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the Ni 2p signal of NiO nanofibers could be deconvoluted into five peaks. The binding energies at 854.2, 856.1, and 861.4 eV were attributed to the Ni 2p3/2 peaks, and the 873.8 and 879.5 eV peaks were attributed to the Ni 2p1/2 peaks. The Ni 2p3/2 peaks were assigned to Ni2+ ions in the NiO nanofibers (30). The peak at 854.2 eV was due to NiO6 in octahedral symmetry, and the peak at 856.1 eV was attributed to NiO5 or Ni2+ in pyramidal symmetry according to the experimental results and theoretical calculation of Sorian et al. |
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