[交流] Se粉如何才能溶解在油胺或者十八烯中，温度，时间怎么控制啊

10楼: Originally posted by nanoli at 2012-03-28 15:52:42:
搜搜清华新上李院士的最近弟子的博士论文，中文的，说的很明白
另外,Se源可以用活性更高的Na2SeSO3代替
Se粉在亚硫酸钠水溶液中回流到黑色Se粉消失就行，用这个水溶液做Se源，反应条件温和的多
希望对你有帮助

2楼: Originally posted by cscsycy at 2012-03-28 08:23:01:
SeODE solution was prepared by adding 2-mmol Se and 20-mL ODE in a three-neck fl ask and then heating the mixture under nitrogen atmosphere at 200 °C for 2 h.