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[求助]
微谱求助2014.12.6 已有1人参与
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70-4 13C NMR (101 MHz, Acetone) δ 217.60, 176.81, 169.15, 137.89, 99.99, 71.50, 68.91, 64.34, 57.57, 49.52, 48.40, 47.97, 46.44, 45.26, 39.90, 36.86, 35.31, 35.00, 34.59, 33.13, 30.41, 26.37, 24.74, 23.93, 22.41, 22.30, 20.17, 19.75, 19.56, 19.17, 18.75. |
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3楼2014-12-06 21:24:26
月宫折桂
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【答案】应助回帖
感谢参与，应助指数 +1
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查询结果：共查到7个化合物(查询结果仅供参考) 1 . Cholest-4α-methyl-8-en-7α-acetoxy-3-one C30H48O3 相似度:58.0% Steroids 2006 71 476-483 Synthesis and antitumor activity of cholest-4α-methyl-7-en-3β-ol derivatives Lan He, Yumei Liu, Jiangong Shi, Qiang Pei Structure 13C NMR 碳谱模拟图 2 . Penicisteroid A C30H50O6 相似度:58.0% Bioorganic & Medicinal Chemistry Letters 2011 21 2894-2897 Penicisteroids A and B, antifungal and cytotoxic polyoxygenated steroids from the marine algα-derived endophytic fungus Penicillium chrysogenum QEN-24S Shu-Shan Gao, Xiao-Ming Li, Chun-Shun Li, Peter Proksch, Bin-Gui Wang Structure 13C NMR 碳谱模拟图 3 . Cholest-4α-methyl-8-en-7α-ecetoxy-3β-ol C28H46O 相似度:54.8% Steroids 2006 71 476-483 Synthesis and antitumor activity of cholest-4α-methyl-7-en-3β-ol derivatives Lan He, Yumei Liu, Jiangong Shi, Qiang Pei Structure 13C NMR 碳谱模拟图 4 . Gardenoin H C30H48O3 相似度:54.8% Chemical & Pharmaceutical Bulletin 2011 59(3) 385-387 Gardenoins E-H, Cycloartane Triterpenes from the Apical Buds of Gardenia obtusifolia Thanesuan NUANYAI, Ruengrit SAPPAPAN, Tirayut VILAIVAN, and Khanitha PUDHOM Structure 13C NMR 碳谱模拟图 5 . schleicheol 2 C30H52O2 相似度:51.6% Journal of Asian Natural Products Research 2001 3 299-311 CONSTITUENTS FROM LIMONIA CRENULATA XUE-ME1 NIU, SHENG-HONG LI, LI-YAN PENG,and HAN-DONG SUN,ZHONG-WEN LIN, GAO-XIONG RAO Structure 13C NMR 碳谱模拟图 6 . β-谷甾醇 相似度:51.6% Lishizhen Medicine and Materia Medica Research 2012 23 619-620 蝎子草抗菌活性成分的研究 江震献; 张晓林; 彭霞; 陈章宝 Structure 13C NMR 碳谱模拟图 7 . roseic acid 相似度:51.6% European Journal of Organic Chemistry 2014 5462-5468 Roseic Acid and Roseolactones A and B, Furan-Cucurbitane Triterpenes from Russula aurora and R. minutula (Basidiomycota) Marco Clericuzio, Giovanni Vidari, Claudio Cassino, Laura Legnani, and Lucio Toma Structure 13C NMR 碳谱模拟图 |
2楼2014-12-06 18:21:48
月宫折桂
木虫 (正式写手)
