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The methylated products were hydrolyzed with 0.5 M HCl/aqueous 80% AcOH at 70 C for 0.5 h, followed by reduction and acetylation to obtain partially methylated alditol acetates (PMAAs).PMAAs were identified by their fragment ions in EI-MS and by their relative retention times in GC. Their molar ratios were estimated from the peak areas of total ion chromatograms from GC¨CMS. Relative molar ratios of [U¨C13C]PMAA from [U¨C13C]glucosyl residue and [U-12C]PMAA from [U-12C]glucosyl residue ([U¨C13C]PMAA/[U-12C]PMAA) were estimated from the peak areas of their characteristic fragment ions (m/z) detected |
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- ×¢²á: 2007-11-21
- רҵ: ΢ÉúÎïÒÅ´«ÓýÖÖѧ

4Â¥2012-02-28 22:55:14













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