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[求助]
微 谱 求 助 ！！！O(∩_∩)O谢谢！ 已有1人参与
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化合物1 13C谱 溶剂为CDCl3： 24.60,26.73,29.70,31.08,39.53,50.89,52.62,57.57,67.31,99.99,102.28,108.62,116.06,119.11,127.59,127.78,128.72,134.18,138.28,158.29,171.57 化合物2 13C 溶剂为DMSO： 22.69,23.97,26.58,30.73,50.94,52.74,57.28,67.27,101.68,107.55,115.43,119.51,124.28,125.96,128.36,128.41,132.57,139.16,151.20,157.85,170.25 万分感谢！！！ |
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【答案】应助回帖
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感谢参与，应助指数 +1
zxy19900804: 金币+10, ★★★★★最佳答案, O(∩_∩)O谢谢！ 2014-12-21 19:38:22
感谢参与，应助指数 +1
zxy19900804: 金币+10, ★★★★★最佳答案, O(∩_∩)O谢谢！ 2014-12-21 19:38:22
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1 1 . Aripiprazole contaminant 相似度:69.5% Bioorganic & Medicinal Chemistry Letters 2003 13 65-68 Synthetic study on the unique dimeric arylpiperazine: access to the minor contaminant of aripiprazole Yasuhiro Torisawa, Koichi Shinhama, Takao Nishi, Jun-ichi Minamikawa Structure 13C NMR Structure & 13C NMR 碳谱模拟图 2 . (-)-(3S,4aS,8aS,2'R,3'R)-2-[3'-Ammino-2'-hydroxy-4'-phenyl-butyl]-N-tert-butyldecahydro-iso-quinoline-3-carboxamide C24H39N3O2 相似度:61.9% Bioorganic & Medicinal Chemistry 2008 16 902-908 Stereocontrolled synthesis and biological activity of two diastereoisomers of the potent HIV-1 protease inhibitor saquinavir Giuliana Righi, Simona Ciambrone,Carlo Bonini and Pietro Campaner Structure 13C NMR Structure & 13C NMR 碳谱模拟图 3 . butyrolactone IV C24H24O8 相似度:59.0% Mycosystema 2013 32 277-285 The antibacterial polyketides of Aspergillus terreus OUCMDZ-1925 from Yellow River delta CHEN Zheng-Qian, LIU Pei-Pei, WANG Yi, ZHU Wei-Ming Structure 13C NMR Structure & 13C NMR 碳谱模拟图 4 . isoalschomine C21H24N2O5 相似度:57.1% Chemical & Pharmaceutical Bulletin 1989 37 887-890 Alschomine and Isoalschomine, New Alkaloids from the Leaves of Alstonia scholaris Fumiko ABE,Rong-Fu CHEN,Tatsuo YAMAUCHI,Nobuhiro MARUBAYASHI and Ikuhiko UEDA Structure 13C NMR Structure & 13C NMR 碳谱模拟图 5 . 7-Benzyl-3-chloro-1-(piperidin-1-yl)-5,6,7,8-tetrahydro-2,7-naphthyridine-4-carbonitrile 相似度:57.1% Bioorganic & Medicinal Chemistry Letters 2010 20 2785-2789 Cheng Guo, Peter R. Guzzo, Mark Hadden, Bruce J. Sargent, Larry Yet, Yanqing Kan, Oksana Palyha, Theresa M. Kelly, Xiaoming Guan, Kim Rosko, Karen Gagen, Joseph M. Metzger, Jasminka Dragovic, Kathryn Lyons, Linus S. Lin, Ravi P. Nargund Cheng Guo, Peter R. Guzzo, Mark Hadden, Bruce J. Sargent, Larry Yet, Yanqing Kan, Oksana Palyha, Theresa M. Kelly, Xiaoming Guan, Kim Rosko, Karen Gagen, Joseph M. Metzger, Jasminka Dragovic, Kathryn Lyons, Linus S. Lin, Ravi P. Nargund Structure 13C NMR Structure & 13C NMR 碳谱模拟图 6 . compound 4d 相似度:57.1% Tetrahedron Letters 1997 38 1293-1296 Autoxidation of pyrrolylurethanes Clotilde Pichon-Santander, Ramaswamy Shankar, A.Ian Scott Structure 13C NMR Structure & 13C NMR 碳谱模拟图 7 . compound 5d 相似度:57.1% Tetrahedron Letters 1997 38 1293-1296 Autoxidation of pyrrolylurethanes Clotilde Pichon-Santander, Ramaswamy Shankar, A.Ian Scott Structure 13C NMR Structure & 13C NMR 碳谱模拟图 8 . 