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huadong1985木虫 (小有名气)
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Acta 求助,请高手指教
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最近投了篇Acta E,编辑回信如下 The ALERT c needs to be explained. There is something not too clear in the data set________________________________________ onlinecheck结果如下: Alert level C PLAT912_ALERT_4_C Missing # of FCF Reflections Above STh/L= 0.600 2 不知该C类错误怎么解决,以及怎么回复编辑。请各位高手指教。谢谢。 |
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brilliant
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huadong1985(金币+1):谢谢参与
huadong1985(金币+1,VIP+0): 12-14 14:14
huadong1985(金币+1):谢谢参与
huadong1985(金币+1,VIP+0): 12-14 14:14
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The data collection strategy used aimed to achieve a complete data set to 2\q = 54 deg. Some higher angle data were collected in the process, but these are generally weak, and were excluded from the refinement. (They are, however, included in the fcf file). |
2楼2009-12-14 08:47:51
huadong1985
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3楼2009-12-14 14:14:08

4楼2009-12-14 14:42:12
huadong1985
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5楼2009-12-14 15:09:12
huahua1216
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6楼2009-12-14 16:16:01
brilliant
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huadong1985(金币+4,VIP+0): 12-15 16:30
huadong1985(金币+4,VIP+0): 12-15 16:30
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Possible causes: Missing cusp of data (due to rotation about one axis), deleted (overflow) reflections or improper stategy (orthorhombic for monoclinic crystal etc.) The data collection strategy used aimed to achieve a complete data set to 2\q = 54 deg. Some higher angle data were collected in the process, but these are generally weak, and were excluded from the refinement. (They are, however, included in the fcf file). 根据你的数据具体情况回复一下应该就可以, [ Last edited by brilliant on 2009-12-14 at 21:17 ] |
7楼2009-12-14 21:16:08












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