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刚刚又查了一遍还是一样查询结果：共查到7个化合物(查询结果仅供参考) 1 . Cholest-4α-methyl-8-en-7α-acetoxy-3-one C30H48O3 相似度:58.0% Steroids 2006 71 476-483 Synthesis and antitumor activity of cholest-4α-methyl-7-en-3β-ol derivatives Lan He, Yumei Liu, Jiangong Shi, Qiang Pei Structure 13C NMR 碳谱模拟图 2 . Penicisteroid A C30H50O6 相似度:58.0% Bioorganic & Medicinal Chemistry Letters 2011 21 2894-2897 Penicisteroids A and B, antifungal and cytotoxic polyoxygenated steroids from the marine algα-derived endophytic fungus Penicillium chrysogenum QEN-24S Shu-Shan Gao, Xiao-Ming Li, Chun-Shun Li, Peter Proksch, Bin-Gui Wang Structure 13C NMR 碳谱模拟图 3 . Cholest-4α-methyl-8-en-7α-ecetoxy-3β-ol C28H46O 相似度:54.8% Steroids 2006 71 476-483 Synthesis and antitumor activity of cholest-4α-methyl-7-en-3β-ol derivatives Lan He, Yumei Liu, Jiangong Shi, Qiang Pei Structure 13C NMR 碳谱模拟图 4 . Gardenoin H C30H48O3 相似度:54.8% Chemical & Pharmaceutical Bulletin 2011 59(3) 385-387 Gardenoins E-H, Cycloartane Triterpenes from the Apical Buds of Gardenia obtusifolia Thanesuan NUANYAI, Ruengrit SAPPAPAN, Tirayut VILAIVAN, and Khanitha PUDHOM Structure 13C NMR 碳谱模拟图 5 . schleicheol 2 C30H52O2 相似度:51.6% Journal of Asian Natural Products Research 2001 3 299-311 CONSTITUENTS FROM LIMONIA CRENULATA XUE-ME1 NIU, SHENG-HONG LI, LI-YAN PENG,and HAN-DONG SUN,ZHONG-WEN LIN, GAO-XIONG RAO Structure 13C NMR 碳谱模拟图 6 . β-谷甾醇 相似度:51.6% Lishizhen Medicine and Materia Medica Research 2012 23 619-620 蝎子草抗菌活性成分的研究 江震献; 张晓林; 彭霞; 陈章宝 Structure 13C NMR 碳谱模拟图 7 . roseic acid 相似度:51.6% European Journal of Organic Chemistry 2014 5462-5468 Roseic Acid and Roseolactones A and B, Furan-Cucurbitane Triterpenes from Russula aurora and R. minutula (Basidiomycota) Marco Clericuzio, Giovanni Vidari, Claudio Cassino, Laura Legnani, and Lucio Toma Structure 13C NMR 碳谱模拟图 |
4楼2014-12-07 00:13:31
月宫折桂
木虫 (正式写手)
- 应助: 335 (大学生)
- 金币: 3183.7
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- 帖子: 360
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【答案】应助回帖
★ ★ ★ ★ ★ ★ ★ ★
listentome: 金币+8, ★★★很有帮助 2014-12-07 15:59:01
listentome: 金币+8, ★★★很有帮助 2014-12-07 15:59:01
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以下是用全部溶剂查得结果 查询结果：共查到1452个化合物(查询结果仅供参考) 1 . alisol C 23-acetate C32H348O6 相似度:78.1% Phytochemistry 1994 36 119-127 Terpenoids of Alisma orientale rhizome and the crude drug alismatis rhizoma Yoshijiro Nakajima, Yohko Satoh, Masumi Katsumata (nee Ohtsuka), Kazuko Tsujiyama (nee Mikoshiba), Yoshiteru Ida, Junzo Shoji Structure 13C NMR 碳谱模拟图 2 . Alisol C 23-acetate C32H48O6 相似度:78.1% Archives of Pharmacal Research 2001 24 524-526 Cytotoxic triterpenoides from Alismatis Rhizoma SangMyung Lee, YungHee Kho, ByungSun Min, JinHee Kim and MinKyun Na, et al. Structure 13C NMR 碳谱模拟图 3 . alisol C monoacetate 相似度:75% Planta