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[求助] 求标准PDF卡图已有1人参与

PDF 图号 01-089-7618，求发图和数据

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1楼 2015-04-13 17:17:47

已阅回复此楼关注TA 给TA发消息送TA红花 TA的回帖

xhtangxh

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【答案】应助回帖

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感谢参与，应助指数 +1
c20070626j: 金币+10, ★★★很有帮助 2015-04-18 09:55:09

图自己作吧。

Card Information
Names: Lead Oxide Sulfate
Pentalead tetraoxide sulfate(VI)
Formula: ( Pb O )4 ( Pb ( S O4 ) )
PDF Number: 000-89-7618
Quality: calculated
Subfiles: inorganic COR FIZ

Cell and Symmetry Information
System: monoclinic Space Group: P21/c (no.  14)
a: 7.297 b: 11.698 c: 11.498
b: 90.93
Density (Dx): 8.093 Z: 4

Instrument Information
Radiation: CuKa1 Wavelength: 1.54060
Instrument(d): calculated Cut Off: 17.7
Instrument(I): calculated I type: peak heights
I/Icor: 9.15

Comments and Additional Information
ICSD Number: 087927
Temperature factor: ATF
TT At least one TF implausible.
TI Crystal structure of tetrabasic lead sulfate (4(Pb O) . (Pb S O4))
WY e14 (P121/C1)
AF AB5X8

Literature References
General:    Calculated from ICSD using POWD-12++          ( )
Structure: Steele, I.M., Pluth, J.J. J. Electrochem. Soc.  145 528 (1998)

