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milobb

新虫 (小有名气)

[求助] 水热法制备的的纳米微粒表面是裸露的吗? 已有3人参与

1.如题,通过水热法制备的纳米微粒(如CdS,ZnO等)表面是否存在稳定剂或包覆剂?或者是否存在官能团?还是裸露的呢?如果是裸露的,那如何保证其在溶剂中的稳定性呢?
2. 水热法制备纳米微粒有什么优势和缺点?

附文献中水热法制备CdS纳米线的过程:
cadmium nitrate (1.9 g) and thiourea (1.42 g) were added into a tefl  on
stainless steel autoclave that had been fi lled with ethylenediamine to
60% of its capacity (50 mL). The autoclave was maintained at 180 °C for
48 h and allowed to cool down to room temperature. A yellow precipitate
(CdS nanowires) was fi ltered and washed several times with absolute
ethanol and deionized water to remove the residue of organic solvent.
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权哥哥景

金虫 (著名写手)

有用

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9楼2015-02-18 08:20:56
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