| 查看: 1265 | 回复: 4 | ||
[求助]
求助！zsm-5结晶度在模板剂烧前后的变化，有没有相关英文文献？谢谢各位虫友了！
|
| 求助！zsm-5结晶度在模板剂烧前后的变化，有没有相关英文文献？谢谢！ |
回复此楼» 猜你喜欢
请问哪里可以代烧带压力的炉子？
已经有6人回复
-
关于合成MIL-125的求助
已经有0人回复
-
物理化学论文润色/翻译怎么收费?
已经有287人回复
-
双非本硕光催化方向想读博，请各位老师看看我！
已经有2人回复
-
瑞典林雪平大学范立洲课题组现招聘博士后、岗位制博士生
已经有0人回复
-
中国科大仿生界面材料科学全国重点实验室戴懿涛研究员/江雷院士团队招聘科研助理
已经有0人回复
-
中国科大仿生界面材料科学全国重点实验室戴懿涛研究员/江雷院士团队招聘科研助理
已经有0人回复
-
寻求物理化学学报最新的投稿模板！
已经有4人回复
-
东南大学杰青/海优团队招聘催化方向博士后
已经有866人回复
-
投稿咨询
已经有7人回复
-
自科面上 散金币 祈福
已经有61人回复
» 本主题相关价值贴推荐，对您同样有帮助:
- 英文文献的不付费项目，怎么回答？ 谢谢。
已经有3人回复
- 帮忙看一下几句话的英文翻译。谢谢！水处理类。帮忙改一下语法和结构。BB
已经有5人回复
- 这句英文怎么翻译好啊，谢谢啦
已经有2人回复
- 【求助】求环氧粉未涂料的专业书和涂装技术专业书（英文版最好。中文也行）谢谢！！！
已经有3人回复
- 【求助】关于ZSM-5分子筛的相对结晶度计算的疑惑
已经有6人回复
- 求助！关于aliquot在英文文献中的含义，还有iL等，谢谢！
已经有5人回复
- 【求助】求助几篇关于固体超强酸催化的英文文献，最好打包发给我谢谢
已经有3人回复
2楼2011-07-22 10:32:19
duyuhai
铁杆木虫 (正式写手)
- 应助: 6 (幼儿园)
- 贵宾: 2.5
- 金币: 7609.8
- 红花: 18
- 帖子: 881
- 在线: 183.5小时
- 虫号: 230679
- 注册: 2006-03-26
- 专业: 天体中基本物理过程的理论
★ ★ ★
tangjy(金币+3): 感谢应助！欢迎常来催化版讨论！ 2011-07-23 18:29:29
tangjy(金币+3): 感谢应助！欢迎常来催化版讨论！ 2011-07-23 18:29:29
|
Calcination of ZSM-5. An in situ synchrotron powder diffraction study. Materials Science Forum (2004), 443-444, (EPDIC 8), 319-322. Publisher: (Trans Tech Publications Ltd., ) CODEN:MSFOEP ISSN:0255-5476. Bibliographic Information Calcination of ZSM-5. An in situ synchrotron powder diffraction study. Stahl, Kenny; Gustavsson, Ester; Jacobsen, Claus J. H.; Schmidt, Iver. Department of Chemistry, Technical University of Denmark, Lyngby, Den. Materials Science Forum (2004), 443-444(EPDIC 8), 319-322. Publisher: Trans Tech Publications Ltd., CODEN: MSFOEP ISSN: 0255-5476. Journal written in English. CAN 141:286051 AN 2004:163481 CAPLUS Abstract The calcination of the zeolite ZSM-5 was studied by in situ x-ray synchrotron powder diffraction. Two samples were studied: one conventionally synthesized (CONV) and one synthesized in a charcoal matrix according to the confined space synthesis method (CSS). The powder diffraction data were collected between 375-975 K in steps of 8 K/5 min. and evaluated by Rietveld refinements. Both sets of powder diffraction patterns displayed the characteristic intensity changes for calcination, but neither of them showed the expected orthorhombic to monoclinic phase transition. Refinements of the extra-framework occupancy showed that the calcination starts at 475 K and is essentially completed at 675 K for CSS, while the CONV calcination starts at 525 K and ends at 650 K. The refinement results agree very well with the TGA results. The C matrix of the CSS sample is combusted between 700-850 K. The unit cell dimensions continuously decrease from 475-975 K. An initial slow 1.2% redn. between 375-875 K is followed by a fast 1.2% redn. between 875-950 K for the CSS sample. This 2nd unit cell redn. step is unrelated to the calcination process and does not involve any wt. loss. It is suggested that this step is a recrystn./annealing process reducing the amt. of defects and strain. Indexing -- Section 75-1 (Crystallography and Liquid Crystals) Calcination Recrystallization (calcination of ZSM-5 studied in situ by synchrotron powder diffractometry) Zeolite ZSM-5 Role: PEP (Physical, engineering or chemical process); PRP (Properties); PYP (Physical process); PROC (Process) (calcination of ZSM-5 studied in situ by synchrotron powder diffractometry) Combustion (calcination of ZSM-5 with combustion of its C matrix) 7440-44-0, Carbon, processes Role: CPS (Chemical process); PEP (Physical, engineering or chemical process); PROC (Process) (calcination of ZSM-5 with combustion of its C matrix) Supplementary Terms zeolite ZSM 5 calcination recrystn Citations 1) Madsen, C; Chem Commun 1999, 673 2) Jacobsen, C; J Am Chem Soc 2000, 122, 7116 3) Cerenius, Y; J Synchr Rad 2000, 7, 203 4) Stahl, K; J Appl Crystallogr 2000, 33, 394 5) Koningsveld, H; Acta Crystallogr B 1987, 43, 127 6) Koningsveld, H; Zeolites 1990, 10, 235 |
3楼2011-07-22 15:46:42
4楼2011-07-23 15:49:04
duyuhai
铁杆木虫 (正式写手)
- 应助: 6 (幼儿园)
- 贵宾: 2.5
- 金币: 7609.8
- 红花: 18
- 帖子: 881
- 在线: 183.5小时
- 虫号: 230679
- 注册: 2006-03-26
- 专业: 天体中基本物理过程的理论
5楼2011-07-25 09:57:07
20