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莉莉丝

铁虫 (小有名气)

[交流] 【求助】B级错误。。哪位大侠帮一下 已有6人参与

_exptl_crystal_description        block
_exptl_crystal_colour             colorless
_exptl_crystal_size_max           0.16
_exptl_crystal_size_mid           0.12
_exptl_crystal_size_min           0.10
_exptl_crystal_density_meas       ?
_exptl_crystal_density_diffrn     1.878
_exptl_crystal_density_method     'not measured'
_exptl_crystal_F_000              848
_exptl_absorpt_coefficient_mu     5.577
_exptl_absorpt_correction_type    none
_exptl_absorpt_correction_T_min   ?
_exptl_absorpt_correction_T_max   ?
_exptl_absorpt_process_details    ?
  
_exptl_special_details

说是
PLAT057 Type_3 Test for correction for absorption needed
--------------------------------------------------------------------------------

You have indicated that an absorption correction has not been applied.
(_exptl_absorpt_correction_type 'none'). However, the predicted values of
Tmin & Tmax, based on the crystal dimensions given in the CIF, are
sufficiently unequal that absorption effects appear to be significant.
Therefore, the application of a suitable absorption correction would
appear to be required. Also check that the crystal dimensions given in the
CIF do represent the actual crystal dimensions as closely as possible.
Inaccuracies here can lead to a poor prediction of Tmin & Tmax and give
rise to these alerts. It should normally be possible to estimate the
crystal dimensions to 2 decimal places. Rough estimates to only 1 decimal
place may be too inaccurate to provide reliable estimates of Tmin & Tmax.

[ Last edited by 莉莉丝 on 2010-6-28 at 23:06 ]
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yunruirui

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wsht212(金币+1):谢谢交流,希望常来! 2010-06-29 12:00:27
莉莉丝(金币+1): 2010-06-29 18:01:15
你把你的晶体size填在INS文件里,然后修过之后,在吸收校正处填上multi-scan就可以了
9楼2010-06-29 11:48:06
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huahua1216

至尊木虫 (文坛精英)


yunruirui:他发错了,哈哈,谢谢回贴 2010-06-28 17:50:12
帝夫(金币+1): 2010-06-29 00:37:59
娘啊  你的错误呢~~
2楼2010-06-28 17:30:36
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gq1017

金虫 (正式写手)


帝夫(金币+1):感谢回帖交流! 2010-06-29 00:38:18
这是cif里面的一段吧 就看这  你想让别人帮你 弄点啥呢
3楼2010-06-28 21:45:42
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莉莉丝

铁虫 (小有名气)

帝夫:感谢回帖交流! 2010-06-29 00:38:27
第一次发,不是很熟,错误贴上~~
4楼2010-06-28 23:07:53
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