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菲你莫属

铁杆木虫 (正式写手)

[求助] 微谱查询求助,多谢

溶剂氯仿,碳谱数据如下:
19.8, 20.9, 23.8, 24.4, 27.0, 30.5, 30.8, 33.3, 74.8, 101.1, 105.3, 110.4, 149.2, 159.8, 165.2, 171.6

谢谢~~
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铁杆木虫 (著名写手)

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菲你莫属: 金币+10, ★★★★★最佳答案, 谢谢! 2013-04-27 21:59:56
1 .     (+)-(R)-de-O-methyllasiodiplodin
C16H22O4     相似度:100%
Journal of Natural Products          2006          69          1218-1221
Secondary Metabolites from the Wood Bark of Durio zibethinus and Durio kutejensis
Rudiyansyah, and Mary J. Garson
Structure      13C NMR   碳谱模拟图
2 .     des-O-methyllasiodiplodin
C16H22O4     相似度:100%
Chemical & Pharmaceutical Bulletin          1991          39          2956-2961
Biologically Active Constituents of Arnebia euchroma : Structure of Arnebinol, an Ansa-Type Monoterpenylbenzenoid with Inhibitory Activity on Prostaglandin Biosynthesis
Xin-Sheng YAO,Yutaka EBIZUKA,Hiroshi NOGUCHI,Fumiyuki KIUCHI,Masaaki SHIBUYA,Yoichi IITAKA,Haruo SETO and Ushio SANKAWA
Structure      13C NMR   碳谱模拟图
3 .     de-O-methyllasiodiplodin
    相似度:100%
China Journal of Chinese Materia Medica          2009          34          414-418
Chemical constituents in roots of Osbeckia opipara
WANG Hongsheng, WANG Yuehu, SHI Yana, LI Xingyu, LONG Chunlin
Structure      13C NMR   碳谱模拟图
4 .     (R)-de-O-methyllasiodiplodin
    相似度:100%
Bioorganic & Medicinal Chemistry Letters          2011          21          1171-1175
Synthesis, modification, and evaluation of (R)-de-O-methyllasiodiplodin and analogs as nonsteroidal antagonists of mineralocorticoid receptor
Cheng-Shi Jiang, Rong Zhou , Jing-Xu Gong, Li-Li Chen, Tibor Kurtán, Xu Shen, Yue-Wei Guo
Structure      13C NMR   碳谱模拟图
5 .     des-O-methyllasiodiplodin
C16H22O4     相似度:81.2%
Phytochemistry          1991          30          287-292
Ent-14[S],16β,17-trihydroxyatisan-3-one and further constituents from Euphorbia fidjiana
Richard C. Cambie, Allick R. Lal, Peter S. Rutledge, Paul D. Woodgate
Structure      13C NMR   碳谱模拟图
6 .     6-oxo-de-O-methyllasiodiplodin
C16H20O5     相似度:68.7%
Bioorganic & Medicinal Chemistry Letters          2006          16          4205-4208
Lactones from a brown alga endophytic fungus (No. ZZF36) from the South China Sea and their antimicrobial activities
Rui-yun Yang, Chun-yuan Li, Yong-cheng Lin, Guang-tian Peng, Zhi-gang She, Shi-ning Zhou
Structure      13C NMR   碳谱模拟图
7 .     myltayl-4(12)-en-5-ol
C15H24O     相似度:56.2%
Phytochemistry          1996          42          1361-1366
Sesquiterpenoids from the liverworts Bazzania trilobata and Porella canariensis
Fumihiro Nagashima, Shiori Momosaki, Yûko Watanabe, Shigeru Takaoka, Siegfried Huneck, Yoshinori Asakawa
Structure      13C NMR   碳谱模拟图
8 .     methyl 2,4-dihydroxy-6-(8-hydroxyoctyl)benzoate
    相似度:56.2%
Journal of Natural Products          1993          Vol 56          1737
Use of Alkenylresorcinols from Ononis speciosa as Synthetic Precursors of Compounds with Potential Biological Activity
Alejandro F. Barrero, Juan F. Sánchez, Ignacio Rodríguez, Mercedes Maqueda
Structure      13C NMR   碳谱模拟图
9 .     methyl 2-(8-hydroxyoctyl)-4,6-dimethoxybenzoate
    相似度:56.2%
Journal of Natural Products          1993          Vol 56          1737
Use of Alkenylresorcinols from Ononis speciosa as Synthetic Precursors of Compounds with Potential Biological Activity
Alejandro F. Barrero, Juan F. Sánchez, Ignacio Rodríguez, Mercedes Maqueda
Structure      13C NMR   碳谱模拟图
10 .     compound 9
C15H24O3     相似度:56.2%
Organic letters          1999          1          1627-1629
First Total Synthesis of (±)-Methyl Gummiferolate Using a Homoallyl−Homoallyl Radical Rearrangement Reaction
Masahiro Toyota, Masahiro Yokota, and Masataka Ihara
Structure      13C NMR   碳谱模拟图
11 .     2-cyclohexyl-6-methyl-4-oxo-5-oxa-1-ethoxycarbonyl-1-azaspiro[2,4]bicycloheptane
C15H23NO4     相似度:56.2%
Heterocycles          2005          65          1447-1454
Spiroaziridines from 4-Substituted α-Ylidene-γ-butyro Lactones
Tecla Gasperi, M. Antonietta Loreto,* Antonella Migliorini, and Paolo A. Tardella
Structure      13C NMR   碳谱模拟图
12 .     compound 4d
C28H50Pd2     相似度:56.2%
European Journal of Organic Chemistry          2012                   1945-1952
Development of the First Menthane-Based Chiral Bis(π-allylpalladium) Catalysis: Asymmetric Allylation of Imines
