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huadong1227木虫 (小有名气)
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[求助]
HD-25 微谱数据求助 已有1人参与
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MeOD溶，13C-NMR 数据如下： 16.16,16.20,16.63,18.51,20.34,28.06,29.37,29.90,30.75,31.13,31.45,31.85,31.89,36.61,37.20,38.14,44.15,44.43,50.06,52.53,61.37, 66.33,68.34,70.42,70.81,71.00,72.54,76.30,77.64,77.81,77.96,89.19,89.89,99.14,100.76,109.56,121.22,104.50 |
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jiangtao2956
木虫 (正式写手)
GT
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【答案】应助回帖
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huadong1227: 金币+6, ★有帮助 2014-12-29 21:46:11
感谢参与，应助指数 +1
huadong1227: 金币+6, ★有帮助 2014-12-29 21:46:11
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查询结果：共查到1267个化合物(查询结果仅供参考) 1 . pennogenin-3-O-α-L-rhamnopyranosyl-(1→2)]β-D-glucopyranoside 相似度:92.3% Chinese Joumal of Experimental Traditional Medical Fomulae 2014 20 99-102 Studies on Chemical Constituents of Trillium tschonoskii JIA Lan-ting, YANG Shang-jun, BAI Shao-yan Structure 13C NMR 碳谱模拟图 2 . compound 13 C39H62O13 相似度:79.4% Steroids 2013 78 670-682 Steroidal glycosides from the bulbs of Fritillaria meleagris and their cytotoxic activities Yukiko Matsuo, Daisuke Shinoda, Aina Nakamaru, Yoshihiro Mimaki Structure 13C NMR 碳谱模拟图 3 . pennogenin3-O-[β-D-xylopyranosyl-(1→5)-α-L-arabinofuranosyl-(1→4)]-[α-L-rhamnopyranosyl-(1→2)]-β-D-glucopyranoside 相似度:78.9% West China Journal of Pharmaceutical Sciences 2010 25 508-511 Isolation and identification of steroidal saponins of Paris polyphylla Smith var. pseudothibetica LIU Xian-bo, ZHANG Hao, YONG Zheng-ping, XUE Dan Structure 13C NMR 碳谱模拟图 4 . 3-O-α-L-rhamnopyranosyl-(1→2)-O-β-D-glucopyranoside 相似度:76.9% Chemical & Pharmaceutical Bulletin 2007 55(4) 551-556 Two New Steroid Glycosides and a New Sesquiterpenoid Glycoside from the Underground Parts of Trillium kamtschaticum Masateru ONO,Chika TAKAMURA,Fumie SUGITA,Chikako MASUOKA,Hitoshi YOSHIMITSU,Tsuyoshi IKEDA,and Toshihiro NOHARAc Structure 13C NMR 碳谱模拟图 5 . 25(R)-pennogenin-3-O-α-L-rhamnopyranosyl(1→2)-β-D-glucopyranoside 相似度:76.9% Chemistry of Natural Compounds 2008 44 821-823 STEROIDAL SAPONINS FROM Paris mairei Xiao-xiao Liu, Lei Wang,Jie Yang, and Qiang Wang Structure 13C NMR 碳谱模拟图 6 . pennogenin-3-O-α-L-rhamnopyranosyl(1→2)-β-D-glucopyranoside 相似度:76.9% Chemistry of Natural Compounds 2007 43 672-677 SEPARATION AND IDENTIFICATION OF STEROIDAL COMPOUNDS WITH CYTOTOXIC ACTIVITY AGAINST HUMAN GASTRIC CANCER CELL LINES IN VITRO FROM THE RHIZOMES OF Paris polyphylla VAR. chinensis Huang Yun, Cui