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| Differential scanning calorimetry (DSC) was performed using a Perkine-Elmer DSC 7 in a nitrogen atmosphere at a heating rate of 10 C/min. Thermal gravimetric analysis (TGA) was performed with a PerkineElmer Pyris1 at a heating rate of 20 C/min in a nitrogen or air atmosphere. Dynamic mechanical analysis (DMA) was performed with a PerkineElmer Pyris Diamond DMA with a sample size of 2.0 1.0 0.2 cm. The storage modulus E' and tan d were determined as the sample was subjected to the temperature scan mode at a programmed heating rate of 5 C/min at a frequency of 1 Hz. The test was performed using a bending mode with an amplitude of 5 mm. Thermal mechanical analysis (TMA) was performed with a PerkineElmer Pyris Diamond TMA at a heating rate of 5 C/min. NMR measurements were performed using a Varian Inova 600 NMR in DMSO-d6, and the chemical shift was calibrated by setting the chemical shift of DMSO-d6 as 2.49 ppm. The infrared spectra were recorded using a Nicolet Avatar 320 FTIR spectrophotometer. |
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武汉一心一译 
捐助贵宾 (著名写手)
- 翻译EPI: 502
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朱岩0308: 金币+28, 翻译EPI+1, ★★★★★最佳答案, 多谢 2015-03-05 14:58:15
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Differential scanning calorimetry (DSC) was performed using a Perkine-Elmer DSC 7 in a nitrogen atmosphere at a heating rate of 10 C/min. Thermal gravimetric analysis (TGA) was performed with a PerkineElmer Pyris1 at a heating rate of 20 C/min in a nitrogen or air atmosphere. 在氮气环境中，以每分钟上升10摄氏度的加热效率，运用铂金埃尔默公司研制的 DSC7号仪器，进行差示扫描量热。同时，在氮氧环境中，以每分钟上升20摄氏度的加热效率，运用铂金埃尔默公司的Pyris1号仪器，进行热重分析。 Dynamic mechanical analysis (DMA) was performed with a PerkineElmer Pyris Diamond DMA with a sample size of 2.0 1.0 0.2 cm. 运用铂金埃尔默公司研制Pyris Diamond号分析仪对大小为2.0cm*1.0cm*0.2cm的样本，进行动态力学分析。 The storage modulus E' and tan d were determined as the sample was subjected to the temperature scan mode at a programmed heating rate of 5 C/min at a frequency of 1 Hz. 温度扫描模型被调试为每分钟升温5摄氏度，1Hz的频率，测量储能模量E 和介质损耗因数作为样品参数。 The test was performed using a bending mode with an amplitude of 5 mm. 该项测试是在振幅为5mm的弯曲模态上进行的。 Thermal mechanical analysis (TMA) was performed with a PerkineElmer Pyris Diamond TMA at a heating rate of 5 C/min. 以每分钟上升5摄氏度的加热效率，运用铂金埃尔默公司研制的 Pyris Diamond仪器，进行热机分析。 NMR measurements were performed using a Varian Inova 600 NMR in DMSO-d6, and the chemical shift was calibrated by setting the chemical shift of DMSO-d6 as 2.49 ppm. 运用600HZ高磁场核磁共振仪，以氘代二甲亚砜作试剂，进行核磁共振测量。 通过将氘代二甲亚砜的化学位移设定在2.49ppm，从而校准化学位移。 The infrared spectra were recorded using a Nicolet Avatar 320 FTIR spectrophotometer. 运用Nicolet Avatar 320傅里叶红外光谱仪，记录本实验的红外光谱。 |
2楼2015-03-05 10:07:37
