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c20070626j捐助贵宾 (著名写手)
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[求助]
求XRD 卡片号 23-0333 和05-0561的图和数据 已有1人参与
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| 如题，求XRD 卡片号 23-0333 和05-0561的图和数据 |
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xhtangxh
木虫 (著名写手)
有木有虫
- CMEI: 6
- 应助: 773 (博后)
- 金币: 17832.4
- 红花: 107
- 帖子: 2676
- 在线: 599.3小时
- 虫号: 428580
- 注册: 2007-08-04
- 专业: 催化化学
【答案】应助回帖
★ ★ ★ ★ ★ ★ ★ ★ ★ ★
感谢参与，应助指数 +1
c20070626j: 金币+10, ★★★★★最佳答案 2015-05-13 20:13:02
感谢参与，应助指数 +1
c20070626j: 金币+10, ★★★★★最佳答案 2015-05-13 20:13:02
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Card Information Names: Lead Oxide Litharge, syn Formula: Pb O PDF Number: 000-05-0561 Quality: indexed Subfiles: inorganic mineral alloy COR CP EDU FOR NBS Cell and Symmetry Information System: tetragonal Space Group: P4/nmm (no. 129) a: 3.9729 c: 5.0217 Density (Dx): 9.354 Z: 2 Instrument Information Radiation: CuKa1 Wavelength: 1.5405 Filter: Ni Instrument(d): unknown Instrument(I): diffractometer I type: unknown Comments and Additional Information General: Crystal system refined in 1975. Source: Sample from National Lead Company. Analysis: Spectroscopic analysis: <0.01% Bi, Cu, Fe, Si; <0.001% Ca, Mg. Temperature: Pattern taken at 27 C. General: Polymorph: massicot (tetragonal). Optical: B=2.665, Q=2.535 Colour: Violet-red Pattern: Validated by calculated pattern. Pattern: See ICSD 62842 (PDF 01-085-1289); See ICSD 26596 (PDF 01-085-0711); See ICSD 62840 (PDF 01-085-1287); See ICSD 62841 (PDF 01-085-1288); See ICSD 62842 (PDF 01-085-1289); See ICSD 62843 (PDF 01-085-1290). Literature References General: Swanson, Fuyat. Natl. Bur. Stand. (U.S.), Circ. 539 II 30 (1953) Peak Data Wavelength 1.5406 used to convert d to 2theta PeakList h k l d 2theta I 0 0 1 5.0180 17.6600 5 1 0 1 3.1150 28.6333 100 1 1 0 2.8090 31.8309 62 0 0 2 2.5100 35.7431 18 1 0 2 2.1240 42.5267 1 2 0 0 1.9880 45.5937 8 1 1 2 1.8720 48.5950 37 2 1 1 1.6750 54.7573 24 2 0 2 1.5580 59.2608 6 1 0 3 1.5420 59.9382 11 1 1 3 1.4380 64.7775 2 2 2 0 1.4050 66.4930 5 3 0 1 1.2820 73.8605 2 3 1 0 1.2560 75.6541 3 2 2 2 1.2260 77.8477 4 3 1 1 1.2190 78.3801 5 1 0 4 1.1977 80.0516 1 1 1 4 1.1462 84.4478 2 3 1 2 1.1232 86.5956 2 3 2 1 1.0768 91.3424 3 2 0 4 1.0610 93.1033 2 3 0 3 1.0386 95.7447 1 2 1 4 1.0254 97.3888 1 1 0 5 0.9738 104.5589 1 4 1 1 0.9462 108.9925 1 3 3 0 0.9365 110.6736 3 3 2 3 0.9200 113.7040 3 |
2楼2015-04-14 10:35:03
xhtangxh
木虫 (著名写手)
有木有虫
- CMEI: 6
- 应助: 773 (博后)
- 金币: 17832.4
- 红花: 107
- 帖子: 2676
- 在线: 599.3小时
- 虫号: 428580
- 注册: 2007-08-04
- 专业: 催化化学
【答案】应助回帖
