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The C7 and C21 tert-butyl groups are disordered over two orientations, with occupancies of 0.567 (14) and 0.433 (14), and 0.668 (7) and 0.332 (7), respectively. The corresponding bond distances involving the disorderded atoms were restrained to be equal. The Uij components of the disordered atoms were approximated to isotropic behaviour. H atoms were positioned geometrically and allowed to ride on their parent C atoms, with C¨CH distances in the range 0.93¨C0.97 Å and with Uiso(H) = 1.5Ueq(C) for methyl H and 1.2Ueq(C) for other H atoms. ±¾È˲»ÊÇѧÎÞ»úµÄ£¬·ÒëÆðÀ´ÓеãÀ§ÄÑ£¬Çó¸ßÊÖ·ÒëÕâ¶Î»°£¬Ð»Ð»£¡ |
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