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To assess fully the correspondence of this signal with the imine carbon, we performed a cross-polarization contact time variation experiment, which shows different trends of increasing intensity for carbons with different protonation states. With the exception of the imine, all of the resonance signals between 120 and 160 ppm corresponded to quaternary carbons (aromatic and amide); therefore, we expected the intensity of the imine carbon signal to be significantly different from those of the rest of the signals in the same range |
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8814402
至尊木虫 (职业作家)
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jjxiang: 金币+10, 翻译EPI+1 2012-05-05 08:09:34
jjxiang: 金币+10, 翻译EPI+1 2012-05-05 08:09:34
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To assess fully the correspondence of this signal with the imine carbon, we performed a cross-polarization contact time variation experiment, which shows different trends of increasing intensity for carbons with different protonation states. 为全面评价信号与亚胺碳间的通信，我们进行了交叉极化接触时间变化试验，显示不同质子化状态的碳强度增加的趋势不同 |
2楼2012-05-04 16:54:58
8814402
至尊木虫 (职业作家)
- 翻译EPI: 509
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- 专业: 药物学其他科学问题
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| With the exception of the imine, all of the resonance signals between 120 and 160 ppm corresponded to quaternary carbons (aromatic and amide); 除了亚胺，所有120和160ppm间的共振信号均与季碳原子（芳香的或氨基碳）相关；therefore, we expected the intensity of the imine carbon signal to be significantly different from those of the rest of the signals in the same range因而，我们预期，亚胺碳原子信号强度将显著有别于同一范围内的其它信号。 |
3楼2012-05-04 16:59:47
8814402
至尊木虫 (职业作家)
- 翻译EPI: 509
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- 虫号: 1184404
- 注册: 2011-01-06
- 专业: 药物学其他科学问题
【答案】应助回帖
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To assess fully the correspondence of this signal with the imine carbon, we performed a cross-polarization contact time variation experiment, which shows different trends of increasing intensity for carbons with different protonation states. 为全面评价信号与亚胺碳间的通信，我们进行了交叉极化接触时间变化试验，显示不同质子化状态的碳强度增加的趋势不同 这里“通信”错了，应为“相关性”；“碳强度”改为“碳原子信号强度” |
4楼2012-05-04 17:01:27