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Card Information Names: Lead Oxide Sulfate Formula: Pb5 O4 S O4 PDF Number: 000-23-0333 Quality: star Subfiles: inorganic COR CP EDU NBS Cell and Symmetry Information System: monoclinic Space Group: P21/a (no. 14) a: 11.532 b: 11.717 c: 7.307 b: 91.00 Density (Dx): 8.047 Z: 4 Instrument Information Radiation: CuKa1 Wavelength: 1.54056 Instrument(d): unknown Standard: Ag Instrument(I): diffractometer I type: unknown I/Icor: 4.90 Comments and Additional Information Colour: Yellowish white Preparation: The sample was prepared by heating a 4:1 molar ratio of PbO and Pb S O4 at 750 C for one hour, grinding and reheating at 750 C for 15 minutes. Temperature: Pattern taken at 25 C. Pattern: To replace 00-006-0308. Literature References General: Natl. Bur. Stand. (U.S.) Monogr. 25 10 27 (1972) Peak Data Wavelength 1.5406 used to convert d to 2theta PeakList h k l d 2theta I 1 1 0 8.2300 10.7408 10 0 0 1 7.3200 12.0808 4 0 1 1 6.2100 14.2505 4 0 2 0 5.8600 15.1064 1 2 0 0 5.7700 15.3435 3 -1 1 1 5.4800 16.1607 2 1 1 1 5.4300 16.3106 4 2 1 0 5.1750 17.1202 2 2 0 1 4.4910 19.7520 1 -1 2 1 4.2690 20.7903 4 1 3 0 3.7000 24.0319 1 0 1 2 3.4890 25.5090 1 0 3 1 3.4440 25.8480 1 1 1 2 3.3260 26.7818 2 1 3 1 3.2940 27.0469 6 -2 3 0 3.2320 27.5759 100 -2 0 2 3.1110 28.6709 45 2 0 2 3.0600 29.1593 45 -2 1 2 3.0060 29.6950 2 -2 3 1 2.9670 30.0945 1 2 3 1 2.9470 30.3036 1 0 4 0 2.9290 30.4944 1 4 0 0 2.8830 30.9931 30 1 4 0 2.8410 31.4630 1 -2 2 2 2.7460 32.5813 1 0 4 1 2.7190 32.9140 1 0 3 2 2.6680 33.5616 45 -1 3 2 2.6060 34.3846 3 -3 3 1 2.5760 34.7977 2 3 1 2 2.5630 34.9799 2 -2 4 1 2.4650 36.4183 1 2 4 1 2.4530 36.6028 2 -2 3 2 2.4330 36.9145 1 3 2 2 2.3970 37.4894 1 -1 1 3 2.3430 38.3868 1 -3 4 0 2.3290 38.6267 1 -4 3 0 2.3200 38.7825 1 1 5 0 2.2970 39.1866 1 0 4 2 2.2850 39.4009 1 5 1 0 2.2620 39.8184 1 -2 0 3 2.2580 39.8919 1 4 0 2 2.2450 40.1328 2 1 4 2 2.2380 40.2638 1 -2 1 3 2.2180 40.6428 2 3 4 1 2.2120 40.7579 2 4 1 2 2.2040 40.9125 2 1 5 1 2.1880 41.2252 1 5 1 1 2.1510 41.9675 1 5 2 0 2.1470 42.0494 1 -2 4 2 2.1320 42.3594 1 -4 2 2 2.1270 42.4638 1 2 4 2 2.1160 42.6954 1 -5 2 1 2.0680 43.7368 1 4 4 0 2.0540 44.0504 1 5 2 1 2.0490 44.1636 1 -1 3 3 2.0400 44.3687 1 3 1 3 2.0100 45.0670 1 -4 4 1 1.9840 45.6908 2 -4 3 2 1.9710 46.0094 18 0 6 0 1.9520 46.4834 14 4 3 2 1.9450 46.6606 20 -5 3 1 1.9230 47.2266 1 5 3 1 1.9090 47.5942 1 0 6 1 1.8860 48.2112 1 -2 5 2 1.8720 48.5950 2 -1 6 1 1.8630 48.8450 3 2 6 0 1.8490 49.2393 1 5 2 2 1.8380 49.5538 1 0 0 4 1.8267 49.8812 10 3 3 3 1.8088 50.4091 1 -2 6 1 1.7955 50.8090 1 -2 4 3 1.7892 51.0007 2 -5 4 1 1.7644 51.7702 1 4 5 1 1.7603 51.8997 1 3 5 2 1.7478 52.2989 1 -6 3 0 1.7239 53.0802 11 2 1 4 1.7137 53.4211 5 0 5 3 1.6886 54.2798 6 6 1 2 1.6710 54.8994 1 4 3 3 1.6676 55.0208 1 -2 6 2 1.6537 55.5230 8 2 6 2 1.6464 55.7906 9 0 7 1 1.6316 56.3415 1 2 5 3 1.6158 56.9425 6 6 4 0 1.6068 57.2908 1 5 2 3 1.5971 57.6713 8 2 3 4 1.5836 58.2099 8 -2 7 1 1.5720 58.6812 1 -4 0 4 1.5552 59.3782 2 4 0 4 1.5304 60.4397 3 |
3楼2015-04-14 10:35:55