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huadong1985

ľ³æ (СÓÐÃûÆø)

[½»Á÷] Acta ÇóÖú£¬Çë¸ßÊÖÖ¸½Ì

×î½üͶÁËÆªActa E,±à¼­»ØÐÅÈçÏÂ

The ALERT c needs to be explained. There is something not too clear in the data set________________________________________

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Alert level C
PLAT912_ALERT_4_C Missing # of FCF Reflections Above STh/L=  0.600          2   
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brilliant

¾èÖú¹ó±ö (Ö°Òµ×÷¼Ò)

¡ï ¡ï
huadong1985(½ð±Ò+1):лл²ÎÓë
huadong1985(½ð±Ò+1,VIP+0): 12-14 14:14
The data collection strategy used aimed to achieve a complete data set to
2\q = 54 deg. Some higher angle data were collected in the process, but these
are generally weak, and were excluded from the refinement. (They are, however,
included in the fcf file).
2Â¥2009-12-14 08:47:51
ÒÑÔÄ   »Ø¸´´ËÂ¥   ¹Ø×¢TA ¸øTA·¢ÏûÏ¢ ËÍTAºì»¨ TAµÄ»ØÌû

huadong1985

ľ³æ (СÓÐÃûÆø)

ÒýÓûØÌû:
Originally posted by brilliant at 2009-12-14 08:47:
The data collection strategy used aimed to achieve a complete data set to
2\q = 54 deg. Some higher angle data were collected in the process, but these
are generally weak, and were excluded from  ...

ÇëÎÊ  ÎҾͰ´Äã˵µÄ»Ø¸´Ã´£¿
3Â¥2009-12-14 14:14:08
ÒÑÔÄ   »Ø¸´´ËÂ¥   ¹Ø×¢TA ¸øTA·¢ÏûÏ¢ ËÍTAºì»¨ TAµÄ»ØÌû

dpzhang

ľ³æ (ÕýʽдÊÖ)

¡ï ¡ï
huadong1985(½ð±Ò+1):лл²ÎÓë
huadong1985(½ð±Ò+1,VIP+0): 12-14 15:09
°´ÕÕÂ¥ÉÏ˵µÄ¾Í¿ÉÒÔ
Éú»î»¹Òª¼ÌÐø
4Â¥2009-12-14 14:42:12
ÒÑÔÄ   »Ø¸´´ËÂ¥   ¹Ø×¢TA ¸øTA·¢ÏûÏ¢ ËÍTAºì»¨ TAµÄ»ØÌû

huadong1985

ľ³æ (СÓÐÃûÆø)

Missing # of FCF Reflections Above STh/L=  0.600          2
ÉÏÃæÕâ¾ä»°Ê²Ã´ÒâË¼ÄØ£¿»¹Çë½â´ð¡£Ð»Ð»¸÷λ
5Â¥2009-12-14 15:09:12
ÒÑÔÄ   »Ø¸´´ËÂ¥   ¹Ø×¢TA ¸øTA·¢ÏûÏ¢ ËÍTAºì»¨ TAµÄ»ØÌû

huahua1216

ÖÁ×ðľ³æ (ÎÄ̳¾«Ó¢)

¡ï ¡ï
huadong1985(½ð±Ò+1):лл²ÎÓë
huadong1985(½ð±Ò+1,VIP+0): 12-14 17:21
ѧϰÁË~~
6Â¥2009-12-14 16:16:01
ÒÑÔÄ   »Ø¸´´ËÂ¥   ¹Ø×¢TA ¸øTA·¢ÏûÏ¢ ËÍTAºì»¨ TAµÄ»ØÌû

brilliant

¾èÖú¹ó±ö (Ö°Òµ×÷¼Ò)

¡ï ¡ï ¡ï ¡ï
huadong1985(½ð±Ò+4,VIP+0): 12-15 16:30
Possible causes: Missing cusp of data (due to rotation about one axis),
deleted (overflow) reflections or improper stategy (orthorhombic for
monoclinic crystal etc.)


The data collection strategy used aimed to achieve a complete data set to
2\q = 54 deg. Some higher angle data were collected in the process, but these
are generally weak, and were excluded from the refinement. (They are, however,
included in the fcf file).
¸ù¾ÝÄãµÄÊý¾Ý¾ßÌåÇé¿ö»Ø¸´Ò»ÏÂÓ¦¸Ã¾Í¿ÉÒÔ£¬

[ Last edited by brilliant on 2009-12-14 at 21:17 ]
7Â¥2009-12-14 21:16:08
ÒÑÔÄ   »Ø¸´´ËÂ¥   ¹Ø×¢TA ¸øTA·¢ÏûÏ¢ ËÍTAºì»¨ TAµÄ»ØÌû
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