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xiaocong金虫 (著名写手)
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求助关于化学吸附仪
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有没有人用过麦克和康塔的化学吸附仪,动态的,有什么区别吗,另外想问下化学吸附仪后面如果接质谱的话,质谱的峰能否定量,色谱的峰出来进质谱延迟时间长吗 [ Last edited by xiaocong on 2008-6-18 at 08:37 ] |
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xiaocong
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4楼2008-06-19 08:21:31
2楼2008-06-18 09:05:27
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根据麦克公司的官方资料，质谱也是可以定量的。 Application Note 122 AutoChem and Mass Spectrometer Gas Calibration The AutoChem TCD level calibration is a powerful tool for converting raw TCD signals to gas concentrations. This built-in calibration provides the AutoChem with known gas concentrations and records the TCD signal associated with each one. The concentration and signal data are then used to generate a polynomial for converting TCD signals to gas concentrations. This capability can also be used to generate a gas calibration for a mass spectrometer. A concentration calibration for hydrogen was generated to demonstrate this technique. During the AutoChem TCD level calibration, a Pfeiffer ThermoStar (QMS 200) was used to monitor the hydrogen concentration in the gas stream. Typical calibration data are shown in Figure 1. The AutoChem was configured with argon as the carrier gas and 10% hydrogen in argon as the loop gas. The built-in TCD level calibration automatically generated 11 gas concentrations using an internal blender. The AutoChem and the Pfeiffer ThermoStar recorded similar signal profiles for the level calibration. The Pfeiffer ThermoStar data can be exported to an ASCII file, and used to generate a calibration curve. Several commercial software packages (Microsoft Excel, Microcal Origin, and Matlab from Mathworks) are suitable for generating the final calibration curve, Figure 2. The calculated polynomial for the hydrogen gas concentration can be used to convert ThermoStar Ion Current (mass = 2) to hydrogen concentrations. Most commercial mass spectrometers can be used with the AutoChem to generate calibration curves for the mass spectrometer. PDF版本 麦克官方网站下载Application Note 122 http://www.micromeritics.com/applications/application_notes.aspx 到质谱时间应该有所延长，看温度的话，只看TCD信号我想就可以了吧。 |
3楼2008-06-18 10:36:12