| 查看: 1917 | 回复: 13 | ||
| 当前只显示满足指定条件的回帖，点击这里查看本话题的所有回帖 | ||
elwew木虫 (正式写手)
|
[求助]
编辑给的回信是这样，是不是就发不了单晶了？还有什么补救办法吗
|
|
|
I have reviewed your structure report and before going into any detail I would like to ask whether there is a possibility to find a better crystal? You report only 1862 observed reflections but 268 refined parameters. Since the data/parameter ratio for a properly refined structure should approximately be 10 your data set contains not enough data to refine such a number of parameters. In additon, there are no negative intensities in the data set. Have they been merged? Probably because there were too much of them due to a either very small or unsufficiently diffracting crystal? If I additionally take into account that for a refinement with a low data/parameter ratio R values are lower due to statistic effects, your structure from my point of view does not meet the standards of Acta E. |
回复此楼» 猜你喜欢
MOF合成
已经有0人回复
-
请问各位大佬ACS投稿状态这样是成功了吗？
已经有6人回复
-
无机化学论文润色/翻译怎么收费?
已经有152人回复
mxhua
铁杆木虫 (正式写手)
- 应助: 13 (小学生)
- 金币: 6410.5
- 散金: 50
- 红花: 5
- 帖子: 765
- 在线: 1252.3小时
- 虫号: 203106
- 注册: 2006-03-01
- 专业: 催化化学
14楼2012-04-06 09:01:01
elwew
木虫 (正式写手)
- 应助: 20 (小学生)
- 金币: 1616.2
- 散金: 48
- 红花: 1
- 帖子: 503
- 在线: 152.1小时
- 虫号: 1020588
- 注册: 2010-05-17
- 性别: GG
- 专业: 有机合成
3楼2012-04-03 08:38:00
marise
木虫 (小有名气)
- 应助: 17 (小学生)
- 金币: 2303.2
- 红花: 1
- 帖子: 257
- 在线: 71.4小时
- 虫号: 434856
- 注册: 2007-08-19
- 性别: MM
- 专业: 英语翻译
elwew4楼2012-04-03 09:14:43
elwew
木虫 (正式写手)
- 应助: 20 (小学生)
- 金币: 1616.2
- 散金: 48
- 红花: 1
- 帖子: 503
- 在线: 152.1小时
- 虫号: 1020588
- 注册: 2010-05-17
- 性别: GG
- 专业: 有机合成
5楼2012-04-03 09:21:39