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谷云飞木虫 (小有名气)
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[求助]
微谱求助，万分感谢 已有2人参与
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化合物 3：13C NMR (151 MHz, MeOD) δ 213.31, 152.77, 140.14, 134.68, 127.74, 127.32, 116.99, 79.28, 54.82, 51.58, 46.34, 40.39, 31.92, 29.39, 27.96, 25.88, 23.24, 23.18, 20.27, 17.08 十分谢谢！ |
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金虫 (正式写手)
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【答案】应助回帖
★ ★
感谢参与，应助指数 +1
谷云飞: 金币+2, ★有帮助, 谢谢提醒，不过您查询的并非我给出的全部数据！ 2015-04-05 11:10:24
感谢参与，应助指数 +1
谷云飞: 金币+2, ★有帮助, 谢谢提醒，不过您查询的并非我给出的全部数据！ 2015-04-05 11:10:24
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????????????? ??????????? ????С??????????????????????????(,)??????磺 21.4,30.4,37.4,73.2,73.7,125.6,126.6,139.6,140.2,168.2 ?????? ?????? (???????????????趨) ?????? %(?????>=50%) ???????????鵽528????????(???????????ο?) 1 . 6??-Acetoxy-7??-hydroxyeudesm-4(15)-ene C17H28O3 ?????:82.3% Journal of Asian Natural Products Research 2006 8 723-731 Eudesmane-type sesquiterpenoids from the liverwort Lepidozia fauriana H.-S. SHY and C.-L. WU Structure 13C NMR ??????? 2 . eudesm-4(15)-en-6??-acetoxy-7??-ol ?????:82.3% Journal of the Chinese Chemical Society 1999 46 191-195 Isocalamenenes from the Liverwort Bazzania tridens ?????(Ran-Chien Chang);?????(Chia-Li Wu) Structure 13C NMR ??????? 3 . 10??-hydroxy-8??-methoxyeremophilenolide C16H24O4 ?????:66.6% Chemical & Pharmaceutical Bulletin 1997 45 1875-1876 Absolute Structure of Eremophilenolide from Soligago dahurica Keisuke KOJIMA,Keiichiro HATANO,Purev ONDOGNIJ,Binderya MUNAAGIN and Yukio OGIHARA Structure 13C NMR ??????? 4 . 4,10-epi-5??-hydroxydihydroeudesmol C15H28O2 ?????:66.6% Chemical & Pharmaceutical Bulletin 1987 35 1460-1463 Novel Eudesmane-Type Sesquiterpenes from Alpinia japonica (THUNB.) MIQ HIDEJI ITOKAWA,HIROSHI MORITA and KINZO WATANABE Structure 13C NMR ??????? 5 . (-)-10??-hydroxy-4-muurolen-3-one B C15H24O2 ?????:66.6% Chinese Chemical Letters 2008 19 1265-1267 First total synthesis of 10??-hydroxy-4-muurolen-3-one and its C10-isomer Fu Qiang Bi, Li Jing Fang, Chen Xi Zhang, Yu Lin Li Structure 13C NMR ??????? 6 . 5??-Hydroxy-??-eudesmol C15H26O2 ?????:66.6% Molecules 2003 8 670-677 Sesquiterpenes from Cymbopogon proximus Hesham I. El-Askary, Meselhy R. Meselhy and Ahmed M. Galal Structure 13C NMR ??????? 7 . 1??,10??,11-trihydroxy-4??,5??,7??-eremophilane C15H28O3 ?????:66.6% Phytochemistry 1999 52 1063-1067 The hydroxylation of the sesquiterpenoid valerianol by Mucor plumbeus Simone Fontes Arantes, James R. Hanson, Peter B. Hitchcock Structure 13C NMR ??????? 8 . (-)-premnaspirodiene ?????:66.6% Phytochemistry 1999 51 987-990 (-)-Spirolepechinene, a spirosesquiterpene from Lepechinia bullata (Lamiaceae) Maren D. Eggers, Volker Sinnwell, Elisabeth Stahl-Biskup Structure 13C NMR ??????? 9 . compound 14 C15H26O ?????:66.6% Phytochemistry 1997 46 1203-1208 Terpenoids from the Japanese liverworts Jackiella javanica and Jungermannia infusca Fumihiro Nagashima, Akiko Tamada, Noriko Fujii, Yoshinori Asakawa Structure 13C NMR ??????? 10 . 3??-hydroperoxyeudesm-4(14)-ene-6??,7??-diol C15H26O4 ?????:66.6% Helvetica Chimica Acta 2007 90 52−57 Rearranged Calamenene and Eudesmane Sesquiterpenoids from two Chinese Liverworts Bin Ma, Zhi-Qiang Lu, Huai-Fang Guo, and Hong-Xiang Lou Structure 13C NMR ??????? 11 . eudesmandiol diastereomer ?????:66.6% Phytochemistry 1989 28 936-938 A eudesmanediol from Cymbopogon distans C.S. Mathela,A.B. Melkani,Alka Pant,Vasu Dev,Thomas E. Nelson,Hakon Hope,Albert T. Bottini Structure 13C NMR ??????? |
