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The experimental parameters for A operations had been carefully scrutinized in terms of sensitivity by using B standard solutions of 10.0 mgL-1, and signal value was employed for quantification. Many factors influence the values of the signal value, mainly X1,X2,X3,X4,X5,X6, etc. In this work, the 6 factors were optimized by uniform experimental design, with uniform design tabulation of C and corresponding use tabulation. According to the test schedule, 6 factors above were selected . At the same time, 10 levels were chosen from each factor.
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The test scheme and test the signal value were listed in Tab. 1.
Within the 6 factors selected by uniform experimental design, change the value of any one factors while keeping the other 5 factors fixed. Test the changed factor¡¯s the signal value in arsenic standard solution.
The signal value of the inspection object was processed through the D software, using quadratic polynomial stepwise regression analysis. The gotten binary regression equation is:E.
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From the equation's anova table, this model was proved to be suitable. The predicted values and measured value had a high degree of correlation. Checking critical value table of F, we got F0.05 (6,4) = H, F = 25, showing that the regression equations were significant. The regression coefficients of the equations significant test showed that within the 6 factors, the other 4 factors had significant influence on the signal value, excluding G, I.
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