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tangzh银虫 (小有名气)
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[求助]
求硫酸银的XRD标准卡 已有1人参与
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2楼2017-01-02 22:00:27
xhtangxh
木虫 (著名写手)
有木有虫
- CMEI: 6
- 应助: 773 (博后)
- 金币: 17832.4
- 红花: 107
- 帖子: 2676
- 在线: 599.3小时
- 虫号: 428580
- 注册: 2007-08-04
- 专业: 催化化学
【答案】应助回帖
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Name and formula Reference code: 00-027-1403 Compound name: Silver Sulfate Empirical formula: Ag2O4S Chemical formula: Ag2SO4 Crystallographic parameters Crystal system: Orthorhombic Space group: Fddd Space group number: 70 a (?): 10.2690 b (?): 12.7060 c (?): 5.8181 Alpha (°): 90.0000 Beta (°): 90.0000 Gamma (°): 90.0000 Calculated density (g/cm^3): 5.45 Volume of cell (10^6 pm^3): 759.13 Z: 8.00 RIR: 2.20 Subfiles and quality Subfiles: Common Phase Corrosion Educational pattern Forensic Inorganic NBS pattern Quality: Star (S) Comments Color: Colorless Creation Date: 1970/1/1 Modification Date: 1970/1/1 Optical Data: A=1.756, B=1.775, Q=1.782, Sign=- Sample Source or Locality: The sample was obtained from J.T. Baker Chemical Company Temperature of Data Collection: Pattern taken at 25 C Analysis: Sample analysis showed: 0.001 to 0.01% each of Al, Fe, Mg, and Si; 0.0001% each of Ca and Pb. Additional Patterns: To replace 00-007-0203. Color: Colorless. References Primary reference: Natl. Bur. Stand. (U.S.) Monogr. 25, 13, 37, (1976) Peak list No. h k l d [A] 2Theta[deg] I [%] 1 1 1 1 4.69900 18.870 10.0 2 2 2 0 3.99400 22.240 25.0 3 1 3 1 3.24900 27.430 3.0 4 0 4 0 3.17700 28.064 70.0 5 3 1 1 2.87300 31.104 100.0 6 0 2 2 2.64400 33.876 90.0 7 4 0 0 2.56800 34.911 1.0 8 2 0 2 2.53000 35.452 17.0 9 3 3 1 2.42100 37.105 30.0 10 2 2 2 2.35200 38.235 3.0 11 1 5 1 2.27200 39.637 8.0 12 2 4 2 1.98000 45.790 11.0 13 2 6 0 1.95700 46.359 8.0 14 3 5 1 1.92600 47.150 30.0 15 5 1 1 1.91500 47.437 12.0 16 1 1 3 1.88400 48.267 5.0 17 5 3 1 1.76200 51.847 3.0 18 1 3 3 1.73760 52.631 3.0 19 0 6 2 1.71230 53.470 17.0 20 3 1 3 1.67300 54.830 12.0 21 6 2 0 1.65270 55.561 4.0 22 2 6 2 1.62430 56.619 1.0 23 0 8 0 1.58810 58.031 3.0 24 3 3 3 1.56750 58.868 13.0 25 3 7 1 1.54620 59.761 8.0 26 5 5 1 1.54040 60.009 6.0 27 6 0 2 1.47510 62.960 4.0 28 0 0 4 1.45420 63.971 3.0 29 3 5 3 1.40570 66.458 6.0 30 2 2 4 1.36680 68.607 3.0 31 1 9 1 1.35980 69.010 1.0 32 2 8 2 1.34570 69.838 2.0 33 6 4 2 1.33800 70.299 6.0 34 6 6 0 1.33120 70.711 6.0 35 0 4 4 1.32250 71.247 6.0 36 8 0 0 1.28370 73.749 1.0 37 3 9 1 1.27360 74.432 3.0 38 3 7 3 1.23590 77.111 3.0 39 5 5 3 1.23310 77.318 3.0 40 8 4 0 1.19050 80.637 1.0 41 2 6 4 1.16780 82.541 1.0 42 0 10 2 1.16450 82.827 3.0 43 8 2 2 1.15490 83.669 1.0 44 5 9 1 