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wangzhuo9736木虫 (正式写手)
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求助解决审稿意见
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1，The accuracy of micro analyses is extremely high deviations being among hundreds of percentages. That is quite surprising considering the non-phase purity problem addressed in 10) 2，I am worried about the structure of 2. There is an Rint of 21.5% and it is not in the same cell setting as 1. In my opinion, isostructural compounds should be reported in the same cell choice. I do not think the Rint would improve simply by choosing P21/c, yet I am concerned as to why this data is so much worse than that for 1. 我的化合物是两个，他们结构是一样的而且都是单斜的但是其中一个是P21/c 一个是p21/n。并且有一个Rint 值比另一个大但是查过了已经接完了呀。转化空间群也试过了都不好使。 |
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xi2004
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4楼2009-12-01 11:57:57
huahua1216
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2楼2009-12-01 11:09:02
xi2004
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小木虫(金币+0.5):给个红包，谢谢回帖交流
paopaomeng(金币+1,VIP+0):谢谢交流 12-1 11:58
小木虫(金币+0.5):给个红包，谢谢回帖交流
paopaomeng(金币+1,VIP+0):谢谢交流 12-1 11:58
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2，I am worried about the structure of 2. There is an Rint of 21.5% and it is not in the same cell setting as 1. In my opinion, isostructural compounds should be reported in the same cell choice. I do not think the Rint would improve simply by choosing P21/c, yet I am concerned as to why this data is so much worse than that for 1. 他的意见是中肯的. 要统一成P21/c 然后2要重收一个好的数据. |
3楼2009-12-01 11:57:08