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mattlyzx木虫 (著名写手)
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[求助]
急需δ-MnO2, JCPDS No. 80-1098的卡片 已有1人参与
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| 急需δ-MnO2, JCPDS No. 80-1098的卡片,pdf卡片或数据请发给18638627329@163.com ,或其他方式如下载,谢谢! |
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xhtangxh
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【答案】应助回帖
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mattlyzx: 金币+5, ★★★很有帮助 2015-04-28 14:35:12
mattlyzx: 金币+5, ★有帮助 2015-05-20 20:39:29
感谢参与,应助指数 +1
mattlyzx: 金币+5, ★★★很有帮助 2015-04-28 14:35:12
mattlyzx: 金币+5, ★有帮助 2015-05-20 20:39:29
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JCPDS No. 80-1098卡片是关于K.46 Mn1.54 Mn.46 O4 ( H2 O )1.4的。δ-MnO2不是纯MnO2,也可参考后一帖子的卡片信息。 Card Information Names: Potassium Manganese Oxide Hydrate Birnessite, syn Formula: K.46 Mn1.54 Mn.46 O4 ( H2 O )1.4 PDF Number: 000-80-1098 Quality: calculated Subfiles: inorganic mineral COR FIZ Cell and Symmetry Information System: monoclinic Space Group: C2/m (no. 12) a: 5.14900 b: 2.84300 c: 7.17600 b: 100.760 Density (Dx): 3.492 Z: 1 Instrument Information Radiation: CuKa1 Wavelength: 1.54060 Instrument(d): calculated Cut Off: 17.7 Instrument(I): calculated I type: peak heights I/Icor: 6.30 Comments and Additional Information ICSD Number: 068918 RM ATOM H 1 +1. 2.80 Atoms not located in unit cell. NT Rietveld profile refinement applied Temperature factor: ITF General: (K-bearing). TI Crystal structure determinations of synthetic sodium, magnesium andpotassium birnessite using TEM and the Rietveld method Literature References General: Calculated from ICSD using POWD-12++ (1997) Structure: Post, J.E., Veblen, D.R. Am. Mineral. 75 477 (1990) Peak Data Wavelength 1.5406 used to convert d to 2theta PeakList h k l d 2theta I 0 0 1 7.0498 12.5456 999 0 0 2 3.5249 25.2447 244 -2 0 1 2.5359 35.3660 30 2 0 0 2.5292 35.4623 42 1 1 0 2.4784 36.2147 39 -1 1 1 2.4081 37.3110 108 0 0 3 2.3499 38.2690 2 1 1 1 2.2739 39.6005 12 -2 0 2 2.2650 39.7634 8 2 0 1 2.2508 40.0242 91 -1 1 2 2.1207 42.5953 114 1 1 2 1.9454 46.6501 23 -2 0 3 1.9084 47.6112 17 2 0 2 1.8943 47.9875 33 -1 1 3 1.7889 51.0092 78 0 0 4 1.7625 51.8314 9 1 1 3 1.6323 56.3137 19 -2 0 4 1.5921 57.8680 11 2 0 3 1.5807 58.3278 22 -1 1 4 1.5027 61.6740 17 -3 1 1 1.4678 63.3076 21 3 1 0 1.4503 64.1635 31 -3 1 2 1.4241 65.4904 25 0 2 0 1.4215 65.6232 25 0 0 5 1.4100 66.2284 2 0 2 1 1.3935 67.1162 11 1 1 4 1.3780 67.9706 30 3 1 1 1.3780 67.9706 30 -2 0 5 1.3427 70.0115 10 2 0 4 1.3336 70.5649 5 -3 1 3 1.3336 70.5649 5 0 2 2 1.3183 71.5043 12 -4 0 1 1.2872 73.5123 1 -1 1 5 1.2767 74.2151 7 3 1 2 1.2713 74.5886 5 -4 0 2 