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傅里叶

新虫 (小有名气)

[求助] 微谱数据查询 已有1人参与

DL-1
溶剂:甲醇
C谱数据如下:16.07,16.11,17.77,21.08,22.39,22.77,23.71,25.91,26.98,27.74,27.8,28.81,37.05,39.85,40.86,40.89,62.69,68.35,72.73,74.35,75.26,78.5,79.19,88.79,102.44,125.41,125.45,125.61,126.19,132.09,132.14,135.7,136.15,172.8
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seuseasoar

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傅里叶: 金币+10, ★★★很有帮助 2015-03-13 17:15:02
.     lyciumoside I
C32H54O12     ?????:67.6%
Chemical & Pharmaceutical Bulletin          1993          41          703-709
Cyclic Peptides, Acyclic Diterpene Glycosides and Other Compounds from Lycium chinense MILL
Shoji YAHARA,Choko SHIGEYAMA,Takeshi URA,Kaori WAKAMATSU,Tadashi YASUHARA and Toshihiro NOHARA
Structure      13C NMR    Structure & 13C NMR     ???????
2 .     saponin K7C
C42H72O13     ?????:66.6%
Chemical & Pharmaceutical Bulletin          1985          33          1400-1406
Studies on the Constituents of Hedera rhombea BEAN. II. On the Dammarane Triterpene Glycosides. (1)
HARUHISA KIZU,MICHIYO KOSHIJIMA,MASATOMI HAYASHI and TSUYOSHI TOMIMORI
Structure      13C NMR    Structure & 13C NMR     ???????
3 .     2'',3'',4'',6'-de-O-acetylcupacinoside
C32H54O10     ?????:64.7%
Natural Product Communications          2013          8          1201-1203
A New Bioactive Diterpene Glycoside from Molinaea retusa from the Madagascar Dry Forest
Alexander L. Eaton, Liva Harinantenaina, Peggy J. Brodie, Maria B. Cassera, Jessica D. Bowman, Martin W. Callmander, Richard Randrianaivo, Roland Rakotondrajaona, Etienne Rakotobe, Vincent E. Rasamison and David G. I. Kingston
Structure      13C NMR    Structure & 13C NMR     ???????
4 .     sapelenin A
C32H58O7     ?????:61.7%
Phytochemistry          1993          34          1603-1607
Sapelenins A, B and C, acyclic triterpenoids from the stem bark of Entandrophragma cylindricum
David Ngnokam, Georges Massiot, Jean-Marc Nuzillard, Joseph D. Connolly, Etienne Tsamo, Christophe Morin
Structure      13C NMR    Structure & 13C NMR     ???????
5 .     (8R)-3??,8-Dihydroxypolypoda-13E,17E,21-triene
C30H52O2     ?????:61.7%
Journal of Natural Products          2011          74          1731-1736
(8R)-3??, 8-Dihydroxypolypoda-13E, 17E, 21-triene Induces Cell Cycle Arrest and Apoptosis in Treatment-Resistant Prostate Cancer Cells
Samy A. F. Morad, Claudia Schmidt, Berthold B?uchele, Bernd Schneider, Michael Wenzler, Tatiana Syrovets, and Thomas Simmet
Structure      13C NMR    Structure & 13C NMR     ???????
6 .     compound 3
    ?????:61.7%
Phytochemistry          1988          27          2209-2211
Trifolioside II,an acyclic sesquiterpene oligoglycoside from pericarps of Sapindus trifoliatus
Ryoji Kasai,Masatoshi Nishi,Kenji Mizutani,Izumi Miyahara,Toshie Moriya,Kazumoto Miyahara,Osamu Tanaka
Structure      13C NMR    Structure & 13C NMR     ???????
7 .     Quassiol A
C30H54O5     ?????:61.7%
Tetrahedron Letters          1993          34          1705-1708
Quassiol A, a novel squalene triterpene from quassia multiflora
Winston F. Tinto, Stewart McLean, William F. Reynolds, Charles A.G. Carter
Structure      13C NMR    Structure & 13C NMR     ???????
8 .     compound 55
