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namujila

金虫 (正式写手)

[求助] 微谱求助4.4已有1人参与

13C NMR (126 MHz, DMSO) δ13.57, 18.53, 18.81, 21.19, 28.56, 30.89, 41.13, 48.49, 54.80, 56.50, 60.87, 60.97, 61.28, 61.39, 61.44, 65.31, 68.18, 68.26, 69.38, 69.75, 69.85, 69.93, 72.98, 73.01, 73.09, 73.89, 76.21, 76.34, 76.68, 77.12, 77.25, 94.83, 96.11, 98.36, 98.60, 99.75, 103.48, 103.76, 104.18, 111.15, 116.07, 116.45, 120.41, 122.15, 123.86, 132.26, 137.47, 142.56, 144.26, 144.62, 147.05, 148.12, 152.00, 152.26, 163.70, 175.41
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seuseasoar

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【答案】应助回帖

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感谢参与,应助指数 +1
namujila: 金币+8, ★★★★★最佳答案 2014-12-07 11:46:13
Natural Product Research          2009          23          963-972
Structure and activities of a steroidal saponin from Chlorophytum nimonii (Grah) Dalz
Vijai Lakshmi; Rajesh Kumar; Kartikey Pandey; Bhawani Shanker Joshi; Raja Roy; Kunnath Padamnabham Madhusudanan; Priti Tiwari; Arvind Kumar Srivastava
Structure      13C NMR   碳谱模拟图
2 .     solanidine-3-O-α-L-rhamnopyranosyl-(1→2)-[β-D-glucopyranosyl-(1→3)-β-D-glucopyranosyl-(1→4)]-β-D-glucopyranoside
    相似度:53.5%
Acta Botanica Boreali-Occidentalia Sinica          2005          25          1158-1162
Glycosidal Steroidal alkaloids from Notholirion bulbuliferum
ZHOU Le, DONG Xu-jun, ZHAO Hai-shuang, GENG Hu i-ling
Structure      13C NMR   碳谱模拟图
3 .     Kaempferol-3-O-β-D-glucopyransoyl-(1→4)-α-L-rhamnopyranosyl-(1→6)-β-D-galactopyranoside7-O-(6′′′′-O-acetyl-β-D-glucopyranosyl-(1→3)-[α-L-rhamnopyranosyl-(1→2)]-β-D-glucopyranoside
C53H72O35     相似度:53.5%
Molecules          2007          12          328-344
Acylated Flavone Glycosides from the Roots of Saussurea lappa and Their Antifungal Activity
Kolisetty S. Rao, Goriparthi V. Babu and Yemireddy V. Ramnareddy
Structure      13C NMR   碳谱模拟图
4 .     Kaempferol-3-O-β-D-glucopyranosyl(1→2)-β-D-(6a′-O-caffeoyl)-glucopyranoside 7-O-(6′′′′-O-acetyl-β-D-glucopyranosyl-(1→3)-[α-L-rhamnopyranosyl-(1→2)]-β-D-glucopyranoside
C53H72O35     相似度:53.5%
Molecules          2007          12          328-344
Acylated Flavone Glycosides from the Roots of Saussurea lappa and Their Antifungal Activity
Kolisetty S. Rao, Goriparthi V. Babu and Yemireddy V. Ramnareddy
Structure      13C NMR   碳谱模拟图
5 .     mutongsaponin E
C57H90O25     相似度:52.6%
Phytochemistry          2006          67          2697-2705
Triterpenoid saponins and phenylethanoid glycosides from stem of Akebia trifoliata var. australis
Huimin Gao, Zhimin Wang
Structure      13C NMR   碳谱模拟图
6 .     Clematangoside A
C59H96O23     相似度:52.5%
Planta Medica          2013          78          673-679
Triterpenoid Saponins with Anti-Myocardial Ischemia Activity from the Whole Plants of Clematis tangutica
Zhang, Wei; Yao, Min-Na; Tang, Hai-Feng; Tian, Xiang-Rong; Wang, Min-Chang; Ji, Lan-Ju; Xi, Miao-Miao:
Structure      13C NMR   碳谱模拟图
7 .     clematibetoside C
C53H86O22     相似度:51.7%
Chemical & Pharmaceutical Bulletin          2001          49(5)          635-638
