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dwaww(金币+1, 翻译EPI+1): 谢啦 可是只有一段呀 2011-03-20 19:44:38
Acetic acid was supplied by Sigma and ethanol and ethyl acetate were supplied by Merck. The components were degassed ultrasonically,dried over molecular sieves (type4A,Aldrich),and kept in an inert argon with a maximum water content of 2*10-6mass fraction. Their mass fraction purities were>99 mass% for acetic acid and>99.8 mass% for methanol,ethanol and ethyl acetate. The water was bidistillated and deionized.
醋酸由Sigma公司提供,乙醇和乙酸乙酯为Merck公司产品。这些原料经超声脱除空气、分子筛(4A型,Aldrich公司产品)干燥,然后保存在内充氩气的干燥器中(里面水含量最大不超过2*10-6质量分数)。醋酸的质量分数纯度大于99%,而乙醇和乙酸乙酯的质量分数超过99.8%。水为二次蒸馏、去离子水。 |
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