C36H51N1O6     ?????:61.7%
Journal of the American Chemical Society          2010          132          5300-5308
Biomimetic Syntheses from Squalene-Like Precursors: Synthesis of ent-Abudinol B and Reassessment of the Structure of Muzitone
Matthew A. Boone, Rongbiao Tong, Frank E. McDonald, Sheri Lense, Rui Cao and Kenneth I. Hardcastle
Structure      13C NMR    Structure & 13C NMR     ???????
9 .     prosapogenin G'
C36H56O8     ?????:61.1%
Journal of the Chemical Society, Perkin Transactions 1          1981                   1923-1927
Three new saponins from the leaves of Hovenia dulcis(Rhamnaceae)
Yasuko Kimura, Yoshimasa Kobayashi, Tadahiro Takeda and Yukio Ogihara
Structure      13C NMR    Structure & 13C NMR     ???????
10 .     Actinostemmoside C
    ?????:60%
Journal of the Korean Society for Applied Biological Chemistry          2010          53          746-751
Antioxidative Constituents from the Whole Plant of Actinostemma lobatum Maxim
Dae Keun Kim*
Structure      13C NMR    Structure & 13C NMR     ???????
11 .     crenulatoside B
C29H48O11     ?????:58.8%
Phytochemistry          2005          66          2714-2718
Acylated farnesyl diglycosides from Guioa crenulata
Abdulmagid Alabdul Magid, Laurence Voutquenne-Nazabadioko,Marc Litaudon, Catherine Lavaud
Structure      13C NMR    Structure & 13C NMR     ???????
12 .     concentricol D
C32H54O6     ?????:58.8%
Phytochemistry          2002          61          345-353
Concentriols B, C and D, three squalene-type triterpenoids from the ascomycete Daldinia concentrica
Dang Ngoc Quang, Toshihiro Hashimoto, Masami Tanaka,Manuela Baumgartner, Marc Stadler, Yoshinori Asakawa
Structure      13C NMR    Structure & 13C NMR     ???????
13 .     sapelenin C
    ?????:58.8%
Natural Product Research          1995          5          289-293
Sapelenin D, a New Acyclic Triterpenoid from the Stem Bark of Entandrophragma cylindricum
David Ngnokam; Georges Massiot; Christophe Bliard; Etienne Tsamo
Structure      13C NMR    Structure & 13C NMR     ???????
14 .     gymnopilin A9
    ?????:58.8%
Journal of Natural Products          1991          Vol 54          184
Minor Constituents of Gymnopilus spectabilis
John A. Findlay, Zheng-quan He
Structure      13C NMR    Structure & 13C NMR     ???????
15 .     (3S*,8R*,13R*,-14R*,15S*,17R*,18R*,21R*) 15-O-acetyl-8,13;14,18-diepoxy-17,18-diepi-13,18-seco-onocerane-3,15,21-triol
    ?????:58.8%
Organic Letters          2011          Vol.13,No.6          1354-1357
Phyteumosides A and B: New Saponins with Unique Triterpenoid Aglycons from Phyteuma orbiculare L.
Christian Abbet, Markus Neuburger, Trixie Wagner, Melanie Quitschau,Matthias Hamburger, and Olivier Potterat
Structure      13C NMR    Structure & 13C NMR     ???????
16 .     (9R,10S)-polypoda-8(26),13E,17E,21-tetraen-3??-ol
    ?????:58.8%
Organic Letters          2008          Vol.10,No.21          4959-4962
Importance of Saccharomyces cerevisiae Oxidosqualene-Lanosterol Cyclase Tyrosine 707 Residue for Chair-Boat Bicyclic Ring Formation and Deprotonation Reactions
Tung-Kung Wu, Tsai-Ting Wang, Cheng-Hsiang Chang, Yuan-Ting Liu, and Wen-Shiang Shie
Structure      13C NMR    Structure & 13C NMR     ???????
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