5-tert-butyl-N-(3-(4-(2,3-dichlorophenyl)piperazin-1-yl)propyl)-1,2-dimethyl-1H-pyrrole-3-carboxamide 相似度:57.1% Bioorganic & Medicinal Chemistry 2010 18 6156-6169 Further optimization of novel pyrrole 3-carboxamides for targeting serotonin 5-HT2A, 5-HT2C, and the serotonin transporter as a potential antidepressant Suk Youn Kang, Eun-Jung Park, Woo-Kyu Park, Hyun Jung Kim, Gildon Choi, Myung Eun Jung, Hee Jeong Seo, Min Ju Kim, Ae Nim Pae, Jeongmin Kim, Jinhwa Lee Structure 13C NMR Structure & 13C NMR 碳谱模拟图 9 . 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Synthesis and Biological Evaluation of Platelet-Activating Factor Antagonists with Anti-HIV-1 Activity Nawal Serradji, Marc Martin, Okkacha Bensaid, Salvatore Cisternino, Christophe Rousselle, Nathalie Dereuddre-Bosquet, Jack Huet, Catherine Redeuilh, Aazdine Lamouri, Chang-Zhi Dong, Pascal Clayette, Jean-Michel Scherrmann, Dominique Dormont, and Françoise Structure 13C NMR Structure & 13C NMR 碳谱模拟图 2 1 . butyrolactone III C24H24O8 相似度:63.6% Mycosystema 2013 32 277-285 The antibacterial polyketides of Aspergillus terreus OUCMDZ-1925 from Yellow River delta CHEN Zheng-Qian, LIU Pei-Pei, WANG Yi, ZHU Wei-Ming Structure 13C NMR Structure & 13C NMR 碳谱模拟图 2 . Aripiprazole contaminant 相似度:60.8% Bioorganic & Medicinal Chemistry Letters 2003 13 65-68 Synthetic study on the unique dimeric arylpiperazine: access to the minor contaminant of aripiprazole Yasuhiro Torisawa, Koichi Shinhama, Takao Nishi, Jun-ichi Minamikawa Structure 13C NMR Structure & 13C NMR 碳谱模拟图 3 . 2-(ethyl(6-(5,6,7,8-tetrahydroacridin-9-ylamino)hexyl)amino)-N-(4-phenylthiazol-2-yl)acetamide 相似度:57.6% Bioorganic & Medicinal Chemistry 2012 20 6513-6522 Novel multipotent phenylthiazole–tacrine hybrids for the inhibition of cholinesterase activity, β-amyloid aggregation and Ca2+ overload Yue Wang, Fang Wang, Jun-Ping Yu, Feng-Chao Jiang, Xin-Lei Guan, Can-Ming Wang, Lei Li, Hui Cao, Ming-Xing Li, Jian-Guo Chen Structure 13C NMR Structure & 13C NMR 碳谱模拟图 4 . 7-(4-(2-(piperidin-1-yl)ethoxy)phenyl)-1,2,3,9-tetrahydropyrrolo[2,1-b]quinazolin-3-ol C24H29N3O2 相似度:57.1% Natural Product Research 2006 20 735-741 Natural products as templates for bioactive compound libraries: synthesis of biaryl derivatives of (±)-vasicine Sergey V. 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