Znn3bq.jpeg
²é¿´: 298  |  »Ø¸´: 1
±¾Ìû²úÉú 1 ¸ö ·­ÒëEPI £¬µã»÷ÕâÀï½øÐв鿴

clytze_520

½ð³æ (СÓÐÃûÆø)


[½»Á÷] °ïæ·­ÒëÒ»¶Î»°£¬»¯¹¤µÄ£¡

Dry diglyme with NaOH pellets or CaH2, then reflux with, and distil(under reduced pressure)it from Na,CaH2,LiAlH4,NaBH4 or NaH. These operations are carried out under N2, The amine-like odour of diglyme has been removed by shaking with a weakly acidic ion-exchange resin before drying and distilling. Addition of 0.01
% NaBH4 to the distillate inhibits peroxidation. Purify it also as for dioxane. it has been passed through a 12-in column of molecular sieves to remove water and peroxides.

» ²ÂÄãϲ»¶

» ÇÀ½ð±ÒÀ²£¡»ØÌû¾Í¿ÉÒԵõ½:

²é¿´È«²¿É¢½ðÌù

ÒÑÔÄ   »Ø¸´´ËÂ¥   ¹Ø×¢TA ¸øTA·¢ÏûÏ¢ ËÍTAºì»¨ TAµÄ»ØÌû

slz146

ľ³æ (ÕýʽдÊÖ)