Studies on the Constituents of Clematis Species. VIII. Triterpenoid Saponins from the Aerial Part of Clematis tibetana KUNTZ
Yukio KAWATA, Haruhisa KIZU, Yukinori MIYAICHI, and Tsuyoshi TOMIMORI
Structure      13C NMR   碳谱模拟图
8 .     pigment 3
C58H64O31     相似度:51.7%
Phytochemistry          2008          69          1029-1036
Triacylated cyanidin 3-(3X-glucosylsambubioside)-5-glucosides from the flowers of Malcolmia maritima
Fumi Tatsuzawa, Norio Saito, Kenjiro Toki, Koichi Shinoda, Atsushi Shigihara, Toshio Honda
Structure      13C NMR   碳谱模拟图
9 .     mutongsaponin B
C52H82O23     相似度:51.7%
Phytochemistry          2006          67          2697-2705
Triterpenoid saponins and phenylethanoid glycosides from stem of Akebia trifoliata var. australis
Huimin Gao, Zhimin Wang
Structure      13C NMR   碳谱模拟图
10 .     3-O-[β-D-3-O-trans-p-coumaroyl-glucopyranosyl-(1→3)]-[β-D-glucopyranosyl-(1→2)]-α-L-arabinopyranosy echinocystic acid 28-O-[α-L-rhamnopyranosyl-(1→4)-β-D-glucopyranosyl-(1→6)-β-D-glucopyrsanosyl] ester
C74H112O34     相似度:51.7%
Phytochemistry          2004          65          3089-3095
Saponins and acylated saponins from Dizygotheca kerchoveana
F.R. Melek, Toshio Miyase, S.M. Abdel-Khalik, I.I. Mahmoud, S.A. Mina
Structure      13C NMR   碳谱模拟图
11 .     3-O-[β-D-3-O-cis-p-coumaroyl-glucopyranosyl-(1→3)]-[β-D-glucopyranosyl-(1→2)]-α-L-arabinopyranosyl echinocystic acid 28-O-[α-L-rhamnopyranosyl-(1→4)-β-D-glucopyranosyl-(1→6)-β-D-glucopyranosyl] ester
C74H112O34     相似度:51.7%
Phytochemistry          2004          65          3089-3095
Saponins and acylated saponins from Dizygotheca kerchoveana
F.R. Melek, Toshio Miyase, S.M. Abdel-Khalik, I.I. Mahmoud, S.A. Mina
Structure      13C NMR   碳谱模拟图
12 .     3-O-β-D-glucopyranosyl-quillaic acid-28-O-α-L-rhamnopyranosyl-(1→2)-α-L-arabinopyranosyl-(1→2)[β-D-glucopyranosyl-(1→6)]-β-D-glucopyranoside
C59H94O28     相似度:51.7%
Journal of Natural Products          2001          64          920-924
Three New Acylated Triterpene Saponins from Acanthophyllum squarrosum
Ghezala Gaidi, Tomofumi Miyamoto, Abdolhossein Rustaiyan, and Marie-Aleth Lacaille-Dubois
Structure      13C NMR   碳谱模拟图
13 .     compound 2
    相似度:51.7%
Chemistry of Natural Compounds          1985          21          197-202
STRUCTURE OF PSOLUSOSIDE A - THE MAIN TRITERPENE GLYCOSIDE FROM THE HOLOTHURIAN Vsolus fahricii
V. I. Kalinin, A. I. Kalinovskii, and V. A. Stonik
Structure      13C NMR   碳谱模拟图
14 .     agamenoside A
C56H92O28     相似度:51.7%
Chinese Chemical Letters          2002          13          629-632
Two New Steroidal Glycosides from Fermented Leaves of Agave americana
Jian Ming JIN, Xi Kui LIU, Rong Wei TENG, Chong Ren YANG
Structure      13C NMR   碳谱模拟图
15 .     3-O-α-L-arabinopyranosyl-30- norhederagenin-28-O-α-L-rhamnopyranosyl-(1→4)-β-D-glucopyranosyl-(1→6)-β-D-glucopyranosyl ester
C52H82O2     相似度:51.7%
Journal of Asian Natural Products Research          2007          9          175-182
Triterpenoid saponins from Stauntonia chinensis
H. GAO, X. ZHANG, N.-L. WANG, H.-W. LIU, Q.-H. ZHANG,S.-S. SONG, Y. YU and X.-S. YAO
Structure      13C NMR   碳谱模拟图
尼赫
2楼2014-12-07 11:17:22
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