2楼2015-04-04 12:29:21
seuseasoar
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【答案】应助回帖
★ ★ ★ ★ ★ ★ ★ ★
感谢参与，应助指数 +1
谷云飞: 金币+8, ★★★★★最佳答案, 非常感谢 2015-04-05 11:10:41
感谢参与，应助指数 +1
谷云飞: 金币+8, ★★★★★最佳答案, 非常感谢 2015-04-05 11:10:41
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1 . 3β,12-dihydroxyabieta-8,11,13-triene-1-one(hinokiol-1-one) C20H28O3 相似度:70% Phytochemistry 1992 31 2789-2792 3β,12-dihydroxyabieta-8,11,13-triene-1-one and other constituents from Juniperus excelsa leaves Jaber S. Mossa, Ilias Muhammad, Farouk S. El-Feraly, Charles D. Hufford Structure 13C NMR Structure & 13C NMR 碳谱模拟图 2 . hinokiol 相似度:70% Natural Product Research and Development 2009 21 737-739 Chemical Constitutes in the Fruit of Torreya nucifera CAO Cong-mei; DONG Mei; WANG Wei; YANG Yan; WU Ming; GU Yu-cheng;SHI Qing-wen Structure 13C NMR Structure & 13C NMR 碳谱模拟图 3 . compound 64 相似度:70% Magnetic Resonance in Chemistry 1994 32 774-781 13C NMR Data for abieta-8,11,13-triene diterpenoids J. M. Miguel Del Corral, M. Gordaliza, M. A. Salinero and A. San Feliciano Structure 13C NMR Structure & 13C NMR 碳谱模拟图 4 . 3β-hydroxysempervirol C20H30O2 相似度:65% Food Chemistry 2013 136 1110-1116 Abietane diterpenoids from Isodon lophanthoides var. graciliflorus and their cytotoxicity Wenting Zhou, Haihui Xie, Ping Wu, Xiaoyi Wei Structure 13C NMR Structure & 13C NMR 碳谱模拟图 5 . Brussonol C20H28O3 相似度:60% Organic Letters 2007 Vol. 9, No. 14 2705-2708 Reconciling Icetexane Biosynthetic Connections with Their Chemical Synthesis: Total Synthesis of (±)-5,6-Dihydro-6r-hydroxysalviasperanol,(±)-Brussonol, and (±)-Abrotanone Eric M. Simmons, Jennifer R. Yen, and Richmond Sarpong Structure 13C NMR Structure & 13C NMR 碳谱模拟图 6 . N-n-Heptyl-9-amino-1,2,3,4-tetrahydroacridine hydro-chloride C20H28N2 相似度:60% Bioorganic & Medicinal Chemistry 1999 7 2569-2575 Dual-site binding of bivalent 4-aminopyridine- and 4-aminoquinoline-based AChE inhibitors: contribution of the hydrophobic alkylene tether to monomer and dimer affinities Yi Fan Han, Crystal P.-L Li, Ella Chow, Hong Wang, Yuan-Ping Pang, Paul R Carlier Structure 13C NMR Structure & 13C NMR 碳谱模拟图 7 . (-)-brussonol 相似度:60% Tetrahedron Letters 2013 54 1356-1359 Obtusinones D and E, linear and angular fused dimeric icetexane diterpenoids from Premna obtusifolia roots Abdul-wahab Salae, Nawong Boonnak Structure 13C NMR Structure & 13C NMR 碳谱模拟图 8 . Brussonol C20H28O3 相似度:60% Journal of Agricultural and Food Chemistry 2005 53 5200-5206 Diterpenes from Salvia broussonetii Transformed Roots and Their Insecticidal Activity Braulio M. Fraga, Carmen E. Díaz, Ana Guadaño, and Azucena González-Coloma Structure 13C NMR Structure & 13C NMR 碳谱模拟图 9 . Hexylene-linked bis-THA bis-hydrochloride C32H38N4 相似度:60% Bioorganic & Medicinal Chemistry 1999 7 351-357 Evaluation of short-tether Bis-THA AChE inhibitors. A further test of the dual binding site hypothesis Paul R. Carlier, Yi Fan Han, Ella S.-H. Chow, Crystal P.-L. Li, Hong Wang, Thuy Xuan Lieu, Hau Sum Wong, Yuan-Ping Pang Structure 13C NMR Structure & 13C NMR 碳谱模拟图 |
3楼2015-04-04 12:30:39