Lijian, Zhan Wenhong Dou Yuhong,Wang Yongli, Wang Qiang, and Zhao Ding Structure 13C NMR 碳谱模拟图 7 . pennogenin diglycoside C39H60O12 相似度:76.9% Chinese Journal of Medicinal Chemistry 2005 15 25-30 Isolation and identif iciation of steroidal saponins from Paris polyphylla Smith KANG Li-ping, MA Bai-ping, ZHANG Jie, XIONG Cheng-qi, TAN Da-wei, CONG Yu-wen Structure 13C NMR 碳谱模拟图 8 . Tb 相似度:76.9% Chinese Jouranl of Magnetic Resonance 2012 29 101-111 An NMR Study on Two Glucosylated Steroidal Saponins of Tb KANG Li-ping, WANG Yong-ze, FENG Bing, ZHOU Wen-bin, XIONG Cheng-qi, ZHAO Yang, TAN Da-wei, LIU Chao, MA Bai-ping Structure 13C NMR 碳谱模拟图 9 . pallidifloside C C39H62O14 相似度:76.9% Journal of Asian Natural Products Research 2011 13 1014-1022 Three new steroidal saponins from Fritillaria pallidiflora Shuo Shen, Chao-Jun Chen, Ren Bu, Lu Ga, Guo-Yu Li, Yong Tan, Xian Li and Jin-Hui Wang Structure 13C NMR 碳谱模拟图 10 . pennogenin-3-O-α-L-rhamnopyranosyl-(1→2)-β-D-glucopyranoside C39H62O13 相似度:76.9% Acta Botanica Yunnanica 1983 5 91-97 STUDLES ON THE SAPONIN COMPONENTS OF PLANTS IN YUNNAN VI. STESOID GLYCOSIDES OF PARIS POLYPHYLLA SM. VAR. YUNNANENSIS (FR.) H-M. (2 ) Chen Changxiang, Zhang Yutong and Zhou Jun Structure 13C NMR 碳谱模拟图 11 . pennogenin 3-O-β-L-rhamnopyranosyl-(1→2)-β-D-glucopyranoside C39H62O13 相似度:76.3% West China Journal of Pharmaceutical Sciences 2009 24 007-009 Chemical constituents of Paris polyphylla var. pseudothibetica XIAO Cao-mao, HUANG Jing, TAN Xiao-yan, TANG Min, ZHANG Hao Structure 13C NMR 碳谱模拟图 12 . pennogenin-3-O-α-L-rhamnopyranosyl(1→2)-[α-L-arabinofuranosyl(1→4)]-β-D-glucopyranoside 相似度:74.3% Chemistry of Natural Compounds 2007 43 672-677 SEPARATION AND IDENTIFICATION OF STEROIDAL COMPOUNDS WITH CYTOTOXIC ACTIVITY AGAINST HUMAN GASTRIC CANCER CELL LINES IN VITRO FROM THE RHIZOMES OF Paris polyphylla VAR. chinensis Huang Yun, Cui Lijian, Zhan Wenhong Dou Yuhong,Wang Yongli, Wang Qiang, and Zhao Ding Structure 13C NMR 碳谱模拟图 13 . hauptsaponine S1 相似度:74.3% Pharmazie 1987 42 143-143 Steroidsaponine aus Dioscorea hispida L. Ng. X. Cuong, D. Zeigan, Gabriele Voigt, und K. Hiller Structure 13C NMR 碳谱模拟图 14 . Paris Saponins VII 相似度:74.3% Natural Product Research and Development 2011 23 1017-1020 Chemical Constituents of Phyllanthus niruri L. ZHU, Hong-lin, WEI, Wan-xing, ZHOU, Min, YANG, Dan, FAN, Xi-wang, LIU, Jian-xiong Structure 13C NMR 碳谱模拟图 15 . 