| 查看: 890 | 回复: 4 | ||
[求助]
求大神帮忙解个晶体,万分感谢(解出结果的有额外金币哦)祝大神中秋节快乐!!! 已有1人参与
|

| up |
2楼2015-10-16 06:42:27
calebby
捐助贵宾 (著名写手)
- 应助: 224 (大学生)
- 金币: 1132.1
- 散金: 963
- 红花: 58
- 帖子: 1332
- 在线: 1180.3小时
- 虫号: 1279605
- 注册: 2011-04-27
- 性别: GG
- 专业: 配位化学
【答案】应助回帖
★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ...
诸葛云: 金币+88, ★★★很有帮助, 第一个已经没有AB错误了,看着好纠结的东西啊,不过还是万分感谢您帮忙解数据! 2015-10-17 13:31:18
诸葛云: 金币+88, ★★★很有帮助, 第一个已经没有AB错误了,看着好纠结的东西啊,不过还是万分感谢您帮忙解数据! 2015-10-17 13:31:18
|
Bond precision: C-C = 0.0097 A Wavelength=0.71073 Cell: a=24.6245(5) b=24.6245(5) c=24.6245(5) alpha=90 beta=90 gamma=90 Temperature: 293 K Calculated Reported Volume 14931.5(9) 14931.5(5) Space group I -4 3 d I-43d Hall group I -4bd 2c 3 ? Moiety formula C44 H20 Br4 Eu N8 O16 ? Sum formula C44 H20 Br4 Eu N8 O16 C44 H20 Br4 Eu N8 O16 Mr 1388.25 1388.28 Dx,g cm-3 1.853 1.853 Z 12 12 Mu (mm-1) 4.548 4.548 F000 8052.0 8052.0 F000' 8040.52 h,k,lmax 29,29,29 29,26,25 Nref 2205[ 1187] 2093 Tmin,Tmax 0.382,0.441 0.434,0.495 Tmin' 0.354 Correction method= # Reported T Limits: Tmin=0.434 Tmax=0.495 AbsCorr = MULTI-SCAN Data completeness= 1.76/0.95 Theta(max)= 24.980 R(reflections)= 0.0416( 1757) wR2(reflections)= 0.1252( 2093) S = 0.798 Npar= 181 The following ALERTS were generated. Each ALERT has the format test-name_ALERT_alert-type_alert-level. Click on the hyperlinks for more details of the test. Alert level C GOODF01_ALERT_2_C The least squares goodness of fit parameter lies outside the range 0.80 <> 2.00 Goodness of fit given = 0.798 PLAT090_ALERT_3_C Poor Data / Parameter Ratio (Zmax > 18) ........ 6.56 Note PLAT309_ALERT_2_C Single Bonded Oxygen (C-O > 1.3 Ang) ........... O5 Check PLAT342_ALERT_3_C Low Bond Precision on C-C Bonds ............... 0.0097 Ang. PLAT701_ALERT_1_C Bond Calc 2.519(5), Rep 2.525(5), Dev.. 1.20 Sigma EU1 -N1 1.555 19.554 ............. Bond # 30 PLAT702_ALERT_1_C Angle Calc 127.1(2), Rep 126.8(2), Dev.. 1.50 Sigma |
» 本帖附件资源列表
-
欢迎监督和反馈:小木虫仅提供交流平台,不对该内容负责。
本内容由用户自主发布,如果其内容涉及到知识产权问题,其责任在于用户本人,如对版权有异议,请联系邮箱:xiaomuchong@tal.com - 附件 1 : 150921_ZYC_1203.rar
2015-10-16 10:24:39, 192.26 K
3楼2015-10-16 10:24:41

4楼2015-10-17 13:26:51
5楼2015-11-10 09:12:54













回复此楼
非常感谢!!!