24小时热门版块排行榜    

查看: 306  |  回复: 1

tyxcn

木虫 (正式写手)

[求助] 50金币求助评审意见

各位大侠:投文章来了评审意见,恳请大家帮助,非常感谢!意见如下:The crystallography section states the datasets were collected using Mo radiation, but structure 1 was collected with Cu radiation.
The cif files are missing vital information such as the crystal system, and cif file 1 is missing hydrogen bond information (added by BOND $H in shelx).
There is a significant peak of residual electron density in structure 1. Presumably this resides beside the metal atom. A note of this peak and its position should be made in the cif file under _exptl_special_details
Modelling the solvent H2O in structure 2 as half occupancy will likely improve the overall quality of this structure.
回复此楼

» 猜你喜欢

» 本主题相关价值贴推荐,对您同样有帮助:

已阅   关注TA 给TA发消息 送TA红花 TA的回帖

luxtal

至尊木虫 (职业作家)

【答案】应助回帖

★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★
感谢参与,应助指数 +1
tyxcn: 金币+10, ★★★很有帮助, 非常感谢! 2013-03-27 10:26:01
tyxcn(lijunjie84代发): 金币+10, 感谢应助! 2013-05-20 15:33:07
The crystallography section states the datasets were collected using Mo radiation, but structure 1 was collected with Cu radiation.
确认并修改收集数据所用的衍射仪的靶材料。

The cif files are missing vital information such as the crystal system, and cif file 1 is missing hydrogen bond information (added by BOND $H in shelx).
CIF不完整,很多信息需要补齐,找个ACTA E上的例子看看。

There is a significant peak of residual electron density in structure 1. Presumably this resides beside the metal atom. A note of this peak and its position should be made in the cif file under _exptl_special_details
结构中还有很高的残余峰,要么指认为原子,要么解释原因。

Modelling the solvent H2O in structure 2 as half occupancy will likely improve the overall quality of this structure.
结构2中水分子的占有率需要精修。
What_we_observe_is_not_nature_itself,_but_nature_exposed_to_our_method_of_questioning----Werner_Karl_Heisenberg
2楼2013-03-27 09:57:27
已阅   关注TA 给TA发消息 送TA红花 TA的回帖
相关版块跳转 我要订阅楼主 tyxcn 的主题更新
最具人气热帖推荐 [查看全部] 作者 回/看 最后发表
[考研] 293求调剂 +5 世界首富 2026-03-11 5/250 2026-03-17 10:16 by Sammy2
[考研] 267一志愿南京工业大学0817化工求调剂 +6 SUICHILD 2026-03-12 6/300 2026-03-17 09:24 by 雾散后相遇lc
[考研] 274求调剂 +5 时间点 2026-03-13 5/250 2026-03-17 07:34 by 热情沙漠
[考研] 328求调剂,英语六级551,有科研经历 +3 生物工程调剂 2026-03-16 4/200 2026-03-16 20:13 by Wangjingyue
[考研] 化学调剂0703 +8 啊我我的 2026-03-11 8/400 2026-03-16 17:23 by 我的船我的海
[考研] 环境工程调剂 +6 大可digkids 2026-03-16 6/300 2026-03-16 17:16 by barlinike
[考研] 312求调剂 +3 陌宸希 2026-03-16 4/200 2026-03-16 15:06 by peike
[考研] 285求调剂 +6 ytter 2026-03-12 6/300 2026-03-16 15:05 by njzyff
[考研] 294求调剂 +3 Zys010410@ 2026-03-13 4/200 2026-03-15 10:59 by zhq0425
[考研] 085601材料工程315分求调剂 +3 yang_0104 2026-03-15 3/150 2026-03-15 10:58 by peike
[考研] 288求调剂 +4 奇点0314 2026-03-14 4/200 2026-03-14 23:04 by JourneyLucky
[考研] 中科大材料与化工319求调剂 +3 孟鑫材料 2026-03-14 3/150 2026-03-14 20:10 by ms629
[考研] 材料371求调剂 +9 鳄鱼? 2026-03-11 11/550 2026-03-13 22:53 by JourneyLucky
[考研] 求材料调剂 +5 隔壁陈先生 2026-03-12 5/250 2026-03-13 22:03 by 星空星月
[考研] 一志愿西南交大,材料专硕317求调剂 +5 lx8568 2026-03-11 5/250 2026-03-13 21:43 by peike
[考研] 310求调剂 +3 【上上签】 2026-03-11 3/150 2026-03-13 16:16 by JourneyLucky
[考研] 314求调剂 +7 无懈可击的巨人 2026-03-12 7/350 2026-03-13 15:40 by JourneyLucky
[考研] 求调剂 +3 程雨杭 2026-03-12 3/150 2026-03-13 15:06 by JourneyLucky
[考研] 289求调剂 +3 李政莹 2026-03-12 3/150 2026-03-13 11:02 by 求调剂zz
[考研] 调剂 +5 呵唔哦豁 2026-03-10 5/250 2026-03-10 22:00 by 28375m
信息提示
请填处理意见