26-O-β-D-glucopyranosyl-(25R)-furost-5-en-3β,17α,22α,26-tetraol-3-O-[2''-OAc-α-L-rhamnopyranosyl-(1→2)]-β-D-xylopyranosyl-(1→3)-β-D-glucopyranoside C52H84O24 相似度:74.3% Chemistry of Natural Compounds 2014 50 489-493 Steroidal Saponins from Polygonatum glaberrimum Rhizomes L. N. Gvazava, V. S. Kikoladze Structure 13C NMR 碳谱模拟图 16 . (25R)-17α-hydroxyspirost-5-en-3β-yl O-α-L-rhamnopyranosyl-(1→2)-β-D-xylopyranoside C38H60O12 相似度:73.6% Steroids 2013 78 670-682 Steroidal glycosides from the bulbs of Fritillaria meleagris and their cytotoxic activities Yukiko Matsuo, Daisuke Shinoda, Aina Nakamaru, Yoshihiro Mimaki Structure 13C NMR 碳谱模拟图 17 . (25R)-spirost-5-en-3β,17α-diol 3-O-[α-L-rhamnopyranosyl-(1→2)]-β-D-glucopyranosyl-(1→4)-β-D-xylopyranoside C44H70O17 相似度:72.5% Chemistry of Natural Compounds 2014 50 489-493 Steroidal Saponins from Polygonatum glaberrimum Rhizomes L. N. Gvazava, V. S. Kikoladze Structure 13C NMR 碳谱模拟图 18 . Diosgenyl β-L-fucopyranosyl-(1→2)-β-D-glucopyranoside C39H62O12 相似度:71.7% Bioorganic & Medicinal Chemistry 2008 16 2063-2076 Synthesis of novel spirostanic saponins and their cytotoxic activity Juan C. Hernández, Francisco León, Ignacio Brouard, Fernando Torres, Sara Rubio, José Quintana, Francisco Estévez, Jaime Bermejo Structure 13C NMR 碳谱模拟图 19 . pennogenin 3-O-α-L-arabinofuranosyl(1→4)-[α-L-rhamnopyranosyl(1→2)]-β-D-glucopyranoside 相似度:71.7% Acta Botanica Yunnanica 1983 5 219-223 STUDIES ON THE SAPONIN COMPONENTS OF PLANTS IN YUNNAN VIII STEROIDAL SAPONINS IN PARIS LUQUANENSIS Chen Changxiang, Zhou Jun, Zhang Yutong, Gao Chongkun Structure 13C NMR 碳谱模拟图 20 . (25S)spirost-5-en-3β,17α,27-triol-3-O-[β-D-glucopyranosy(1-4)[α-L-arabinopyranpsy](1-6)]-β-D-glucopyranoside 相似度:71.0% Chinese Chemical Letters 1992 3 431-432 NEW MINOR STEROIDAL SAPONINS FROM SMILAXLEBRUNII ZHONG JIAN JIA,YONG JU AND MEI DU Structure 13C NMR 碳谱模拟图 21 . Aspafilioside F C38H62O13 相似度:71.0% Steroids 2008 73 83-87 Steroidal saponins from the roots of Asparagus filicinus Li-Bo Zhou, Dao-Feng Chen Structure 13C NMR 碳谱模拟图 22 . compound 7 相似度:71.0% Phytochemistry 1994 36 1005-1008 Steroidal prosapogenins from Dioscorea olfersiana Mitsue Haraguchi, Ana Paula Zaccarias Dos Santos, Maria Claudia Marx Young, Edison Paulo Chui Structure 13C NMR 碳谱模拟图 23 . (25S)-spirost-5-en-3β,17α,27-triol-3-O-[α-L-arabinopyranosyl(1→6)]-β-D-glucopyranoside 相似度:71.0% Phytochemistry 1993 33 1193-1195 Minor steroidal glycosides from the roots of Smilax lebrunii Ju Zhong-Jian Jia Yong Structure 13C NMR 碳谱模拟图 24 . pennogenin-3-O-β-D-glucopyranoside 相似度:71.0% Chinese Traditional and Herbal Drugs 2005 36 978-982 Biotransformation of polyphyllins by Curvularia lunata fermentation FENG Bing; MA Bai-ping; KANG Li-ping; XIONG Cheng-qi; WANG Sheng-qi Structure 13C NMR 碳谱模拟图 25 . pennogenin-3-O-β-D-glucopyrano-side 相似度:71.0% Tetrahedron 2007 63 6796-6812 The substrate