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qqzhao

金虫 (正式写手)

[求助] 求微普解析化合物结构

化合物1
26.49,27.00,30.65,35.90,45.62,47.32,66.85,86.61,112.95,171.82,182.32
溶剂CDCl3
化合物2
15.67,17.33,18.62,19.48,21.26,22.72,26.52,26.64,29.80,34.37,34.90,37.63,45.15,47.26,47.88,51.00,116.89,123.78,140.02,148.05,217.74
溶剂CDCl3
化合物3
32.48,35.88,55.32,56.34,61.95,64.83,88.16,110.56,115.70,116.37,116.86,119.64,129.82,134.71,136.33,141.64,146.07,147.18,148.37
溶剂(CD3 )2CO
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??????1
1 .     pubinernoid A
C11H16O3     ?????:100%
Helvetica Chimica Acta          2006          Vol. 89          1169
Three Novel Terpenoids from Schisandra pubescens var. pubinervis
Sheng-Xiong Huang, Jing Yang, Wei-Lie Xiao, Yan-Ling Zhu, Rong-Tao Li, Li-Mei Li, Jian-Xin Pu, Xian Li, Sheng-Hong Li, and Han-Dong Sun
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

2 .     cyclohexenone
C11H16O3     ?????:100%
Phytochemistry          2004          65          1123-1128
Two compounds from allelopathic rice accession and their inhibitory activity on weeds and fungal pathogens
Chuihua Kong, Xiaohua Xu, Bin Zhou, Fei Hua, Chaoxian Zhang,Maoxin Zhang
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

3 .     loliolide
C15H22O4     ?????:100%
Planta Medica          1987          53          304
Loliolide (Calendin) from Calendula officinalis
G??nter Willuhn and Rolf-Gflnther Westhaus
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

4 .     Loliolide
C11H16O3     ?????:100%
Chemistry of Natural Compounds          2009          45          547-549
CYTOTOXIC CONSTITUENTS FROM Viscum coloratum
Bai-Nian Chen, Guan-E Yang, Jian-Kuan Li,Hui-Jing Du, Qing-Shan Li, and Zhao-Ming Zhang
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

5 .     Loliolide
C11H16O3     ?????:100%
Chemistry of Natural Compounds          2009          45          896-897
CHEMICAL CONSTITUENTS FROM THE AERIALPARTS OF Sophora mollis
Dong-Qing Fei, Mohammad Arfan,Jamal Rafiq, and Kun Gao
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

6 .     Loliolide
    ?????:100%
Biochemical Systematics and Ecology          2008          36          447-451
Apo-fucoxanthinoids and loliolide from the brown alga Cladostephus spongiosus f. verticillatus (Heterokonta, Sphacelariales)
Mohamed El Hattab, G??rald Culioli, Robert Valls, Mireille Richou, Louis Piovetti
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

7 .     (-)-loliolide
C11H16O3     ?????:100%
Natural Product Research          1997          10          181-186
(-)-Loliolide and Other Germination Inhibitory Active Constituents in Equisetum Arvense
Yoshikazu Hiraga; Kazuya Taino; Masashi Kurokawa; Ryukichi Takagi; Katsuo Ohkata
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

8 .     loliolide
C11H16O3     ?????:100%
Natural Product Research          2003          17          301-306
Dichotenone-A and -B: Two New Enones from the Marine Brown Alga Dictyota Dichotoma (Hudson) Lamour.
Muhammad Shaiq Ali; Muhammad Kashif Pervez; Muhammad Saleem; Farman Ahmed
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

9 .     loliolide
    ?????:100%
China Journal of Chinese Materia Medica          2009          34          1114-1116
Studies on chemical constituents from herbs of Viola yedoensis
HUANG Jiqiu, YANG Jingzhi, XUE Qingchun, YU Lei, ZHANG Dongming
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

10 .     loliolide
    ?????:100%
China Journal of Chinese Materia Medica          2009          34          2060-2062
Chemical constituents in the introduced Coleus forskohlii
ZHANG Weiwei, KONG Lingyi

??????2
1 .     neoverrucosanol
    ?????:66.6%
Chemistry Letters          1997          26          489-490
Umabanol, a New Tetracyclic Diterpene from a Marine Sponge
Junichi Tanaka, Irvina Nurrachmi and Tatsuo Higa
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

2 .     albifolione
C20H32O2     ?????:66.6%
Chemistry & Biodiversity          2012          9          2254-2261
Bioactive Sesquiterpenoids and Diterpenoids from the Liverwort Bazzania albifolia
Na Liu, Dong-Xiao Guo, Shu-Qi Wang, Yan-Yan Wang, Li Zhang, Gang Li and Hong-Xiang Lou
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

3 .     mansumbinone
    ?????:63.6%
Phytochemistry          2002          59          399-403
Two octanordammarane triterpenes from Commiphora kua
Aman Dekebo, Ermias Dagne, Lars K. Hansen, Odd R. Gautun, Arne J. Aasen
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

4 .     mansumbinone
C22H32O2     ?????:63.6%
Phytochemistry          1992          31          2065-2068
Mansumbinane derivatives from stem bark of Commiphora kua
Gordon J. Provan, Alexander I. Gray, Peter G. Waterman
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

