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Pitfalls and Errors of HPLC in Pictures, Third Edition
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Pitfalls and Sources of Error Dr. Veronika R. Meyer Published Online: 6 FEB 2013 DOI: 10.1002/9783527659104.part2 Copyright © 2013 Wiley-VCH Verlag GmbH & Co. KGaA  Keywords: sources of error;mobile phase;inadequate purity;incomplete degassing;peaks;quantitative analysis;chemical reaction within the column;flow rate;run time;detection properties Summary This part contains sections titled: Mixing of the Mobile Phase Mobile Phase pH Adjustment of Mobile Phase pH Influence of the Acid Type and Concentration in the Eluent Water as an Unintentional Additive in the Mobile Phase Inadequate Purity of Mobile Phase Water Inadequate Purity of a Mobile Phase Solvent Inadequate Purity of a Mobile Phase Reagent Incomplete Degassing System Peaks and Quantitative Analysis Sample Preparation with Solid Phase Extraction Inadequate Stabilization of the Extraction Solvent Poor Choice of Sample Solvent: Peak Distortion Poor Choice of Sample Solvent: Tailing Sample Solvent and Calibration Curve Impurities in the Sample Formation of a By-Product in the Sample Solution Decomposition by the Sample Vial Artifact Peaks from the Vial Septum Formation of an Associate in the Sample Solution Precision and Accuracy with Loop Injection Injection Technique Injection of Air Sample Adsorption in the Loop Extra-Column Volumes Dwell Volume Elution at t0 Classification of C18 Reversed Phases Different Selectivity of C18 Reversed Phases Different Batches of Stationary Phase Chemical Reaction within the Column Tailing of Phosphate Compounds in the Presence of Steel Recovery and Peak Shape Problems with Proteins Double Peaks from Stable Conformers Influence of Temperature on the Separation Thermal Non-Equilibrium within the Column Influence of the Flow Rate on the Separation Influence of Run Time and Flow Rate on Gradient Separations UV Spectra and Quantitative Analysis UV Detection Wavelength Different Detection Properties of Diastereomers Fluorescence Quenching by Air Detector Overload in UV Detector Overload in ELSD Influence of the Retention Factor on Peak Height Influence of the Flow Rate on Peak Area Leaks in the HPLC Instrument Impairment of Precision as a Result of Noise Determination of Peak Area and Height at High Noise Peak Height Ratios Incompletely Resolved Peaks Area Rules for Incompletely Resolved Peaks Areas of a 1 : 10 Peak Pair Heights of a 1 : 10 Peak Pair Quantitative Analysis of a Small Peak Incompletely Resolved Peaks with Tailing Integration Threshold and Number of Detected Peaks Detector Time Constant and Peak Shape Quantitative Analysis in the 99% Range Correlation Coefficient of Calibration Curves111 [ Last edited by skdrat on 2013-7-10 at 22:57 ] |
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