specificity of a glucoamylase with steroidal saponin-rhamnosidase activity from Curvularia lunata Bing Feng, Li-ping Kang, Bai-ping Ma, Bo Quan, Wen-bin Zhou, Yong-ze Wang, Yu Zhao, Yi-xun Liu, Sheng-qi Wang Structure 13C NMR 碳谱模拟图 26 . pennogenin-3-O-α-L-arabinofuranosyl-(1→4)-β-D-glucopyranoside 相似度:71.0% Tetrahedron 2007 63 6796-6812 The substrate specificity of a glucoamylase with steroidal saponin-rhamnosidase activity from Curvularia lunata Bing Feng, Li-ping Kang, Bai-ping Ma, Bo Quan, Wen-bin Zhou, Yong-ze Wang, Yu Zhao, Yi-xun Liu, Sheng-qi Wang Structure 13C NMR 碳谱模拟图 27 . compound A1 相似度:71.0% Acta Botanica Yunnanica 1990 12 323-329 STEROID SAPONINS OF AERIAL PARTS OF PARIS POLYPHYLLA VAR. YUNNANENSIS Chen Changxiang, Zhou Jun, Zhang Yutong, Zhao Yongyan Structure 13C NMR 碳谱模拟图 28 . (25S)-17α,27-dihydroxyspirost-5-en-3β-yl O-(4-O-acetyl-α-L-rhamnopyranosyl)-(1→2)-β-D-glucopyranoside C41H64O15 相似度:70.7% Phytochemistry 2008 69 2724-2730 Steroidal glycosides from the underground parts of Trillium erectum and their cytotoxic activity Akihito Yokosuka , Yoshihiro Mimaki Structure 13C NMR 碳谱模拟图 29 . diosgenin 3-O-α-L-rhamnopyranosyl-(1→2)-β-D-glucuroniduronic acid methyl ester 相似度:70% Zeitschrift für Naturforschung C 2006 61 171-176 Diosgenin Glucuronides from Solanum lyratum and their Cytotoxicity against Tumor Cell Lines L.-X. Sun, W.-W. Fu, W. Li, K.-S. Bi, and M.-W. Wang Structure 13C NMR 碳谱模拟图 30 . (3β,17α,25R)-spirost-5-ene-3,17-diol-3-O-β-D-xylopyranosyl-(1→5)-α-L-arabinofuranosyl-(1→4)-β-D-glucopyranoside C43H68O17 相似度:69.7% Phytochemistry 2012 81 133-143 Steroidal saponins from Paris polyphylla var. yunnanensis Xia Wu, Lei Wang, Hui Wang, Yi Dai, Wen-Cai Ye, Yao-Lan Li Structure 13C NMR 碳谱模拟图 31 . trikamsteroside A C39H62O14 相似度:69.2% Chemical & Pharmaceutical Bulletin 2007 55(4) 551-556 Two New Steroid Glycosides and a New Sesquiterpenoid Glycoside from the Underground Parts of Trillium kamtschaticum Masateru ONO,Chika TAKAMURA,Fumie SUGITA,Chikako MASUOKA,Hitoshi YOSHIMITSU,Tsuyoshi IKEDA,and Toshihiro NOHARAc Structure 13C NMR 碳谱模拟图 32 . (25S)spirost-5-en-3β,17α,27-triol-3-O-(α-L-rhamnopyranosyl(1-4))-β-D-glucopyranoside 相似度:69.2% Chinese Chemical Letters 1993 4 137-138 TWO MINOR SPIROSTANOL GLYCOSIDES FROM YONG JU,ZHONG JIAN JIA,HAI RUO PENG AND XUE JUN SUN Structure 13C NMR 碳谱模拟图 33 . (25S)spirost-5-en-3β,17α,27-triol-3-O-[α-1-rhamnopyranosyl(1→4)]-β-D-galactopyranoside 相似度:69.2% Phytochemistry 1994 37 1433-1436 Steroidal saponins from Smilax menispermoidea and S. Lebrunii Ju Yong, Jia Zhongjian, Sun Xuejun Structure 13C NMR 碳谱模拟图 34 . Pennogenin-3-O-α-L-rhamnopyranosyl-(1→3)-β-D-glucopyranoside 