Medica 1988 54 445-447 li-Deoxyalisol C and Alisol D: New Protostane-Type Triterpenoids from Alisma plantago-aquatica Yoshiaysu Fukuyama, Geng Pei-Wu, Wang Rei, Toshihide Yamada, and Kazuyuki Nakagawa Structure 13C NMR 碳谱模拟图 4 . alisolC monoacetate 相似度:75% Phytochemistry 1988 27 1161-1164 Triterpenoids from the rhizome of Alisma plantago-aquatica Geng Pei-Wu,Yoshiyasu Fukuyama,Toshihide Yamada,Wang Rei,Bao Jinxian,Kazuyuki Nakagawa Structure 13C NMR 碳谱模拟图 5 . alisol C monoacetate 相似度:75% Natural Product Research and Development 1996 8(1) 5-9 THE CONSTITUENTS FROM THE RHIZOMA OF ALTSMA ORIENTALIS (SAM) JUZEP. Cai Lining; Wang Hongshu; Cao Hongxing; Zhang Ruyi Structure 13C NMR 碳谱模拟图 6 . alisol B 23-acetate 相似度:75% Natural Product Sciences 2012 18 121-129 Protective Effects of Methanol Extract and Alisol B 23-acetate of Alisma orientale on Acetaminophen-Induced Hepatotoxicity in Rats Yang, Ki-Ho; Choi, Seong-Hee; Park, Jong-Cheol Structure 13C NMR 碳谱模拟图 7 . 11-deoxyalisol C 23-acetate C32H48O5 相似度:71.8% Phytochemistry 1994 36 119-127 Terpenoids of Alisma orientale rhizome and the crude drug alismatis rhizoma Yoshijiro Nakajima, Yohko Satoh, Masumi Katsumata (nee Ohtsuka), Kazuko Tsujiyama (nee Mikoshiba), Yoshiteru Ida, Junzo Shoji Structure 13C NMR 碳谱模拟图 8 . alisol C 23-acetate C32H48O6 相似度:71.8% Biological and Pharmaceutical Bulletin 2012 35 1581-1587 The Rhizomes of Alisma orientale and Alisol Derivatives Inhibit Allergic Response and Experimental Atopic Dermatitis Je Hyeong Lee, Oh Song Kwon, Hong-Guang Jin, Eun-Rhan Woo, Yeong Shik Kim, Hyun Pyo Kim Structure 13C NMR 碳谱模拟图 9 . Alisol C 23-acetate 相似度:71.8% Archives of Pharmacal Research 2012 35 1919-1926 A new triterpenoid from Alisma orientale and their antibacterial effect Hong-Guang Jin, Qinglong Jin, A. Ryun Kim, Hyemin Choi, Je Hyun Lee, Yeong Shik Kim, Dong Gun Lee, Eun-Rhan Woo Structure 13C NMR 碳谱模拟图 10 . alisol C 23-acetate 相似度:68.7% Natural Product Research and Development 2001 13(4) 1-4 TERPENOIDS OF ALISMA ORIENTALIS JUZEP. PENG Guo ping; LOU Feng chang Structure 13C NMR 碳谱模拟图 11 . Alisol C Diacetate C34H50O7 相似度:67.6% Phytochemistry 1994 36 119-127 Terpenoids of Alisma orientale rhizome and the crude drug alismatis rhizoma Yoshijiro Nakajima, Yohko Satoh, Masumi Katsumata (nee Ohtsuka), Kazuko Tsujiyama (nee Mikoshiba), Yoshiteru Ida, Junzo Shoji Structure 13C NMR 碳谱模拟图 12 . alisol L-13-acetate C32H46O5 相似度:65.6% Chemical & Pharmaceutical Bulletin 1999 47 524-528 Studies on Alismatis Rhizoma. III. Stereostructures of New Protostane-Type Triterpenes, Alisols H, I, J-23-Acetate, K-23-Acetate, L-23-Acetate, M-23-Acetate, and