1.14080 84.944 1.0 45 1 3 5 1.11540 87.356 1.0 46 5 7 3 1.11360 87.533 1.0 47 3 1 5 1.09750 89.154 2.0 48 6 2 4 1.09190 89.735 3.0 49 3 9 3 1.08290 90.687 4.0 50 6 8 2 1.08090 90.901 3.0 51 3 11 1 1.07580 91.455 3.0 52 0 8 4 1.07270 91.795 3.0 53 3 3 5 1.06630 92.507 2.0 54 0 12 0 1.05890 93.347 1.0 55 8 6 2 1.02720 97.164 1.0 56 9 5 1 1.02460 97.494 1.0 57 6 10 0 1.02030 98.046 1.0 58 10 2 0 1.01380 98.896 1.0 59 3 5 5 1.01090 99.281 1.0 60 5 9 3 0.99760 101.095 1.0 61 5 11 1 0.99200 101.885 1.0 62 6 6 4 0.98200 103.334 2.0 63 0 2 6 0.95860 106.944 1.0 64 3 11 3 0.95310 107.842 1.0 65 3 7 5 0.94190 109.733 1.0 66 2 10 4 0.94070 109.941 1.0 67 3 13 1 0.92790 112.229 1.0 68 8 4 4 0.92100 113.518 1.0 |
3楼2017-01-04 08:46:51
xhtangxh
木虫 (著名写手)
有木有虫
- CMEI: 6
- 应助: 773 (博后)
- 金币: 17832.4
- 红花: 107
- 帖子: 2676
- 在线: 599.3小时
- 虫号: 428580
- 注册: 2007-08-04
- 专业: 催化化学
【答案】应助回帖
|
Name and formula Reference code: 00-027-1403 Compound name: Silver Sulfate Empirical formula: Ag2O4S Chemical formula: Ag2SO4 Crystallographic parameters Crystal system: Orthorhombic Space group: Fddd Space group number: 70 a (?): 10.2690 b (?): 12.7060 c (?): 5.8181 Alpha (°): 90.0000 Beta (°): 90.0000 Gamma (°): 90.0000 Calculated density (g/cm^3): 5.45 Volume of cell (10^6 pm^3): 759.13 Z: 8.00 RIR: 2.20 Subfiles and quality Subfiles: Common Phase Corrosion Educational pattern Forensic Inorganic NBS pattern Quality: Star (S) Comments Color: Colorless Creation Date: 1970/1/1 Modification Date: 1970/1/1 Optical Data: A=1.756, B=1.775, Q=1.782, Sign=- Sample Source or Locality: The sample was obtained from J.T. Baker Chemical Company Temperature of Data Collection: Pattern taken at 25 C Analysis: Sample analysis showed: 0.001 to 0.01% each of Al, Fe, Mg, and Si; 0.0001% each of Ca and Pb. Additional Patterns: To replace 00-007-0203. Color: Colorless. References Primary reference: Natl. Bur. Stand. (U.S.) Monogr. 25, 13, 37, (1976) Peak list No. h k l d [A] 2Theta[deg] I [%] 1 1 1 1 4.69900 18.870 10.0 2 2 2 0 3.99400 22.240 25.0 3 1 3 1 3.24900 27.430 3.0 4 0 4 0 3.17700 28.064 70.0 5 3 1 1 2.87300 31.104 100.0 6 0 2 2 2.64400 33.876 90.0 7 4 0 0 2.56800 34.911 1.0 8 2 0 2 2.53000 35.452 17.0 9 3 3 1 2.42100 37.105 30.0 10 2 2 2 2.35200 38.235 3.0 11 1 5 1 2.27200 39.637 8.0 12 2 4 2 1.98000 45.790 11.0 13 2 6 0 1.95700 46.359 8.0 14 3 5 1 1.92600 47.150 30.0 15 5 1 1 1.91500 47.437 12.0 16 1 1 3 1.88400 48.267 5.0 17 5 3 1 1.76200 51.847 3.0 18 1 3 3 1.73760 52.631 3.0 19 0 6 2 1.71230 53.470 17.0 20 3 1 3 1.67300 54.830 12.0 21 6 2 0 1.65270 55.561 4.0 22 2 6 2 1.62430 56.619 1.0 23 0 8 0 1.58810 58.031 3.0 24 3 3 3 1.56750 58.868 13.0 25 3 7 1 1.54620 59.761 8.0 26 5 5 1 1.54040 60.009 6.0 27 6 0 2 1.47510 62.960 4.0 28 