相似度:69.2% Archives of Pharmacal Research 2008 31 653-658 In vivo anti-inflammatory effect of a new steroidal saponin, mannioside A, and its derivatives isolated from Dracaena mannii Leon Azefack Tapondjou, Kemvoufo Beaudelaire Ponou, Remy Bertrand Teponno, Marius Mbiantcha and Jules Désiré Djoukeng, et al. Structure 13C NMR 碳谱模拟图 35 . penogenin 3-O-β-D-glucopyranoside 相似度:68.4% Chemical & Pharmaceutical Bulletin 2007 55(4) 551-556 Two New Steroid Glycosides and a New Sesquiterpenoid Glycoside from the Underground Parts of Trillium kamtschaticum Masateru ONO,Chika TAKAMURA,Fumie SUGITA,Chikako MASUOKA,Hitoshi YOSHIMITSU,Tsuyoshi IKEDA,and Toshihiro NOHARAc Structure 13C NMR 碳谱模拟图 36 . compound 7 相似度:68.4% Chemical & Pharmaceutical Bulletin 1989 37 116-118 Studies on the Constituents of Heloniopsis orientalis (THUNB.) C. TANAKA Kimiko NAKANO,Kotaro MURAKAMI,Yoshihisa TAKAISHI,Toshiaki TOMIMATSU and Toshihiro NOHARA Structure 13C NMR 碳谱模拟图 37 . Diosgenyl β-D-xylopyranosyl-(1→2)-β-D-glucopyranoside C38H60O12 相似度:68.4% Bioorganic & Medicinal Chemistry 2008 16 2063-2076 Synthesis of novel spirostanic saponins and their cytotoxic activity Juan C. Hernández, Francisco León, Ignacio Brouard, Fernando Torres, Sara Rubio, José Quintana, Francisco Estévez, Jaime Bermejo Structure 13C NMR 碳谱模拟图 38 . 偏诺皂苷元-3-O-β-D-葡萄糖苷 相似度:68.4% Chinese Traditional and Herbal Drugs 2005 36 978-982 Biotransformation of polyphyllins by Curvularia lunata fermentation FENG Bing; MA Bai-ping; KANG Li-ping; XIONG Cheng-qi; WANG Sheng-qi Structure 13C NMR 碳谱模拟图 39 . ruscogenin 1-O-β-D-glucopyranoside 相似度:68.4% Natural Product Research and Development 2013 25 1017-1021 Study on the Biotransformation of Pennogenin by Gliocladium deliquescens NRRL 1086 DU Chen-Hui, ZHANG Jian*, YU Bo-Yang* Structure 13C NMR 碳谱模拟图 40 . diosbulbiside A C39H62O14 相似度:66.6% Journal of Natural Products 2009 72 1964-1968 Steroidal Sapogenins and Glycosides from the Rhizomes of Dioscorea bulbifera Hai Liu, Gui-Xin Chou,Tao Wu,Yin-Long Guo, Shun-Chun Wang, Chang-Hong Wang, and Zheng-Tao Wang Structure 13C NMR 碳谱模拟图 41 . (25S)-27-hydroxypenogenin 3- O-α-L-rhamnopyranosyl-(1→2)-O-β-D-glucopyranoside C39H62O14 相似度:66.6% Chemical & Pharmaceutical Bulletin 2007 55(4) 551-556 Two New Steroid Glycosides and a New Sesquiterpenoid Glycoside from the Underground Parts of Trillium kamtschaticum Masateru ONO,Chika TAKAMURA,Fumie SUGITA,Chikako MASUOKA,Hitoshi YOSHIMITSU,Tsuyoshi IKEDA,and Toshihiro NOHARAc Structure 13C NMR 碳谱模拟图 42 . compound 2a C39H64O13 相似度:66.6% Chemical & Pharmaceutical Bulletin 1988 36 3226-3229 26-O-ACYLATED FUROSTANOL