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Dimethyl pyridine-2,6-dicarboxylate (1.0161 g) was stirred at 0 oC in MeOH (3 mL), and 30% aqueous H2SO4 (7 mL).  H2O2 (4 mL of 30% solution) and FeSO4•7 H2O (1.44 g in 8 mL H2O) were added simultaneously and separately over one hour, after which the reaction was stirred at room temperature for 25 minutes.  
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