles: XI—Tetrahydropyrans (oxanes) Ernest L. Eliel, Muthiah Manoharan, K. Michal Pietrusiewicz and Karl D. Hargrave Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 4 . carbonyl-bis-(L-valine ethyl ester) 相似度:62.5% Organic Magnetic Resonance 1973 5 353-356 Carbon-13 and proton magnetic resonance studies of some carbonyl-bis-(amino acid esters) C. H. Lochmüller and R. W. Souter Structure 13C NMR 碳谱模拟图 |
2楼2013-05-19 17:04:07
yaolan123
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查询结果：共查到79个化合物(查询结果仅供参考) -------------------------------------------------------------------------------- 1 . 1,3-di(1-butyl)-5-iodopyrimidine-2,4(1H,3H)-dione C12H20IN2O2 相似度:58.3% Molecules 2009 14 2768-2779 Synthesis of N-Substituted 5-Iodouracils as Antimicrobial and Anticancer Agents Supaluk Prachayasittikul, Nirun Sornsongkhram, Ratchanok Pingaew, Apilak Worachartcheewan, Somsak Ruchirawat and Virapong Prachayasittikul Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 2 . (±)-(3aS,9aR)-2,3,3a,4,9,9a-Hexahydro-1H-cyclopenta-quinoline C12H15N 相似度:58.3% Journal of Heterocyclic Chemistry 2003 40 101-106 Diastereoselective synthesis of linear-fused tricyclic nitrogen heterocycles by a tandem reduction-reductive amination reaction Richard A. Bunce,Derrick M. Herron,Jason R. Lewis,Sharadsrikar V. Kotturi and Elizabeth M. Holt Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 3 . Taiwapyrone C10H14O4 相似度:58.3% Helvetica Chimica Acta 2010 93 925-933 Seven Novel Linear Polyketides from Xylaria sp. NCY2 Zhi-Yu Hu, Yao-Yao Li, Chun-Hua Lu, Ting Lin, Ping Hu and Yue-Mao Shen Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 4 . cis-carvone epoxide 相似度:58.3% Phytochemistry 1985 24 863-865 Trans-carvone oxide, a monoterpene epoxide from the fragrance of Catasetum Niels Lindquist, Merle A. Battiste, W. Mark Whitten, Norris H. Williams, Lucjan Strekowski Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 5 . 2,2,7-Trimethyl-2,3-dihydroquinazolin-4(1H)-one C11H14N2O 相似度:58.3% Journal of Heterocyclic Chemistry 2012 49 533-542 The Divergent Transformations of Aromatic o-Aminonitrile with Carbonyl Compound Jianhong Tang, Jiarong Li, Lijun Zhang, Shuling Ma, Daxin Shi, Qi Zhang, Liupan Yang, Xiuzhen Wang, Xuan Liu and Change Liu Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 6 . 9-hydroxymethyl-12-methyl-3-oxa-endo-tricy-clo[6.2.2.01,6]dodec-11-en-10-one C13H18O3 相似度:53.8% Indian Journal of Chemistry 2009 48B 1148-1155 Intramolecular cycloaddition in cyclohexa-2,4-dienone and photochemical reactions: Synthesis of 12-methyl-3-oxa-endo-tricyclo[6.2.2.01,6]dodec-11-en-10-one,and pyran annulated bicyclo[3.3.0]octane and bicyclo[4.2.0]octane frameworks Singh,Vishwakarma; Sahu,Bharat C Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 7 . 1-(4-methoxyphenyl)-2-propylpiperidine C15H23NO 相似度:53.8% Heterocycles 2006 70 335-344 Enantioselective Synthesis of ent-Sedridine and (+)-Coniine via Proline-Catalyzed Mannich Reaction Kazuhiro Nagata, Kosuke Nishimura, Masashi Yokoya, and Takashi Itoh* Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 8 . ethyl (1S,4R,5S)-5,8,8-trimethyl-3-oxo-2-oxabicyclo[3.2.1]octane-4-carboxylate C13H20O4 相似度:53.8% European Journal of Organic Chemistry 2011 5002-5011 Control of the Regio- and Diastereoselectivity for the Preparation of Highly Functionalized Terpenic Cyclopentanes through Radical Cyclization Jesús F. Arteaga, Horacio R. Diéguez, José A. González-Delgado, José F. Quílez del Moral and Alejandro F. Barrero Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 9 . compound 10b C16H30OSi 相似度:53.8% Australian Journal of Chemistry 1996 49 741-749 7,9-Dihydroxy-1,8-cineole and 2α,7-Dihydroxy-1,8-cineole: Two New Possum Urinary Metabolites RM Carman and AC Garner Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 10 . 