SAPONINS PARDARINOSIDE A AND B FROM THE BULBS OF LILIUM PARDARINUM Hiroko Shimomura,Yutaka Sashida and Yoshihiro Mimaki Structure 13C NMR 碳谱模拟图 43 . Diosgenyl α-L-rhamnopyranosyl-(1→2)-β-D-glucopyranoside C39H62O12 相似度:66.6% Bioorganic & Medicinal Chemistry 2008 16 2063-2076 Synthesis of novel spirostanic saponins and their cytotoxic activity Juan C. Hernández, Francisco León, Ignacio Brouard, Fernando Torres, Sara Rubio, José Quintana, Francisco Estévez, Jaime Bermejo Structure 13C NMR 碳谱模拟图 44 . solanoside A 相似度:66.6% Chemistry of Natural Compounds 2014 49 1091-1094 Two New Steroidal Glycosides from Solanum surattense Haq Nawaz, Ejaz Ahmed, Ahsan Sharif, Muhammad Arshad, Nayab Batool, Muhammad Azam Rasool, Mukhtar-Ul-Hassan Structure 13C NMR 碳谱模拟图 45 . Diosgenin 3-O-[α-L-rhamnopyranosyl(1→2)]-[β-D-glucopyranosyl(1→3)-β-D-glucopyranosyl(1→4)]-β-D-glucopyranoside 相似度:66.6% Journal of Separation Science 2008 31 2486-2491 Preparative separation of dioscin derivatives from Dioscorea villosa by centrifugal partition chromatography coupled with evaporative light scattering detection Kee Dong Yoon and Jinwoong Kim Structure 13C NMR 碳谱模拟图 46 . paris saponin V 相似度:66.6% Chinese Traditional and Herbal Drugs 2013 44 2808-2811 Studies on chemical constituents in roots and rhizomes of Trillium tschonoskii (II) ZHANG Zhong-li, ZUO Yue-ming, CAI Miao-ting, WANG Yan-yan Structure 13C NMR 碳谱模拟图 47 . diosgenin3-O-β-D-glucopyranosyl-(1→3)-[α-L-rhamnopyranosyl-(1→2)]-β-D-glucopyranoside 相似度:65.8% West China Journal of Pharmaceutical Sciences 2010 25 508-511 Isolation and identification of steroidal saponins of Paris polyphylla Smith var. pseudothibetica LIU Xian-bo, ZHANG Hao, YONG Zheng-ping, XUE Dan Structure 13C NMR 碳谱模拟图 48 . diosgenin 3-O-[α-L-pyranrhamnose(1→2)][β-D-pyranxylose(1→3)]-β-D-pyranglycoside C44H70O16 相似度:65.8% Northwest Pharmaceutical Journal 2013 28 562-565 Studies on the chemical constituents of the flowers of Ophiopogon japonicus ZHANG Jinghua, REN Lu, MA Yufang, BAO He, ZHAO Guilan, JING Hang, WANG Junxian Structure 13C NMR 碳谱模拟图 49 . compopund 15 相似度:65.7% Chemical & Pharmaceutical Bulletin 1982 30 712-718 Steroid Saponins from Paris polyphylla SM.-Supplement MITSUHIKO MIYAMURA,KIMIKO NAKANO,TOSHIHIRO NOHARA,TOSHIAKI TOMIMATSU and TOSHIO KAWASAKI Structure 13C NMR 碳谱模拟图 50 . (25S)spirost-5-en-3β,17α,27-triol-3-O-[β-D-glucopyranosy(1-4)[α-L-arabinopyranpsy](1-6)]-β-D-glucopyranoside 相似度:65.7% Chinese Chemical Letters 1991 2 853-854 A NEW STEROIDAL SAPONIN FROM SMILAX LEBRUNII YONG JU ZHONG JIAN JJA AND YI NAN WU Structure 13C NMR 碳谱模拟图 |
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