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- ɳ·¢: 2
- Ìû×Ó: 527
- ÔÚÏß: 115.3Сʱ
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lichun1210: ½ð±Ò+1, ¹ÄÀø»ØÌû~ 2012-05-15 00:01:06
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À¤µÄ·çóÝ: »ØÌûÖö¥ 2012-05-14 23:18:44
lichun1210: ½ð±Ò+1, ¹ÄÀø»ØÌû~ 2012-05-15 00:01:06
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2.3.1.2. cis-Ru(phen)2Cl2.RuCl3¡¤3H2O(3.92g,15 mmol),1,10-phenanthrolinemonohydrate(5.95g,30 mmol)andLiCl(4.2g,100mmol)wererefluxedin degassedDMF(50ml)for8hunderstirring.The reactionmixturewascooledtor.t.andpouredinto 250mlof10%ofLiClaqueoussolution,stirredfor 30minandfilteredtoobtainabrown¨Cblacksolid. Thesolidwaswashedthreetimeswith25-mlportions ofwaterandether.Thecrudeproductwasrecrystal- lizedbysuspendingitin300mlof1:1water¨Cethanol andrefluxingthemixtureuntilallsolidshaddissolved toformadeepbrown¨Credsolution.Thissolutionwas filteredwhilehotandevaporateddowninthepres- enceoflithiumchloride(20g)toremoveallthealco- hol.After4hat r.t.,the cis-Ru(phen)2Cl2 complex recrystallizedleavingayellow¨Cgreenmotherliquor.Thecrystalswerecollectedandwashedwithwater(20 ml),ethanol(20ml),andfinallyether.Thecompound wasdriedundervacuum.Agreen¨Cblackproductwas obtainedin69%yield. |

7Â¥2012-05-14 17:45:25
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½ð³æ (ÕýʽдÊÖ)
ÏÐÉ¢ÈËÔ±
- CMEI: 1
- Ó¦Öú: 30 (СѧÉú)
- ½ð±Ò: 472.2
- É¢½ð: 323
- ºì»¨: 3
- ɳ·¢: 2
- Ìû×Ó: 527
- ÔÚÏß: 115.3Сʱ
- ³æºÅ: 1055398
- ×¢²á: 2010-07-11
- ÐÔ±ð: GG
- רҵ: »·¾³·ÖÎö»¯Ñ§

2Â¥2012-05-13 18:38:18
À¤µÄ·çóÝ
Òø³æ (СÓÐÃûÆø)
- Ó¦Öú: 2 (Ó×¶ùÔ°)
- ½ð±Ò: 65.5
- É¢½ð: 49
- ºì»¨: 2
- Ìû×Ó: 155
- ÔÚÏß: 102.3Сʱ
- ³æºÅ: 1426960
- ×¢²á: 2011-10-04
- ÐÔ±ð: MM
- רҵ: ÓлúºÏ³É
3Â¥2012-05-13 22:21:59
ljlnby
½ð³æ (ÕýʽдÊÖ)
ÏÐÉ¢ÈËÔ±
- CMEI: 1
- Ó¦Öú: 30 (СѧÉú)
- ½ð±Ò: 472.2
- É¢½ð: 323
- ºì»¨: 3
- ɳ·¢: 2
- Ìû×Ó: 527
- ÔÚÏß: 115.3Сʱ
- ³æºÅ: 1055398
- ×¢²á: 2010-07-11
- ÐÔ±ð: GG
- רҵ: »·¾³·ÖÎö»¯Ñ§

4Â¥2012-05-13 22:43:41
À¤µÄ·çóÝ
Òø³æ (СÓÐÃûÆø)
- Ó¦Öú: 2 (Ó×¶ùÔ°)
- ½ð±Ò: 65.5
- É¢½ð: 49
- ºì»¨: 2
- Ìû×Ó: 155
- ÔÚÏß: 102.3Сʱ
- ³æºÅ: 1426960
- ×¢²á: 2011-10-04
- ÐÔ±ð: MM
- רҵ: ÓлúºÏ³É
5Â¥2012-05-13 23:11:51
À¤µÄ·çóÝ
Òø³æ (СÓÐÃûÆø)
- Ó¦Öú: 2 (Ó×¶ùÔ°)
- ½ð±Ò: 65.5
- É¢½ð: 49
- ºì»¨: 2
- Ìû×Ó: 155
- ÔÚÏß: 102.3Сʱ
- ³æºÅ: 1426960
- ×¢²á: 2011-10-04
- ÐÔ±ð: MM
- רҵ: ÓлúºÏ³É
6Â¥2012-05-13 23:49:01
ljlnby
½ð³æ (ÕýʽдÊÖ)
ÏÐÉ¢ÈËÔ±
- CMEI: 1
- Ó¦Öú: 30 (СѧÉú)
- ½ð±Ò: 472.2
- É¢½ð: 323
- ºì»¨: 3
- ɳ·¢: 2
- Ìû×Ó: 527
- ÔÚÏß: 115.3Сʱ
- ³æºÅ: 1055398
- ×¢²á: 2010-07-11
- ÐÔ±ð: GG
- רҵ: »·¾³·ÖÎö»¯Ñ§

8Â¥2012-05-14 17:46:37
ljlnby
½ð³æ (ÕýʽдÊÖ)
ÏÐÉ¢ÈËÔ±
- CMEI: 1
- Ó¦Öú: 30 (СѧÉú)
- ½ð±Ò: 472.2
- É¢½ð: 323
- ºì»¨: 3
- ɳ·¢: 2
- Ìû×Ó: 527
- ÔÚÏß: 115.3Сʱ
- ³æºÅ: 1055398
- ×¢²á: 2010-07-11
- ÐÔ±ð: GG
- רҵ: »·¾³·ÖÎö»¯Ñ§
linhua0402313: , »¶Ó»ØÌû½»Á÷ 2012-05-15 00:50:27
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9Â¥2012-05-14 17:48:16
À¤µÄ·çóÝ
Òø³æ (СÓÐÃûÆø)
- Ó¦Öú: 2 (Ó×¶ùÔ°)
- ½ð±Ò: 65.5
- É¢½ð: 49
- ºì»¨: 2
- Ìû×Ó: 155
- ÔÚÏß: 102.3Сʱ
- ³æºÅ: 1426960
- ×¢²á: 2011-10-04
- ÐÔ±ð: MM
- רҵ: ÓлúºÏ³É
10Â¥2012-05-14 23:39:50









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