0 0 4 1.45420 63.971 3.0 29 3 5 3 1.40570 66.458 6.0 30 2 2 4 1.36680 68.607 3.0 31 1 9 1 1.35980 69.010 1.0 32 2 8 2 1.34570 69.838 2.0 33 6 4 2 1.33800 70.299 6.0 34 6 6 0 1.33120 70.711 6.0 35 0 4 4 1.32250 71.247 6.0 36 8 0 0 1.28370 73.749 1.0 37 3 9 1 1.27360 74.432 3.0 38 3 7 3 1.23590 77.111 3.0 39 5 5 3 1.23310 77.318 3.0 40 8 4 0 1.19050 80.637 1.0 41 2 6 4 1.16780 82.541 1.0 42 0 10 2 1.16450 82.827 3.0 43 8 2 2 1.15490 83.669 1.0 44 5 9 1 1.14080 84.944 1.0 45 1 3 5 1.11540 87.356 1.0 46 5 7 3 1.11360 87.533 1.0 47 3 1 5 1.09750 89.154 2.0 48 6 2 4 1.09190 89.735 3.0 49 3 9 3 1.08290 90.687 4.0 50 6 8 2 1.08090 90.901 3.0 51 3 11 1 1.07580 91.455 3.0 52 0 8 4 1.07270 91.795 3.0 53 3 3 5 1.06630 92.507 2.0 54 0 12 0 1.05890 93.347 1.0 55 8 6 2 1.02720 97.164 1.0 56 9 5 1 1.02460 97.494 1.0 57 6 10 0 1.02030 98.046 1.0 58 10 2 0 1.01380 98.896 1.0 59 3 5 5 1.01090 99.281 1.0 60 5 9 3 0.99760 101.095 1.0 61 5 11 1 0.99200 101.885 1.0 62 6 6 4 0.98200 103.334 2.0 63 0 2 6 0.95860 106.944 1.0 64 3 11 3 0.95310 107.842 1.0 65 3 7 5 0.94190 109.733 1.0 66 2 10 4 0.94070 109.941 1.0 67 3 13 1 0.92790 112.229 1.0 68 8 4 4 0.92100 113.518 1.0 |
4楼2017-01-04 08:47:48
xhtangxh
木虫 (著名写手)
有木有虫
- CMEI: 6
- 应助: 773 (博后)
- 金币: 17832.4
- 红花: 107
- 帖子: 2676
- 在线: 599.3小时
- 虫号: 428580
- 注册: 2007-08-04
- 专业: 催化化学
【答案】应助回帖
|
Name and formula Reference code: 00-040-1471 Compound name: Silver Sulfate Empirical formula: Ag2O4S Chemical formula: Ag2SO4 Crystallographic parameters Crystal system: Hexagonal a (?): 5.5310 b (?): 5.5310 c (?): 7.4560 Alpha (°): 90.0000 Beta (°): 90.0000 Gamma (°): 120.0000 Volume of cell (10^6 pm^3): 197.53 RIR: - Status, subfiles and quality Status: Diffraction data collected at non ambient temperature Subfiles: Corrosion Inorganic Quality: Star (S) Comments Creation Date: 1970/1/1 Modification Date: 1970/1/1 Temperature of Data Collection: Pattern taken at 440 C in vacuum. References Primary reference: Masciocchi, N., Parrish, W., Powder Diffraction, 5, 50, (1990) Peak list No. h k l d [A] 2Theta[deg] I [%] 1 1 0 0 4.79202 18.500 3.0 2 1 0 1 4.03059 22.036 8.0 3 0 0 2 3.72565 23.865 1.0 4 1 0 2 2.93902 30.389 100.0 5 1 1 0 2.76419 32.362 37.0 6 2 0 1 2.27889 39.512 4.0 7 1 0 3 2.20387 40.916 1.0 8 2 0 2 2.01301 44.997 25.0 9 0 0 4 1.86268 48.855 1.0 10 2 1 0 1.80881 50.410 1.0 11 2 1 1 1.75790 51.977 2.0 12 1 0 4 1.73565 52.695 2.0 13 2 0 3 1.72313 53.107 1.0 14 2 1 2 1.62756 56.496 5.0 15 3 0 0 1.59602 57.716 2.0 16 1 1 4 1.54498 59.813 4.0 17 2 0 4 1.47027 63.191 1.0 18 2 2 0 1.38227 67.735 6.0 19 3 1 2 1.25110 76.005 2.0 20 0 0 6 1.24274 76.609 3.0 21 3 0 4 1.21262 78.875 1.0 |
5楼2017-01-04 08:48:33












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