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题目：Synthesis and structural characterizationof 2,3-bis(hydroxymethyl)-2,3-dinitro-1,4-butanediol tetra p-toluenesulfonate 作者：Juan Wang, Da-bin Liu & Xin-li Zhou 期刊：Research on Chemical Intermediates，201541（4）：2257-2264 |
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baiyuefei
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感谢参与，应助指数 +1
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https://apps.webofknowledge.com/ ... age=1&doc=1 Synthesis and structural characterization of 2,3-bis(hydroxymethyl)-2,3-dinitro-1,4-butanediol tetra p-toluenesulfonate 作者:Wang, J (Wang, Juan)[ 1 ] ; Liu, DB (Liu, Da-bin)[ 1 ] ; Zhou, XL (Zhou, Xin-li)[ 1 ] RESEARCH ON CHEMICAL INTERMEDIATES 卷: 41 期: 4 页: 2257-2264 DOI: 10.1007/s11164-013-1343-5 出版年: APR 2015 查看期刊信息 摘要 2,3-Bis(hydroxymethyl)-2,3-dinitro-1,4-butanediol tetra p-toluenesulfonate has been synthesized from nitromethane via condensation, cyclization, oxidative coupling, hydrolysis, and sulfonation. The total yield was 46.5 %. The structures of the title compound and intermediates were characterized by H-1 NMR, IR, and MS. X-ray single-crystal diffraction analysis revealed the title compound belongs to triclinic system; the space group is P-1. Mr = 856.89. The crystal cell data were: a = 11.341(2) nm, b = 13.743(3) nm, c = 14.845(3) nm, alpha = 104.69(3)A degrees, beta = 98.80(3)A degrees, gamma = 110.30(3)A degrees, V = 2023.7(9) nm(3), Z = 2, Dc = 1.406 g cm(-3), F(000) = 892, mu = 0.306 mm(-1), R = 0.0749, and wR (2) = 0.1893. Results from study of the thermal properties of the compound by DSC indicated its melting point and decomposition temperature were 400.25 and 510.70 K, respectively. 关键词 作者关键词:p-Toluenesulfonate; Synthesis; Crystal structure KeyWords Plus:SUPLATAST-TOSILATE 作者信息 通讯作者地址: Zhou, XL (通讯作者) Nanjing Univ Sci & Technol, Sch Chem Engn, Nanjing 210094, Jiangsu, Peoples R China. 地址: [ 1 ] Nanjing Univ Sci & Technol, Sch Chem Engn, Nanjing 210094, Jiangsu, Peoples R China 电子邮件地址:xinlizhou@yahoo.com.cn 出版商 SPRINGER, VAN GODEWIJCKSTRAAT 30, 3311 GZ DORDRECHT, NETHERLANDS 类别 / 分类 研究方向:Chemistry Web of Science 类别:Chemistry, Multidisciplinary 文献信息 文献类型:Article 语种:English 入藏号: WOS:000350895900028 ISSN: 0922-6168 eISSN: 1568-5675 其他信息 IDS 号: CD2HI Web of Science 核心合集中的 "引用的参考文献": 14 Web of Science 核心合集中的 "被引频次": 0 |
2楼2015-11-27 07:00:41
baiyuefei
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【答案】应助回帖
★ ★ ★ ★ ★
580802: 金币+5 2015-11-27 12:11:27
lazy锦溪: LS-EPI+1, 感谢应助！ 2015-11-27 12:48:28
580802: 金币+5 2015-11-27 12:11:27
lazy锦溪: LS-EPI+1, 感谢应助！ 2015-11-27 12:48:28
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3楼2015-11-27 07:00:59
