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好书 STUDIES ON THE TRANSFORMATION FROM AN INTERMEDIATE
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Title: STUDIES ON THE TRANSFORMATION FROM AN INTERMEDIATE ALUMINOPHOSPHATE PHASE TO THREE-DIMENSIONAL OPEN-FRAMEWORKS Source: HYDROTHERMAL REACTIONS AND TECHNIQUES Author(s): CAIJIN LI State Key Laboratory of Inorganic Synthesis and Preparative Chemistry, Jilin University, Changchun 130023, P. R. China, China JIHONG YU State Key Laboratory of Inorganic Synthesis and Preparative Chemistry, Jilin University, Changchun 130023, P. R. China, China KAIXUE WANG State Key Laboratory of Inorganic Synthesis and Preparative Chemistry, Jilin University, Changchun 130023, P. R. China, China LI PENG State Key Laboratory of Inorganic Synthesis and Preparative Chemistry, Jilin University, Changchun 130023, P. R. China, China RUREN XU State Key Laboratory of Inorganic Synthesis and Preparative Chemistry, Jilin University, Changchun 130023, P. R. China, China Abstract: An intermediate aluminophosphate phase [Al2P2O8(OH)2]·2[HOCH2CH2NH3], denoted as APO-M, is isolated in a pure form during the crystallization of a three-dimensional open-framework APO-CJ3, and characterized by XRD, TG-DTA, MAS NMR, ICP and CHN analyses. Our studies show that APO-M can transform to APO-CJ3, as well as to AlPO4-21 under hydrothermal treatment. The phase transformation process has been further studied. It is believed that the phase transformation from APO-M to AlPO4-21 is via a solid-to-solid conversion process, which has been confirmed by the dry-crystal conversion experiment. Full Text: View full text in PDF format TOC: Back to Table of Contents 不知哪位可以共享？ |
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