N-23-Acetate, from the Dried Rhizome of Alisma orientale Masayuki YOSHIKAWA,Norimichi TOMOHIRO,Toshiyuki MURAKAMI,Akira IKEBATA,Hisashi MATSUDA,Hideaki MATSUDA and Michinori KUBO Structure 13C NMR 碳谱模拟图 13 . alisol B 23-acetate C32H50O5 相似度:65.6% Phytochemistry 1994 36 119-127 Terpenoids of Alisma orientale rhizome and the crude drug alismatis rhizoma Yoshijiro Nakajima, Yohko Satoh, Masumi Katsumata (nee Ohtsuka), Kazuko Tsujiyama (nee Mikoshiba), Yoshiteru Ida, Junzo Shoji Structure 13C NMR 碳谱模拟图 14 . 11-deoxy-alisol C 23-acetate C32H48O5 相似度:65.6% Chinese Traditional and Herbal Drugs 2008 39 1788-1790 泽泻化学成分的研究 胡雪艳;陈海霞;高文远;刘新桥 Structure 13C NMR 碳谱模拟图 15 . alisol B 23-acetate 相似度:65.6% Natural Product Research and Development 2001 13(4) 1-4 TERPENOIDS OF ALISMA ORIENTALIS JUZEP. PENG Guo ping; LOU Feng chang Structure 13C NMR 碳谱模拟图 16 . alisol B monoacetate 相似度:65.6% Natural Product Research and Development 1996 8(1) 5-9 THE CONSTITUENTS FROM THE RHIZOMA OF ALTSMA ORIENTALIS (SAM) JUZEP. Cai Lining; Wang Hongshu; Cao Hongxing; Zhang Ruyi Structure 13C NMR 碳谱模拟图 17 . alisol M 23-acetate 相似度:65.6% Bioorganic & Medicinal Chemistry Letters 2012 22 4787-4792 Triterpenes from Alisma orientalis act as farnesoid X receptor agonists Hsiang-Ru Lin Structure 13C NMR 碳谱模拟图 18 . alisol B 23-acetate C32H50O5 相似度:65.6% Biological and Pharmaceutical Bulletin 2012 35 1581-1587 The Rhizomes of Alisma orientale and Alisol Derivatives Inhibit Allergic Response and Experimental Atopic Dermatitis Je Hyeong Lee, Oh Song Kwon, Hong-Guang Jin, Eun-Rhan Woo, Yeong Shik Kim, Hyun Pyo Kim Structure 13C NMR 碳谱模拟图 19 . Alisol B 23-acetate 相似度:65.6% Archives of Pharmacal Research 2012 35 1919-1926 A new triterpenoid from Alisma orientale and their antibacterial effect Hong-Guang Jin, Qinglong Jin, A. Ryun Kim, Hyemin Choi, Je Hyun Lee, Yeong Shik Kim, Dong Gun Lee, Eun-Rhan Woo Structure 13C NMR 碳谱模拟图 20 . alisol M 23-acetate 相似度:65.6% Bioorganic & Medicinal Chemistry Letters 2014 24 3626-3632 Triterpenes from Alisma orientalis act as androgen receptor agonists,progesterone receptor antagonists, and glucocorticoid receptor antagonists Hsiang-Ru Lin Structure 13C NMR 碳谱模拟图 21 . 2α,3β,23-trihydroxy-urs-12,18-dien-28-oic acid methyl ester 相似度:64.5% Chemical & Pharmaceutical Bulletin 2003 51(2) 200-202 A New Triterpene Glucosyl Ester from the Fruit of the Blackberry (Rubus allegheniensis) Masateru ONO,Michiko TATEISHI, Chikako MASUOKA,Hiromasa KOBAYASHI,Keiji IGOSHI,Haruki KOMATSU,Yasuyuki ITO,Masafumi OKAWA,and Toshihiro NOHARA Structure 13C NMR 碳谱模拟图 22 . alisol O C30H48O5 相似度:64.5% Phytochemistry 