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huadong1985

木虫 (小有名气)

[交流] Acta 求助,请高手指教

最近投了篇Acta E,编辑回信如下

The ALERT c needs to be explained. There is something not too clear in the data set________________________________________

onlinecheck结果如下:
Alert level C
PLAT912_ALERT_4_C Missing # of FCF Reflections Above STh/L=  0.600          2   
不知该C类错误怎么解决,以及怎么回复编辑。请各位高手指教。谢谢。
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brilliant

捐助贵宾 (职业作家)

★ ★
huadong1985(金币+1):谢谢参与
huadong1985(金币+1,VIP+0): 12-14 14:14
The data collection strategy used aimed to achieve a complete data set to
2\q = 54 deg. Some higher angle data were collected in the process, but these
are generally weak, and were excluded from the refinement. (They are, however,
included in the fcf file).
2楼2009-12-14 08:47:51
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huadong1985

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引用回帖:
Originally posted by brilliant at 2009-12-14 08:47:
The data collection strategy used aimed to achieve a complete data set to
2\q = 54 deg. Some higher angle data were collected in the process, but these
are generally weak, and were excluded from  ...

请问  我就按你说的回复么?
3楼2009-12-14 14:14:08
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dpzhang

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huadong1985(金币+1):谢谢参与
huadong1985(金币+1,VIP+0): 12-14 15:09
按照楼上说的就可以
生活还要继续
4楼2009-12-14 14:42:12
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huadong1985

木虫 (小有名气)

Missing # of FCF Reflections Above STh/L=  0.600          2
上面这句话什么意思呢?还请解答。谢谢各位
5楼2009-12-14 15:09:12
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huahua1216

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★ ★
huadong1985(金币+1):谢谢参与
huadong1985(金币+1,VIP+0): 12-14 17:21
学习了~~
6楼2009-12-14 16:16:01
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brilliant

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huadong1985(金币+4,VIP+0): 12-15 16:30
Possible causes: Missing cusp of data (due to rotation about one axis),
deleted (overflow) reflections or improper stategy (orthorhombic for
monoclinic crystal etc.)


The data collection strategy used aimed to achieve a complete data set to
2\q = 54 deg. Some higher angle data were collected in the process, but these
are generally weak, and were excluded from the refinement. (They are, however,
included in the fcf file).
根据你的数据具体情况回复一下应该就可以,

[ Last edited by brilliant on 2009-12-14 at 21:17 ]
7楼2009-12-14 21:16:08
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