24小时热门版块排行榜    

查看: 1563  |  回复: 4

beijingliu

金虫 (正式写手)

[交流] 【求助】氩气测孔体积,表面积

各位:最近听说氩气做表面吸附比氮气要好一些,打算做一下。大家知道哪里可以做吗?最好能提供联系方式!!谢谢!!!
回复此楼
已阅   回复此楼   关注TA 给TA发消息 送TA红花 TA的回帖

fengleba

银虫 (著名写手)

beijingliu(金币+1): 2010-09-20 16:57:22
气体的选择和催化剂的孔尺寸有关系吧。具体效果就不清楚。

不知道自己自备氩气钢瓶是否可以。

[ Last edited by fengleba on 2010-9-19 at 21:56 ]
招聘地点:沈阳。http://www.penhuiji88.com/cn
2楼2010-09-19 21:55:33
已阅   回复此楼   关注TA 给TA发消息 送TA红花 TA的回帖

aust_jhe

至尊木虫 (著名写手)

★ ★
催化大师(金币+2):谢谢指点,欢迎常来催化版讨论! 2010-09-20 08:34:47
beijingliu(金币+2): 2010-09-20 16:57:29
For a number of reasons, nitrogen (at 77 K) is generally considered to be the most suitable adsorptive for the determination of the surface area of non-porous, macroporous or mesoporous solids.
Since the nitrogen–surface interactions are dependent on the adsorbent structure, some variation in Am is to be expected.
it is not easy to obtain completely independent verification of BET nitrogen areas.
Argon may seem to be an alternative adsorptive for surface area determination.
An alternative is argon adsorption at 87 K, i.e. at liquid argon temperature.
A cross-sectional area, AAr, of 0.142 nm2 is usually assumed.
For operational reasons, it becomes difficult to measure the adsorption of nitrogen if the specific surface area is relatively low (i.e. if As < 2 m2 g-1).
In this event, krypton adsorption at 77 K can be used to minimize the dead space correction and hence improve the accuracy in measuring the small amounts adsorbed.
天天学习,好好向上
3楼2010-09-19 22:32:28
已阅   回复此楼   关注TA 给TA发消息 送TA红花 TA的回帖

demonyuu

木虫 (著名写手)

一次在麦克比表面仪产品介绍会上听说过氩气做比表面吸附更好,但是好像液态氩很贵吧,所以很少用?
在每一个没有你在的日子,内心不能安宁。这么久了,怎么忍得?
4楼2010-09-25 11:12:51
已阅   回复此楼   关注TA 给TA发消息 送TA红花 TA的回帖

catzzzzz

禁虫 (小有名气)

★ ★ ★
催化大师(金币+3):谢谢指点,欢迎常来催化版讨论! 2010-09-28 19:07:04
beijingliu(金币+1): 2010-09-29 08:40:04
本帖内容被屏蔽

5楼2010-09-28 17:06:08
已阅   回复此楼   关注TA 给TA发消息 送TA红花 TA的回帖
相关版块跳转 我要订阅楼主 beijingliu 的主题更新
普通表情 高级回复 (可上传附件)
最具人气热帖推荐 [查看全部] 作者 回/看 最后发表
[博后之家] 售SCI一区T0P文章,我:8.O.55.1.O54,科目全,可伽急 +3 DpSrDtM079iu 2026-08-22 5/250 2026-08-23 04:07 by OEbVnUOu01ol
[硕博家园] 售SCI一区T0P文章,我:8.O.55.1.O.5.4,科目全,可+急 +3 2JOx3r2CYEgw 2026-08-22 7/350 2026-08-23 03:55 by OEbVnUOu01ol
[论文投稿] 售SCI一区T0P文章,我:8.O.55.1.O.5.4,科目全,可+急 +3 QTy3jDtz1uLt 2026-08-21 9/450 2026-08-23 03:04 by OEbVnUOu01ol
[硕博家园] 售SCI一区T0P文章,我:8O.55.1.O.54,科目全,可伽急 +4 QTy3jDtz1uLt 2026-08-21 11/550 2026-08-23 02:55 by OEbVnUOu01ol
[考博] 售SCI文章,我:8O.5.5.1O.54,科目全,可十急 +3 DpSrDtM079iu 2026-08-22 3/150 2026-08-23 00:55 by OEbVnUOu01ol
[基金申请] 2026国自然函评费到账 +11 羊腰板 2026-08-21 11/550 2026-08-22 22:03 by lsbin3733
[基金申请] 只有每年这种时候来逛逛小木虫 +24 yaoyewhu2008 2026-08-20 26/1300 2026-08-22 17:43 by kammury
[基金申请] 今天基金会出结果吗?20260819 +16 kkkl_v 2026-08-19 17/850 2026-08-22 16:12 by 阿布Abu
[基金申请] 建议基金发布提前给出明确的时间点 +10 kulium 2026-08-21 13/650 2026-08-21 21:58 by alongwaytogo
[基金申请] 今日不放榜?网传国自然预计 8 月 27 日可查结果 +16 医学老男孩 2026-08-20 20/1000 2026-08-21 21:13 by Ldrop2023
[基金申请] 科研孤儿太难了 +17 我4大白菜 2026-08-20 18/900 2026-08-21 20:57 by zhangev
[基金申请] 时间戳又变了 +13 wuchongjun 2026-08-20 19/950 2026-08-21 17:21 by 紫杉醇
[基金申请] 感觉是下周放榜了 +7 angus9576 2026-08-17 12/600 2026-08-21 13:38 by weiyin
[基金申请] 我面上完蛋了 +7 且听虎啸 2026-08-20 8/400 2026-08-21 12:31 by 酷酷墨镜
[论文投稿] 投稿咨询 +5 wwm09 2026-08-17 7/350 2026-08-21 10:11 by 期刊论文帮手
[基金申请] 今天放榜没戏了吧 +9 yuleib84 2026-08-19 11/550 2026-08-21 10:06 by gltch
[基金申请] 基金啊基金 +4 longfie172 2026-08-20 4/200 2026-08-21 08:58 by mark mao
[基金申请] 估计是周四 +3 archvillain 2026-08-18 3/150 2026-08-21 01:48 by jnhyjjm
[基金申请] 今天放榜吗? +14 布布和一二 2026-08-19 15/750 2026-08-19 18:07 by gltch
[基金申请] 朋友圈看到的 +6 wangzilk 2026-08-18 8/400 2026-08-19 10:55 by Haru815
信息提示
请填处理意见