1.2680 74.8179 9 4 0 0 1.2646 75.0489 6 -2 2 1 1.2400 76.8082 6 2 2 0 1.2400 76.8082 6 -3 1 4 1.2201 78.2944 4 0 2 3 1.2163 78.5892 3 -4 0 3 1.2120 78.9184 5 4 0 1 1.2062 79.3727 1 -2 2 2 1.2040 79.5474 2 2 2 1 1.2019 79.7173 12 1 1 5 1.1800 81.5022 8 0 0 6 1.1750 81.9264 5 3 1 3 1.1541 83.7370 1 -2 0 6 1.1509 84.0283 4 2 0 5 1.1440 84.6443 2 -2 2 3 1.1400 85.0146 4 2 2 2 1.1370 85.2948 8 -4 0 4 1.1325 85.7121 5 4 0 2 1.1254 86.3828 3 0 2 4 1.1065 88.2404 3 -3 1 5 1.1034 88.5521 2 -1 1 6 1.1014 88.7500 1 |
2楼2015-04-28 11:07:02
xhtangxh
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Card Information Names: Sodium Manganese Oxide Hydrate Birnessite, syn Formula: Na0.55 Mn2 O4 !1.5 H2 O PDF Number: 000-43-1456 Quality: star Subfiles: inorganic mineral COR Cell and Symmetry Information System: monoclinic Space Group: C2/m (no. 12) a: 5.175 b: 2.849 c: 7.338 b: 103.19 Density (Dm): 3.000 Z: 1 Instrument Information Radiation: CuKa1 Wavelength: 1.54059 Instrument(d): diffractometer Instrument(I): diffractometer I type: unknown I/Icor: 6.70 Comments and Additional Information Colour: Black Preparation: Sample prepared by oxygenating Mn Cl2 + NaOH in aqueous solution. (Prepared by D.C. Golden). Analysis: Chemical analysis: Na0.55 Mn2 O4 !1.4 H2 O. General: Patterns from natural birnessite specimens typically show broad reflections; only 00l reflections might be prominent. Structure: Rancieite is the Ca analogue. Optical: A=1.69, B=1.73, Sign=- General: Optical data on specimen from Birness, Aberdeenshire, Scotland, UK. Literature References General: Post, J., National Museum of Natural History,Smithsonian Institution, Washington, DC, USA. ICDD Grant-in-Aid (1989) Unit Cell: Post, J., Veblen, D. Am. Mineral. 75 477 (1990) Optical: Jones, L., Milne, A. Mineral. Mag. 31 283 (1956) Peak Data Wavelength 1.5406 used to convert d to 2theta PeakList h k l d 2theta I 0 0 1 7.1440 12.3796 100 0 0 2 3.5720 24.9066 27 2 0 -1 2.5670 34.9236 1 2 0 0 2.5190 35.6112 14 1 1 0 2.4800 36.1904 2 1 1 -1 2.4290 36.9775 13 2 0 -2 2.3240 38.7131 2 1 1 1 2.2650 39.7634 2 2 0 1 2.2220 40.5664 5 1 1 -2 2.1540 41.9063 7 1 1 2 1.9378 46.8443 1 2 0 2 1.8678 48.7113 3 1 1 -3 1.8231 49.9865 4 0 0 4 1.7861 51.0956 1 2 0 -4 1.6449 55.8459 2 1 1 3 1.6288 56.4470 2 2 0 3 1.5618 59.1023 1 1 1 -4 1.5333 60.3135 2 3 1 -1 1.4756 62.9345 5 3 1 0 1.4468 64.3359 3 3 1 -2 1.4433 64.5107 4 0 2 0 1.4245 65.4677 3 0 2 1 1.3970 66.9237 1 2 0 -5 1.3860 67.5258 1 1 1 4 1.3778 67.9823 1 3 1 1 1.3667 68.6111 1 3 1 -3 1.3609 68.9446 1 |
3楼2015-04-28 11:07:23
mattlyzx
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4楼2015-04-28 14:36:32







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