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zyz128木虫 (小有名气)
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[求助]
求助：PDF卡片号为97-016-1796（CaAlSiN3）的XRD标准卡片已有1人参与
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如题，求助PDF #97-016-1796（CaAlSiN3）的XRD标准衍射图谱，注：应当在最新的数据库中，PDF2004的数据库中没有，非常感谢！ |
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bible2
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2楼2016-02-27 20:57:21
xhtangxh
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Name and formula Reference code: 00-039-0747 Compound name: Calcium Aluminum Silicon Nitride PDF index name: Calcium Aluminum Silicon Nitride Empirical formula: AlCaN3Si Chemical formula: CaAlSiN3 Crystallographic parameters Crystal system: Orthorhombic Space group: Ccm21 E Space group number: 36 a (?): 5.6290 b (?): 9.5840 c (?): 4.9860 Alpha (°): 90.0000 Beta (°): 90.0000 Gamma (°): 90.0000 Volume of cell (10^6 pm^3): 268.99 Z: 4.00 RIR: - Subfiles and quality Subfiles: Alloy, metal or intermetalic Inorganic Quality: Indexed (I) Comments Creation Date: 1970/1/1 Modification Date: 1970/1/1 Sample Preparation: E-phase. Decomposition product of M-phase (2CaO:Si3N4 :AlN) by hot pressing at 1500 C for 1 hour. Accompanied by AlN phase. References Primary reference: Huang, Z., Sun, W., Yan, D., J. Mater. Sci. Lett., 4, 255, (1985) Peak list No. h k l d [A] 2Theta[deg] I [%] 1 1 1 0 4.83900 18.319 10.0 2 0 2 0 4.78900 18.512 10.0 3 1 1 1 3.48200 25.562 10.0 4 2 0 0 2.81900 31.716 50.0 5 1 3 0 2.77300 32.256 100.0 6 0 0 2 2.49500 35.966 100.0 7 2 0 1 2.45300 36.604 100.0 8 1 3 1 2.42200 37.089 100.0 9 0 4 0 2.39400 37.539 10.0 10 2 2 1 2.18300 41.325 20.0 11 2 0 2 1.86600 48.763 10.0 12 1 3 2 1.85400 49.099 20.0 13 3 3 0 1.61800 56.860 50.0 14 0 6 0 1.59800 57.637 10.0 15 3 3 1 1.53900 60.069 10.0 16 2 0 3 1.43300 65.033 30.0 17 1 3 3 1.42600 65.392 20.0 18 2 2 3 1.37100 68.368 10.0 19 3 3 2 1.35600 69.231 30.0 20 2 6 1 1.33900 70.238 10.0 |
3楼2016-02-28 10:30:45