¡ï ¡ï ¡ï ¡ï ¡ï
clytze_520(½ð±Ò+5, ·­ÒëEPI+1): 2011-01-14 11:51:47
ringzhu(½ð±Ò+5): ~~ 2011-01-25 14:42:20
ÒÔNa,CaH2,LiAlH4,NaBH4 »òÕß NaHΪԭÁÏ£¬¾­¹ý»ØÁ÷£¬ÕôÁó£¨ÔÚ¶Ô±ÈѹÁ¦Ï£©£¬¿ÉµÃµ½´øÓÐ NaOH »òÕßCaH2¿ÅÁ£µÄ¸ÉÔïµÄ¶þ¸Ê´¼¶þ¼×ÃÑ¡£ÕâЩ²Ù×÷ÔÚµªÆø±£»¤Ï½øÐе쬶þ¸Ê´¼¶þ¼×ÃѾßÓа·ÀàÆøÎ¶£¬ÔÚ¸ÉÔïºÍÕôÁóǰÕâÐ©ÆøÎ¶¿ÉÒÔͨ¹ýÈõËáÐÔÀë×Ó½»»»Ê÷Ö¬Ïà»ìºÏ²¢Ò¡»ÎÀ´È¥³ý¡£¼ÓÈë0.01% NaBH4µ½Áó³öÎïÖÐÀ´ÒÖÖÆ¹ýÑõ»¯×÷Óá£ÖÁÓÚ¶þÑõÔÓ»·ÒÒÍ飬Ҳ¾»»¯Ëü¡£Ëü¿ÉÒÔͨ¹ýÒ»ÖÖ12ÁÐÐÍ·Ö×Óɸȥ³ýË®ºÍ¹ýÑõ»¯Îï
2Â¥2011-01-12 16:31:50
ÒÑÔÄ   »Ø¸´´ËÂ¥   ¹Ø×¢TA ¸øTA·¢ÏûÏ¢ ËÍTAºì»¨ TAµÄ»ØÌû
Ïà¹Ø°æ¿éÌø×ª ÎÒÒª¶©ÔÄÂ¥Ö÷ clytze_520 µÄÖ÷Ìâ¸üÐÂ
×î¾ßÈËÆøÈÈÌûÍÆ¼ö [²é¿´È«²¿] ×÷Õß »Ø/¿´ ×îºó·¢±í
[¿¼ÑÐ] Ò»Ö¾Ô¸0807 ÊýÒ»Ó¢Ò» 313 ÓÐûÓжþÂÖµ÷¼Á +7 emokidd 2026-04-08 7/350 2026-04-09 00:11 by Evan_Liu
[¿¼ÑÐ] »¯Ñ§µ÷¼ÁÇóÖú +13 LULONG1 2026-04-03 18/900 2026-04-08 21:54 by LULONG1
[¿¼ÑÐ] 293·ÖÇóµ÷¼Á£¬ÍâÓïΪ¶íÓï +7 ¼ÓÒ»Ò»¾Å 2026-04-07 10/500 2026-04-08 20:14 by yutian743
[¿¼ÑÐ] 288Çóµ÷¼Á£¬Ò»Ö¾Ô¸»ªÄÏÀí¹¤´óѧ071005 +11 ioodiiij 2026-04-08 11/550 2026-04-08 16:48 by tjzhao
[¿¼ÑÐ] ÇóÖú071001µ÷¼Á£¡£¡£¡ +6 »ÆÊØËÉ 2026-04-05 7/350 2026-04-08 11:54 by Öí»á·É
[¿¼ÑÐ] ²ÄÁϵ÷¼Á +13 ºº123456 2026-04-07 14/700 2026-04-07 22:53 by À´¿´Á÷ÐÇÓê10
[¿¼ÑÐ] 315Çóµ÷¼Á +17 СÑòСÑò_ 2026-04-02 18/900 2026-04-07 22:01 by lijunpoly
[¿¼ÑÐ] ±¾¿ÆÉúÎïÐÅϢѧ£¬×Ü·Ö362 Çó07 08µ÷¼Á +6 qСٻ1210 2026-04-06 6/300 2026-04-07 19:40 by macy2011
[¿¼ÑÐ] ÉúÎïѧµ÷¼Á ¿Éµ÷¼Áµ½ÉúÎïÓëÒ½Ò© +3 ÀîÕþÓ¨ 2026-04-06 3/150 2026-04-06 19:02 by macy2011
[¿¼ÑÐ] ר˶304ÕÒµ÷¼Á£¬Ò»Ïß³ÇÊÐ×îºÃ +3 ÀîlslÀî 2026-04-05 3/150 2026-04-06 12:16 by ffffjjjj
[¿¼ÑÐ] 0855Çóµ÷¼Á²ÄÁÏ +11 ºìÌÒׯׯ 2026-04-04 12/600 2026-04-06 10:26 by À¶ÔÆË¼Óê
[¿¼ÑÐ] 332Çóµ÷¼Á +17 ССÃÏ... 2026-04-05 18/900 2026-04-06 09:51 by À¶ÔÆË¼Óê
[¿¼ÑÐ] ¸´ÊÔµ÷¼Á +5 asdasdassda 2026-04-05 5/250 2026-04-06 09:32 by dongzh2009
[¿¼ÑÐ] 344²ÄÁÏÓ뻯¹¤µ÷¼Á +9 µ÷¼ÁÉϰ¶«^ 2026-04-03 9/450 2026-04-04 23:10 by happyddm
[¿¼ÑÐ] 334Çóµ÷¼Á +8 ÔøÑöÖ® 2026-04-03 8/400 2026-04-04 11:16 by w_xuqing
[¿¼ÑÐ] µ÷¼Á0855-288 +5 xÐܶþa 2026-04-03 5/250 2026-04-04 00:19 by Öí»á·É
[¿¼ÑÐ] 085601Ò»Ö¾Ô¸±±Àí325·ÖÇóµ÷¼Á +6 ÕÒµ÷¼Á£¬£¬ 2026-04-02 6/300 2026-04-03 22:20 by –¹Æ?
[¿¼ÑÐ] Êý¶þÓ¢¶þ348Çóµ÷¼Á +4 hxdzj1 2026-04-03 5/250 2026-04-03 21:25 by zhq0425
[¿¼ÑÐ] 322Çóµ÷¼Á +4 FZAC123 2026-04-03 4/200 2026-04-03 20:55 by zhq0425
[¿¼ÑÐ] 372·Ö²ÄÁÏÓ뻯¹¤£¨085600£©Ò»Ö¾Ô¸ºþÄÏ´óѧÇóµ÷¼Á +5 À¶¼ãƬ 2026-04-02 6/300 2026-04-02 21:37 by dongzh2009
ÐÅÏ¢Ìáʾ
ÇëÌî´¦ÀíÒâ¼û