Rodney A. Fernandes and Dipali A. Chaudhari
Structure      13C NMR   碳谱模拟图
13 .     compound 4e
C30H54Pd2     相似度:56.2%
European Journal of Organic Chemistry          2012                   1945-1952
Development of the First Menthane-Based Chiral Bis(π-allylpalladium) Catalysis: Asymmetric Allylation of Imines
Rodney A. Fernandes and Dipali A. Chaudhari
Structure      13C NMR   碳谱模拟图
14 .     compound 4f
C28H50Pd2     相似度:56.2%
European Journal of Organic Chemistry          2012                   1945-1952
Development of the First Menthane-Based Chiral Bis(π-allylpalladium) Catalysis: Asymmetric Allylation of Imines
Rodney A. Fernandes and Dipali A. Chaudhari
Structure      13C NMR   碳谱模拟图
15 .     (R)-2,4-dihydroxy-7-methyl-7,8,9,10,11,12-hexahydro-6-oxa-benzocyclodecen-5-one
C14H18O4     相似度:56.2%
Tetrahedron          2001          57          5377-5384
Syntheses of β-resorcylic acid derivatives, novel potato micro-tuber inducing substances isolated from Lasiodiplodia theobromae
Qing Yang, Hiroaki Toshima, Teruhiko Yoshihara
Structure      13C NMR   碳谱模拟图
16 .     norsecoswartzianin
C14H20O3     相似度:56.2%
Tetrahedron          1996          52          6339-6354
Novel sesquiterpenoids from the Colombian liverwort Porella swartziana
Motoo Tori, Katsuyuki Nakashima, Tomoko Takeda, Yukiko Kan, Shigeru Takaoka, Yoshinori Asakawa
Structure      13C NMR   碳谱模拟图
17 .     (±)-(1R*,11S*,12S*)-12-hydroxy-1-nitrobicyclo[9.3.1]pentadecan-15-one
C15H25NO4     相似度:56.2%
European Journal of Organic Chemistry          2011                   2101-2110
A General, Diastereoselective Synthesis of Highly Functionalized Bicyclo[n.3.1]alkane Systems Based on an Anionic Domino Reaction of -Nitrocycloalkanones
Giorgio Giorgi, Sonia Miranda, Miriam Ruiz, Jean Rodriguez, Pilar López-Alvarado and J. Carlos Menéndez
Structure      13C NMR   碳谱模拟图
18 .     ethyl-2,4-dihydroxy-6-pentylbenzoate
    相似度:56.2%
Chemistry of Natural Compounds          2012          48          392-395
Secondary metabolites of the lichen Cladonia stellaris
M. P. Polovinka, N. I. Komarova, D. V. Korchagina, D. N. Sokolov and O. A. Luzina, et al.
Structure      13C NMR   碳谱模拟图
19 .     diethyl 2-decanoylmalonate
    相似度:52.9%
Heterocycles          2005          65          77-94
Synthesis and Cyclization Reaction of Pyrazolin-5-one Derivatives
Jae-Chul Jung, E. Blake Watkins, and Mitchell A. Avery*
Structure      13C NMR   碳谱模拟图
20 .     Ethylidenebis(3-prenylphloracetophenone)
C28H34O8     相似度:52.9%
European Journal of Organic Chemistry          2012                   772-779
A Multicomponent Carba-Betti Strategy to Alkylidene Heterodimers – Total Synthesis and Structure–Activity Relationships of Arzanol
Alberto Minassi, Lavinia Cicione, Andreas Koeberle, Julia Bauer, Stefan Laufer, Oliver Werz and Giovanni Appendino
Structure      13C NMR   碳谱模拟图
21 .     monoalcool
    相似度:52.9%
Química Nova          1997          20          616-620
Chemical modifications of (+)-allo-aromadendrane-10b,14-diol isolated from duguetia glabriuscula r. e. fries (r. e. fries) (annonaceae) and biological evaluation of some obtained derivatives
Lima, Dênis Pires de; Beatriz, Adilson; Ramos, Alexandre Ayoroa; Siqueira, João Máximo de; Oliveira, Celso Corrêa de; Marques, Maria Rita
Structure      13C NMR   碳谱模拟图
22 .     D2-zearalanone
    相似度:52.3%
Journal of Agricultural and Food Chemistry          2002          50          2494-2501
Concentration Levels of Zearalenone and Its Metabolites in Urine, Muscle Tissue, and Liver Samples of Pigs Fed with Mycotoxin-Contaminated Oats
Peter Zöllner, Justus Jodlbauer, Martina Kleinova, Hermann Kahlbacher, Thomas Kuhn, Werner Hochsteiner, and Wolfgang Lindner
Structure      13C NMR   碳谱模拟图
23 .     (+)-5,6-dehydrolupanine
    相似度:50%
Chemical & Pharmaceutical Bulletin          2000          48(5)          641-645
Lupin Alkaloids from Chinese Maackia amurensis
Yong-Hong WANG,Jia-Shi LI,Ze-Rong JIANG,Hajime KUBO,Kimio HIGASHIYAMA and Shigeru OHMIYA
Structure      13C NMR   碳谱模拟图
24 .     6-epi-β-cubebene
C15H24     相似度:50%
Phytochemistry          2002          59          805-810
epi-Cubebanes from Solidago canadensis
Adeleke A. Kasali, Olusegun Ekundayo, Claudia Paul, Wilfried A. König
Structure      13C NMR   碳谱模拟图
艰难困苦,玉汝于成。
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