Peak Data
Wavelength 1.5406 used to convert d to 2theta

PeakList
   h    k    l       d    2theta    I
   0    1    1    8.1996    10.7808 189
   1    0    0    7.2960    12.1206    59
   1    1    0    6.1906    14.2953    51
   0    2    0    5.8490    15.1350    8
   0    0    2    5.7482    15.4019    38
   1    1    1    5.4196    16.3422    55
   0    1    2    5.1590    17.1735    21
   1    2    0    4.5513    19.4877    4
-1    0    2    4.5513    19.4877    4
   1    0    2    4.4800    19.8008    10
-1    2    1    4.2565    20.8522    31
-1    1    2    4.2565    20.8522    31
   1    1    2    4.1837    21.2190    1
   0    2    2    4.0998    21.6586    2
   0    3    1    3.6927    24.0800    3
   2    0    0    3.6480    24.3795    1
   0    1    3    3.6480    24.3795    1
-1    2    2    3.5920    24.7660    4
   1    2    2    3.5566    25.0161    4
   2    1    0    3.4826    25.5566    9
   1    3    0    3.4390    25.8862    11
-2    1    1    3.3475    26.6070    3
   2    1    1    3.3188    26.8411    13
   1    3    1    3.2878    27.0985    42
-1    1    3    3.2787    27.1759    47
   0    3    2    3.2269    27.6201 999
-2    0    2    3.1030    28.7466 449
   2    2    0    3.1030    28.7466 449
   2    0    2    3.0577    29.1813 448
-2    2    1    2.9993    29.7632    24
-2    1    2    2.9993    29.7632    24
   2    2    1    2.9786    29.9746    8
-1    3    2    2.9612    30.1552    21
   2    1    2    2.9612    30.1552    21
   1    3    2    2.9413    30.3641    16
   0    4    0    2.9201    30.5892    18
   1    2    3    2.9201    30.5892    18
   0    0    4    2.8741    31.0912 336
   0    4    1    2.8342    31.5400    8
   0    1    4    2.7911    32.0404    3
-2    2    2    2.7411    32.6409    2
   0    3    3    2.7332    32.7383    2
   1    4    0    2.7146    32.9695    7
   2    2    2    2.7098    33.0291    6
-1    0    4    2.6890    33.2913    12
   2    3    0    2.6640    33.6140 525
   1    0    4    2.6640    33.6140 525
-1    1    4    2.6207    34.1859    5
-2    1    3    2.5974    34.5017    29
   1    1    4    2.5974    34.5017    29
   2    3    1    2.5885    34.6249    20
-1    3    3    2.5693    34.8916    23
   2    1    3    2.5577    35.0553    18
   1    3    3    2.5498    35.1667    10
-1    4    2    2.4604    36.4896    10
   1    4    2    2.4489    36.6661    13
-1    2    4    2.4432    36.7547    7
   3    0    0    2.4320    36.9300    3
-2    2    3    2.4243    37.0514    4
   1    2    4    2.4243    37.0514    4
   2    3    2    2.4062    37.3414    1
   2    2    3    2.3919    37.5723    4
   3    1    0    2.3811    37.7491    2
-3    1    1    2.3390    38.4549    8
   0    4    3    2.3249    38.6984    10
   3    1    1    2.3249    38.6984    10
   0    3    4    2.3136    38.8946    14
   0    5    1    2.2926    39.2648    9
-2    0    4    2.2757    39.5696    9
   0    1    5    2.2561    39.9264    10
-3    0    2    2.2561    39.9264    10
   3    2    0    2.2456    40.1211    7
-2    4    1    2.2400    40.2259    13
   2    0    4    2.2400    40.2259    13
   2    4    1    2.2338    40.3433    12
-2    1    4    2.2338    40.3433    12
   1    5    0    2.2269    40.4740    8
   3    0    2    2.2269    40.4740    8
-1    4    3    2.2215    40.5769    5
-1    3    4    2.2137    40.7254    12
-3    1    2    2.2137    40.7254    12
-3    2    1    2.2088    40.8190    17
   1    4    3    2.2088    40.8190    17
   3    2    1    2.1971    41.0469    16
   1    3    4    2.1971    41.0469    16
   3    1    2    2.1876    41.2335    10
   1    5    1    2.1876    41.2335    10
   0    5    2    2.1652    41.6798    2
-1    1    5    2.1652    41.6798    2
   1    1    5    2.1458    42.0738    6
   0    2    5    2.1399    42.1958    4
-2    4    2    2.1282    42.4381    10
-2    2    4    2.1208    42.5942    7
   2    4    2    2.1135    42.7490    9
   2    2    4    2.0919    43.2127    1
   3    2    2    2.0811    43.4468    1
-1    5    2    2.0811    43.4468    1
   1    5    2    2.0738    43.6073    1
   3    3    0    2.0635    43.8360    9
-1    2    5    2.0635    43.8360    9
   0    4    4    2.0499    44.1434    9
   1    2    5    2.0451    44.2529    5
-3    1    3    2.0360    44.4613    7
-3    3    1    2.0360    44.4613    7
   3    1    3    2.0082    45.1089    6
   0    5    3    1.9969    45.3798    1
   0    3    5    1.9794    45.8018    9
-1    4    4    1.9794    45.8018    9
   1    4    4    1.9654    46.1473 198
-2    3    4    1.9654    46.1473 198
-3    2    3    1.9497    46.5422 108
   0    6    0    1.9497    46.5422 108
-2    5    1    1.9423    46.7283 217
   2    3    4    1.9423    46.7283 217
   2    5    1    1.9383    46.8317 115
   3    2    3    1.9249    47.1764    6
-1    3    5    1.9161    47.4076    8
   0    0    6    1.9161    47.4076    8
   2    1    5    1.9047    47.7081    8
   1    3    5    1.9047    47.7081    8
   0    1    6    1.8909    48.0789    1
   1    6    0    1.8836    48.2771    6
   3    4    0    1.8699    48.6525    7
-2    5    2    1.8699    48.6525    7
-1    6    1    1.8600    48.9278    28
-2    2    5    1.8600    48.9278    28
   0    6    2    1.8463    49.3147    5
   1    0    6    1.8463    49.3147    5
   3    4    1    1.8420    49.4384    5
   3    0    4    1.8420    49.4384    5
-1    1    6    1.8376    49.5662    4
   2    2    5    1.8337    49.6773    9
   4    0    0    1.8240    49.9598    86
   1    1    6    1.8240    49.9598    86
   0    2    6    1.8209    50.0519    48
   3    1    4    1.8209    50.0519    48
   0    4    5    1.8065    50.4772    7
   3    3    3    1.8065    50.4772    7
   4    1    0    1.8022    50.6058    5
-2    4    4    1.7960    50.7944    3
-1    6    2    1.7922    50.9107    5
   1    6    2    1.7877    51.0462    11
-4    1    1    1.7849    51.1333    13
-3    2    4    1.7849    51.1333    13
   2    4    4    1.7783    51.3356    7
   4    1    1    1.7761    51.4029    4
   3    4    2    1.7717    51.5412    2
-1    5    4    1.7651    51.7497    1
-1    4    5    1.7579    51.9762    6
-2    5    3    1.7579    51.9762    6
-4    0    2    1.7454    52.3759    5
   2    5    3    1.7454    52.3759    5
   4    2    0    1.7413    52.5090    3
   0    6    3    1.7377    52.6261    2
   0    3    6    1.7197    53.2207 111
   4    2    1    1.7197    53.2207 111
-2    0    6    1.7078    53.6211    54
-2    6    1    1.7025    53.8011    29
-3    3    4    1.6851    54.4015    61
   2    0    6    1.6851    54.4015    61
-1    3    6    1.6793    54.6061    32
-4    2    2    1.6737    54.8023    5
   2    1    6    1.6673    55.0315    7
-3    1    5    1.6673    55.0315    7
   3    5    1    1.6654    55.0989    6
   3    3    4    1.6654    55.0989    6
   4    3    0    1.6509    55.6271    91
-2    6    2    1.6509    55.6271    91
   2    6    2    1.6439    55.8821    97
   0    5    5    1.6399    56.0308    53
-4    3    1    1.6399    56.0308    53
-2    4    5    1.6279    56.4807    9
   0    1    7    1.6279    56.4807    9
-3    5    2    1.6228    56.6727    6
   4    1    3    1.6209    56.7470    4
   0    6    4    1.6135    57.0322    72
   2    4    5    1.6135    57.0322    72
   0    7    2    1.6047    57.3728    9
   0    4    6    1.6047    57.3728    9
-4    3    2    1.5941    57.7889    89
-1    1    7    1.5941    57.7889    89
   4    3    2    1.5817    58.2853    89
   0    2    7    1.5817    58.2853    89
-1    6    4    1.5784    58.4185    52
   4    2    3    1.5784    58.4185    52
   1    6    4    1.5724    58.6652    9
-1    4    6    1.5687    58.8151    7
-1    7    2    1.5687    58.8151    7
   2    6    3    1.5643    58.9976    13
-2    3    6    1.5643    58.9976    13
   1    4    6    1.5610    59.1372    10
   3    4    4    1.5585    59.2390    7
-4    0    4    1.5515    59.5345    32
-3    5    3    1.5515    59.5345    32
   2    3    6    1.5468    59.7316    24
-3    3    5    1.5468    59.7316    24
   1    2    7    1.5403    60.0090    3
-4    1    4    1.5380    60.1093    3
   3    5    3    1.5380    60.1093    3

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