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微波法合成金属氧化物纳米粉体，有人做吗？
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老板给的题目，微波法在液相中合成SnO2纳米晶，原料是SnCl4（5水），打算用水、乙醇做溶剂。 目前实验室里只有一台家用微波炉，不知道能不能用。 有谁做过微波液相合成金属氧化物纳米晶的，请指导一下！！！ 或者提供一些这方面的资料。 先谢过了！！！！！！！！！！ |
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3楼2007-09-11 18:59:26
caosw2001
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jackchen145(金币+2,VIP+0):3X积极回复
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我们组是做微波合成的，不过我现在只是偶尔做做，顺便给你提个醒，家用微波很多参数都不好控制，我们用的是美国CEM公司生产的微波反应设备。我可以给你提供一些我们组发的文章信息： 1.Ying-Jie Zhu, Wei-Wei Wang, Rui-Juan Qi, Xian-Luo Hu Microwave-assisted Synthesis of Single-crystalline Tellurium Nanorods and Nanowires in Ionic Liquids Angewandte Chemie International Edition, 43, 1410-1014 (2004). 2.Wei-Wei Wang, Ying-Jie Zhu and Li-Xia Yang ZnO/SnO2 Hollow Spheres and Hierarchical Nanosheets: Hydrothermal Preparation, Formation Mechanism and Photocatalytic Properties Advanced Functional Materials, (in press, 2006). 3.Jie-Fang Zhu, Ying-Jie Zhu Microwave-Assisted One-step Synthesis of Polyacrylamide-metal (M=Ag, Pt, Cu) Nanocomposites in Ethylene Glycol The Journal of Physical Chemistry B, 110, 8593-8597 (2006). 4.Rui-Juan Qi, Ying-Jie Zhu Microwave-assisted Synthesis of Calcium Carbonate (Vaterite) of Various Morphologies in Water-Ethylene Glycol Mixed Solvents The Journal of Physical Chemistry B, 110, 8302-8306 (2006). 5.Ya Jiang, Ying-Jie Zhu Microwave-Assisted Synthesis of Sulfide M2S3 (M = Bi, Sb) Nanorods Using an Ionic Liquid The Journal of Physical Chemistry B, 109, 4361-4364 (2005). 6.Ya Jiang, Ying-Jie Zhu, Guo-Feng Cheng Synthesis of Bi2Se3 Nanosheets by Microwave Heating Using an Ionic Liquid Crystal Growth & Design, 2006 7.Wei-Wei Wang, Ying-Jie Zhu Synthesis of PbCrO4 and Pb2CrO5 Rods via a Microwave-assisted Ionic Liquid Method Crystal Growth and Design, 5, 505-507 (2005). 8.Ming-Guo Ma, Ying-Jie Zhu, Jie-Fang Zhu, Guo-Feng Cheng Microwave-assisted Synthesis and Characterization of BaCO3 Nanorods Chemistry Letters, 2006 9.Wei-Wei Wang, Ying-Jie Zhu, Mei-Ling Ruan Microwave-assisted Synthesis and Magnetic Property of Magnetite and Hematite Nanoparticles Journal of Nanoparticle Research, 2006 10.Ya Jiang, Ying-Jie Zhu, Zi-Li Xu Rapid Synthesis of Bi2S3 Nanocrystals with Different Morphologies by Microwave Heating Materials Letters, 60, 2294-2298 (2006). 11.Wei-Wei Wang, Ying-Jie Zhu, Guo-Feng Cheng, Yue-Hong Huang Microwave-assisted Synthesis of Cupric Oxide Nanosheets and Nanowhiskers Materials Letters, 60, 609-612 (2006). 12.Wei-Wei Wang, Ying-Jie Zhu Microwave-assisted Synthesis of Cobalt Oxalate Nanorods and Their Thermal Conversion to Co3O4 Rods Materials Research Bulletin, 40, 1929-1935 (2005). 13. Ya Jiang, Ying-Jie Zhu Microwave-assisted Synthesis of Nanocrystalline Metal Sulfides Using an Ionic Liquid Chemistry Letters, 33 (10), 1390-1391 (2004). 14.Zhen-Hua Liang, Ying-Jie Zhu Microwave-assisted Synthesis of Single-crystalline CuO Nanoleaves Chemistry Letters, 33 (10), 1314-1315 (2004). 15.Xian-Luo Hu, Ying-Jie Zhu, Shi-Wei Wang Sonochemical and Microwave-assisted Synthesis of Linked Single-crystalline ZnO Rods Materials Chemistry and Physics, 88, 421-426 (2004). 16. Ying-Jie Zhu, Xian-Luo Hu Microwave-assisted Polythiol Reduction Method: A New Solid-liquid Route to Fast Preparation of Silver Nanowires Materials Letters, 58, 1517-1519 (2004). 17. Ying-Jie Zhu, Xian-Luo Hu Tellurim Nanorods and Nanowires Prepared by the Microwave-polyol Method Chemistry Letters, 33 (6), 760-761 (2004). 18Wei-Wei Wang and Ying-Jie Zhu Shape-Controlled Synthesis of Zinc Oxide by Microwave Heating Using an Imidazolium Salt Inorganic Chemistry Communications, 7, 1003-1005 (2004). |
2楼2007-09-11 17:54:11
4楼2007-09-12 07:36:51
5楼2007-11-02 21:46:37
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