2008 69 527-532 Alisolide, alisols O and P from the rhizome of Alisma orientale Ming Zhao Li-Jia Xu Chun-Tao Che Structure 13C NMR 碳谱模拟图 23 . (24R)-24,25-epoxycycloartan-3-one C30H48O2 相似度:64.5% Journal of Natural Products 1996 59 1131-1136 Antimycobacterial Cycloartanes from Borrichia frutescens Charles L. Cantrell, Tiansheng Lu, Frank R. Fronczek, and Nikolaus H. Fischer Structure 13C NMR 碳谱模拟图 24 . alisol G C30H48O4 相似度:64.5% Chemical & Pharmaceutical Bulletin 1993 41 1948-1954 Crude Drugs from Aquatic Plants. I. On the Constituents of Alismatis Rhizoma. (1). Absolute Stereostructures of Alisols E 23-Acetate, F, and G, Three New Protostane-Type Triterpenes from Chinese Alismatis Rhizoma Masayuki YOSHIKAWA,Shoko HATAKEYAMA,Nobumitsu TANAKA,Youichi FUKUDA,Johji YAMAHARA and Nobutoshi MURAKAMI Structure 13C NMR 碳谱模拟图 25 . alisol B monoacetate 相似度:64.5% Chemical & Pharmaceutical Bulletin 1993 41 2109-2112 Crude Drugs from Aquatic Plants. II. On the Constituents of the Rhizome of Alisma orientale JUZEP. Originating from Japan, Taiwan, and China. Absolute Stereostructures of 11-Deoxyalisols B and B 23-Acetate Masayuki YOSHIKAWA,Shoko HATAKEYAMA,Nobumitsu TANAKA,Toshiro MATSUOKA,Johji YAMAHARA and Nobutoshi MURAKAMI Structure 13C NMR 碳谱模拟图 26 . Alisol C C30H46O5 相似度:64.5% Phytochemistry 1994 36 119-127 Terpenoids of Alisma orientale rhizome and the crude drug alismatis rhizoma Yoshijiro Nakajima, Yohko Satoh, Masumi Katsumata (nee Ohtsuka), Kazuko Tsujiyama (nee Mikoshiba), Yoshiteru Ida, Junzo Shoji Structure 13C NMR 碳谱模拟图 27 . 24(S),25-epoxy-5α-protost-20,25-dien-3-one C30H48O2 相似度:64.5% Phytochemistry 2012 76 83-91 Diterpenoids and triterpenoids with potential anti-inflammatory activity from the leaves of Aglaia odorata Orapun Yodsaoue,Jarinthon Sonprasit,Chatchanok Karalai,Chanita Ponglimanont,Supinya Tewtrakul,Suchada Chantrapromma Structure 13C NMR 碳谱模拟图 28 . alisol C 相似度:64.5% Natural Product Research and Development 2001 13(4) 1-4 TERPENOIDS OF ALISMA ORIENTALIS JUZEP. PENG Guo ping; LOU Feng chang Structure 13C NMR 碳谱模拟图 29 . halipeptin C C29H50N4O6S 相似度:64.5% Chemistry-A European Journal 2006 12 6572-6584 Asymmetric Total Syntheses of Marine Cyclic Depsipeptide Halipeptins A–D Shouyun Yu, Xianhua Pan and Dawei Ma Structure 13C NMR 碳谱模拟图 30 . compound 13 相似度:64.5% Journal of Agricultural and Food Chemistry 2003 51 2949-2957 Isolation, Structural Elucidation, and Inhibitory Effects of Terpenoid and Lipid Constituents from Sunflower Pollen on Epstein−Barr Virus Early Antigen Induced by Tumor Promoter, TPA Motohiko Ukiya, Toshihiro Akihisa, Harukuni Tokuda, Kazuo