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qingming1984

木虫 (著名写手)


[交流] 【求助】审稿意见,怎么解决

审稿意见:
1、Esd's for a, c and c are abnormally large, assuming that your crystal was collected using a CCD detector. The used cell looks like to be a preliminary cell, which was (wrongly) maintained until the last steps of refinement. Please check if cell parameters were actually refined, and process to refine the structure again. All files (except scheme) must be updated.
Note that this cell inaccuracy generates an ALERT B in the PLATON listing, which should be addressed.
  
    refine时,有个B类错误:
PLAT148_ALERT_3_B su on the      a  - Axis is Too Large (x 1000) .         30 Ang.
PLAT148_ALERT_3_B su on the      b  - Axis is Too Large (x 1000) .          5 Ang.
PLAT148_ALERT_3_B su on the      c  - Axis is Too Large (x 1000) .         14 Ang.
   这个错误怎么解决呢?请高手赐教。

2、During refinement, please omit reflection 100, which is actually not measured because of the beam-stopper (this fact is also claimed in a PLATON ALERT). In SHELX, just insert:
OMIT 1 0 0

    我加了这个命令,结果refine不下去,请问加在那个文件里?我加的是ins文件里。

多谢高手帮我解决啊
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guozhichao88

木虫 (正式写手)


同问,请指教
2楼2011-03-18 09:48:19
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454106649

木虫 (著名写手)


★
qingming1984(金币+1): 谢谢 2011-03-18 10:13:57
qingming1984(金币+1): 2011-03-18 10:14:07
yunruirui(金币+1): 谢谢参与交流 2011-03-18 14:03:24
第一个是参数误差问题,看你哪里弄错了,重新xprep试试!
第二个你加omit 1 0 0应该不会有错,这个指令就是删掉一些坏点!还有你之前用过什么omit指令没有?
新手,说一些自己观点,大家共同讨论!
3楼2011-03-18 09:53:04
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csl200

银虫 (正式写手)


1

qingming1984(金币+8): 2011-03-18 10:13:43
yunruirui: 谢谢参与 2011-03-18 14:04:11
例如:
CELL 0.71073  17.8352  12.4207  19.0287  95.005  98.890  100.120
ZERR   4.00   0.0037   0.0025   0.0039   0.070   0.060   0.050

把误差:         0.0037   0.0025   0.0039   0.070   0.060   0.050
改小一点如:      0.001     0.001     0.001     0.002    0.001  0.002

试试看能不能解决第一个问题
4楼2011-03-18 09:54:53
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454106649

木虫 (著名写手)


引用回帖:
Originally posted by csl200 at 2011-03-18 09:54:53:
例如:
CELL 0.71073  17.8352  12.4207  19.0287  95.005  98.890  100.120
ZERR   4.00   0.0037   0.0025   0.0039   0.070   0.060   0.050

把误差:         0.0037   0.0025   0.0039   0.070   0.060  ...

这样改不算造假
5楼2011-03-18 10:54:49
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