5 .     mansumbinone
C22H34O     ?????:63.6%
Phytochemistry          1986          25          917-922
The mansumbinanes: Octanordammaranes from the resin of Commiphora incisa
Gordon J. Provan, Peter G. Waterman
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

6 .     17-hydroxy-ent-pimara-8(14),15-dien-3-one
C20H30O2     ?????:61.9%
Journal of Natural Products          2008          71(2)          195-198
Diterpenoids from the Roots of Suregada glomerulata
Ren-Yi Yan, Yong-Xia Tan, Xi-Qiang Cui, Ruo-Yun Chen, and De-Quan Yu
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

7 .     8S-Kolavic acid 18-methyl ester
    ?????:61.9%
Natural Product Communications          2007          2          9-12
A Bioactive Diterpene from Entada abyssinica
Alembert T. Tchinda, Victorine Fuendjiep, Yalemtsehay Mekonnen, Bernadette B. Ngo andErmias Dagne
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

8 .     compound 8
    ?????:61.9%
Natural Product Communications          2008          3          399-412
Structural Elucidation of Pimarane and IsopimaraneDiterpenoids: The 13C NMR Contribution
Ana M. L. Seca, Diana C. G. A. Pinto and Artur M. S. Silva
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

9 .     compound 32
    ?????:61.9%
Natural Product Communications          2008          3          399-412
Structural Elucidation of Pimarane and IsopimaraneDiterpenoids: The 13C NMR Contribution
Ana M. L. Seca, Diana C. G. A. Pinto and Artur M. S. Silva
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

10 .     compound 36
    ?????:61.9%
Natural Product Communications          2008          3          399-412
Structural Elucidation of Pimarane and IsopimaraneDiterpenoids: The 13C NMR Contribution
Ana M. L. Seca, Diana C. G. A. Pinto and Artur M. S. Silva

??????3
1 .     compound 9a
    ?????:100%
Chemical & Pharmaceutical Bulletin          1995          43          2187-2194
Studies on the Constituents of Clematis Species. VI. The Constituents of Clematis stans SIEB. et ZUCC.
Haruhisa KIZU,Hideki SHIMANA and Tsuyoshi TOMIMORI
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

2 .     cedrusin
    ?????:100%
Journal of Natural Products          1992          Vol 55          214
The Structure of a New Neolignan Glycoside from Stauntonia chinensis
Huai-Bin Wang, De-Quan Yu, Xiao-Tian Liang, Naoharu Watanabe, Masaharu Tamai, Sadafumi Omura
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

3 .     cedrusin
    ?????:100%
Acta Pharmaceutica Sinica          2001          Vol 36          832-835
STUDIES ON THE CHEMICAL CONSTITUENTS FROM PINENEEDLES OF PINUS MASSONIANA LAMB.
BI Yue-feng; ZHENG Xiao-ke; LIU Hong-min; FENG Wei-sheng; JI Chun-ru; ZHANG Yong-zhong
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

4 .     2-[2-hydroxy-5-(3-hydroxypropyl)-3-methoxyphenyl]-1-(2,3-dihydroxyphenyl)propane-1,3-diol
C19H24O7     ?????:100%
Zeitschrift f??r Naturforschung B          2010          65b          765-769
Abietane Diterpenoids and a Lignan from Pinus yunnanensis
Tao Feng, Xiang-Hai Cai, Qin-Gang Tan, and Xiao-Dong Luo
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

5 .     cedrusin
    ?????:100%
Natural Product Research and Development          2008          20          257-261
Chemical Constituents of Keteleeria evelyniana
FU Zhao-hui;ZHANG Yu-mei; TAN Ning-hua; CHU Hong-biao; JI Chang-jiu;
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

6 .     cedrusin
    ?????:100%
Organic Magnetic Resonance          1983          21          119-121
13C NMR spectral analysis of dihydrobenzofuran lignans
P. K. Agrawal, R. P. Rastogi and B.-G. Osterdahl
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

7 .     3-O-demethyldihydrodehydrodiconiferyl alcohol
    ?????:94.7%
Journal of the Chinese Chemical Society          1999          46          811-818
Lignans, Flavonoids and Phenolic Derivatives from Taxus mairei
????(Shung-Jim Yang);??????(Jim-Min Fang);?????(Yu-Shia Cheng)
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

8 .     (7S,8R)-4,9-dihydroxy-3,3'-dimethoxy-7,8-dihydrobenzofuran-1'-propylneolignan
    ?????:85%
Acta Pharmaceutica Sinica          2003          Vol 38          927-930
Isolation and structure identification of lignans from pine needles of pinus massoniana Lamb.
FENG Wei-sheng; ZHENG Xiao-ke; WANG Yan-zhi; BI Yue-feng
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

9 .     (-)-2,3-Dihydro-2-(4-hydroxy-3-methoxyphenyl)-3-hydroxymethyl-5(-hydroxypropyl)-7-hydroxybenzofuran
C20H24O6     ?????:84.2%
Phytochemistry          1994          37          409-413
Lignans in cell cultures of Picea glehnii
Kensuke Nabeta, Megumi Hirata, Yuriko Ohki, S.W.Ananda Samaraweera, Hiroshi Okuyama
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

10 .     9-O-formacyl cedrusin
    ?????:80%
Natural Product Research          2004          18          439-446
Chemical constituents from Pseudolarix Kaempferi
Sheng-Ping Yang; Ying Wang; Yan Wu; Jian-Min Yue
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