Koike, Junko Takayasu, Hiroki Okuda, Yumiko Kimura, Tamotsu Nikaido, and Hoyoku Nishino Structure 13C NMR 碳谱模拟图 31 . compound 14 相似度:64.5% Journal of Agricultural and Food Chemistry 2003 51 2949-2957 Isolation, Structural Elucidation, and Inhibitory Effects of Terpenoid and Lipid Constituents from Sunflower Pollen on Epstein−Barr Virus Early Antigen Induced by Tumor Promoter, TPA Motohiko Ukiya, Toshihiro Akihisa, Harukuni Tokuda, Kazuo Koike, Junko Takayasu, Hiroki Okuda, Yumiko Kimura, Tamotsu Nikaido, and Hoyoku Nishino Structure 13C NMR 碳谱模拟图 32 . alisol G 相似度:64.5% Chinese Traditional and Herbal Drugs 2012 43 841-843 A new triterpene in rhizome of Alisma orientale XU Nan; ZHANG Hong-da; XIE Xue Structure 13C NMR 碳谱模拟图 33 . 3β-methoxycycloartan-24(241)-ene C32H54O2 相似度:62.5% Journal of Natural Products 2002 65 79-81 Lanostanoids of Amentotaxus formosana Huey-Jen Su, Shiow-Hwa Day, Sheng-Zehn Yang,Michael Y.Chiang,and Chun-Nan Lin Structure 13C NMR 碳谱模拟图 34 . alisol B monoacetate 相似度:62.5% Planta Medica 1988 54 445-447 li-Deoxyalisol C and Alisol D: New Protostane-Type Triterpenoids from Alisma plantago-aquatica Yoshiaysu Fukuyama, Geng Pei-Wu, Wang Rei, Toshihide Yamada, and Kazuyuki Nakagawa Structure 13C NMR 碳谱模拟图 35 . 13β,17β-epoxyalisol B 23-acetate C32H50O6 相似度:62.5% Phytochemistry 1994 36 119-127 Terpenoids of Alisma orientale rhizome and the crude drug alismatis rhizoma Yoshijiro Nakajima, Yohko Satoh, Masumi Katsumata (nee Ohtsuka), Kazuko Tsujiyama (nee Mikoshiba), Yoshiteru Ida, Junzo Shoji Structure 13C NMR 碳谱模拟图 36 . alisol B monoacetate 相似度:62.5% Phytochemistry 1988 27 1161-1164 Triterpenoids from the rhizome of Alisma plantago-aquatica Geng Pei-Wu,Yoshiyasu Fukuyama,Toshihide Yamada,Wang Rei,Bao Jinxian,Kazuyuki Nakagawa Structure 13C NMR 碳谱模拟图 37 . alisol E 23-acetate 相似度:62.5% Natural Product Research and Development 2002 14(2) 7-10 A NEW BISCHROMAN FROM SIEGESBECKIA PUBESCENS XIONG Jiang XU Yun-long Structure 13C NMR 碳谱模拟图 38 . 13β,17β-epoxyalisol B 23-acetate 相似度:62.5% Archives of Pharmacal Research 2012 35 1919-1926 A new triterpenoid from Alisma orientale and their antibacterial effect Hong-Guang Jin, Qinglong Jin, A. Ryun Kim, Hyemin Choi, Je Hyun Lee, Yeong Shik Kim, Dong Gun Lee, Eun-Rhan Woo Structure 13C NMR 碳谱模拟图 39 . dihydroschizandronic acid 相似度:61.2% Journal of Natural Products 2003 66 263-268 Natural Anti-HIV Agents. Part IV. Anti-HIV Constituents from Vatica cinerea Hong-Jie Zhang, Ghee Teng Tan, Vu Dinh Hoang, Nguyen Van Hung, Nguyen Manh Cuong, D. Doel Soejarto, John M. Pezzuto, and Harry H. S. Fong Structure 13C NMR 碳谱模拟图 |
5楼2014-12-07 00:15:07