8-Chloro-5-isopropyl-8-methylnona-2,6-dione C13H23ClO2 相似度:53.8% Chemical & Pharmaceutical Bulletin 2012 60 793-797 Titanium(IV) Chloride-Mediated Ring Cleavage and Michael Addition of 3,3-Dialkylcyclobutanones and 3-[(Trimethylsilyl)methyl]-cyclobutanones Ryosuke Okuno, Jun-ichi Matsuo, Hiroyuki Ishibashi Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 11 . (3RS,5'SR,6'SR)-(E)-3-Methyl-5-(2',5',6'-trimethyl-2'-cyclohexenylidene)-l-pentyn-3-ol 相似度:53.3% Helvetica Chimica Acta 1980 63 293-314 Synthesis and Configuration of the Eight Diastereoisomeric Racemates of Dactyloxene-B. The relative configuration of dactyloxene-B and -C Bruno Maurer, Arnold Hauser, Walter Thommen, Karl H. Schulte-Elte, Günther Ohloff Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 12 . (3RS,5'RS,6'RS)-(E)-3-Methyl-5-(2',5',6'-trimethyl-2'-cyclohexenylidene)-l-pentyn-3-ol 相似度:53.3% Helvetica Chimica Acta 1980 63 293-314 Synthesis and Configuration of the Eight Diastereoisomeric Racemates of Dactyloxene-B. The relative configuration of dactyloxene-B and -C Bruno Maurer, Arnold Hauser, Walter Thommen, Karl H. Schulte-Elte, Günther Ohloff Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 13 . compound 20 C15H22O 相似度:53.3% Canadian Journal of Chemistry 2006 84 1456-1469 Intramolecular [4 + 3] cycloadditions -Stereochemical issues in the cycloaddition reactions of cyclopentenyl cations - A synthesis of (+)-dactylol1 Michael Harmata, Paitoon Rashatasakhon, and Charles L. Barnes Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 14 . 5,5-dimethyl-2-oxo-3-(1,1,2-trimethylprop-2-enyl)-3,4,5,6-tetrahydro-2H-pyran-3-carbonitrile 相似度:50% Helvetica Chimica Acta 1999 Vol. 82 177 Photocycloaddition of 2-Oxopyran-3-carbonitriles to 2,3-Dimethylbut-2-ene Dirk Schwebel, Jeanette Ziegenbalg, Jürgen Kopf and Paul Margaretha Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 15 . 14-hydroxycornexistin 相似度:50% Journal of Natural Products 1996 59 698-700 Hydroxycornexistin: A New Phytotoxin from Paecilomyces variotii S. C. Fields, L. Mireles-Lo, and B. C. Gerwick Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 16 . N-ethylisocarvomenthylamine 相似度:50% Chemistry of Natural Compounds 1980 16 397-402 SYNTHESIS AND STUDY OF THE STRUCTURE OF NEW N-SUBSTITUTED 2-METHYL-5-(1-METHYLETHYL)CYCLOHEXYLAMINES I. I, Bardyshev, N. G. Kozlov, T. K. Vyalimyae, and T. I. Pekhk Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 17 . 2-Butyl-1-ethyl-3-methylimidazolium tetrafluoroborate C10H19N2 相似度:50% Molecules 2009 14 2181-2194 Synthesis of Two New Hemisynthetic Diterpenylhydroquinones from Natural Ent-Labdanes Luis Espinoza Catalán, Karen Catalán Marín, Alejandro Madrid Villegas, Héctor Carrasco Altamirano, Joan Villena García and Mauricio Cuellar Fritis Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 18 . 1,3,3-trimethyl-2-(methanesulfonyl-methyl)-7-oxabicyclo[2.2.1]heptane 相似度:50% Journal of Natural Products 1990 Vol 53 1357 A Short Synthesis of (±)-3',6'-Epoxycycloaurapten Michael P. DiFazio, Albert T. Sneden Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 19 . 2,4,6-trimethylnonane-1-sodium sulfate C12H25SO4Na 相似度:50% Journal of Natural Products 1991 Vol 54 302 Novel Sulfated Hydrocarbons from the Sea Cucumber Cucumaria frondosa John A. Findlay, Nurettin Yayli, Larry A. Calhoun Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 20 . compound 12 相似度:50% Journal of Natural Products 1992 Vol 55 1186 Secondary Metabolites of the Yellow and Gray Morphs of the Soft Coral Parerythropodium fulvum fulvum: Comparative Aspects D. Green, Y. Kashman, Y. Benayahu Structure 13C NMR 碳谱模拟图 |
3楼2013-05-19 17:10:01
yaolan123
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追索晨曦: 金币+20, ★★★★★最佳答案, 谢谢了啊 2013-05-19 17:12:23
追索晨曦: 金币+20, ★★★★★最佳答案, 谢谢了啊 2013-05-19 17:12:23
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查询结果：共查到2个化合物(查询结果仅供参考) -------------------------------------------------------------------------------- 1 . Compound 10 相似度:50% Bioorganic & Medicinal Chemistry Letters 1995 5 3079-3084 Aromatic guanyl hydrazones: Synthesis, structural studies and in vitro activity against Trypanosoma cruzi J. C. Messeder, L. W. Tinoco, J. D. Figueroa-Villar, E. M. Souza, R. Santa Rita and, S. L. de Castro Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 2 . [4-methylthio-3,5-bis(methoxymethoxy)phenyl]methanethiol C12H18O4S2 相似度:50% European Journal of Organic Chemistry 2010 2701-2708 Effect of Substituents on the Molecular Shapes of π-Basic Macrotricyclic Receptors Anne Lélias-Vanderperre, Emmanuel Aubert, Jean-Claude Chambron and Enrique Espinosa Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- |
4楼2013-05-19 17:10:35