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杨大松至尊木虫 (文坛精英)
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[求助]
求助微谱数据，谢谢
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碳谱数据如下： 57.0,57.1,62.6,63.5,71.4,75.7,76.0,77.8,78.3,78.3,105.4,105.5,105.6,114.9,130.1,131.3,135.3,136.0,141.6,142.0,154.2,154.4 辛苦各位了，谢谢。 |
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二氯甲烷
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【答案】应助回帖
★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★
感谢参与，应助指数 +1
杨大松: 金币+17, ★★★★★最佳答案 2012-07-10 16:56:35
感谢参与，应助指数 +1
杨大松: 金币+17, ★★★★★最佳答案 2012-07-10 16:56:35
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1 . syringin 相似度:77.2% Acta Pharmaceutica Sinica 2006 Vol 41 738-741 Water-soluble phenolic glycosides from the whole plant of Bulbophyllum odoratissimum LIU Dai-lin; PANG Fa-gen; ZHANG Xue; GAO Hao; WANG Nai-li; YAO Xin-sheng Structure 13C NMR 碳谱模拟图 2 . xylocoside D C23H32O11 相似度:72.7% Helvetica Chimica Acta 2008 Vol. 91 1346 Xylocosides A–G, Phenolic Glucosides from the Stems of Xylosma controversum Zheng-Ren Xu, Xing-Yun Chai, Chang-Cai Bai, Hong-Yan Ren, Ya-Nan Lu, Hai-Ming Shi, and Peng-Fei Tu Structure 13C NMR 碳谱模拟图 3 . isosyringinoside 相似度:72.7% Phytochemistry 1993 33 1215-1219 Lignan and phenylpropanoid glycosides from Osmanthus asiaticus Masataka Sugiyama, Eiko Nagayama, Masao Kikuchi Structure 13C NMR 碳谱模拟图 4 . (-)-(2R-)-1-O-β-D-glucopyranosyl-2-{2,6-dimethoxy-4-[1-(E)-propen-3-ol]phenoxyl}propane-3-ol 相似度:72.7% China Journal of Chinese Materia Medica 2010 35 456-467 Constituents from a water-soluble portion of ethanolic extract of Iodes cirrhosa GAN Maoluo; ZHU Chenggen; ZHANG Yanling; ZI Jiachen; SONG Weixia; YANG Yongchun; SHI Jiangong Structure 13C NMR 碳谱模拟图 5 . syringin 相似度:72.7% Chinese Traditional and Herbal Drugs 1998 29 586-587 刺人参的化学成分研究(Ⅱ) 许颂,梁华清 Structure 13C NMR 碳谱模拟图 6 . syringin 相似度:72.7% Journal of Shenyang Pharmaceutical University 2002 19 183-185 Glycosides from Glehnia littoralis YUAN Zhong, ZHOU Bi-ye, ZHANG Zi-cheng, KADOTA Shigetoshi, LI Xian Structure 13C NMR 碳谱模拟图 7 . 3-hydroxy-1-(4-hydroxy-3,5-dimethoxyphenyl)-2-[4-(3-hydroxy-1-(E)-propenyl)-2,6-dimethoxyphenoxy]propyl-β-D-glucopyranoside 相似度:72.7% Bioscience, Biotechnology, and Biochemistry 2003 66 29-35 New Antioxidative Phenolic Glycosides Isolated from Kokuto Non-centrifuged Cane Sugar Kensaku TAKARA, Daigo MATSUI, Koji WADA, Toshio ICHIBA and Yoko NAKASONE Structure 13C NMR 碳谱模拟图 8 . Oplopanpheside C C23H32O13 相似度:69.5% Chemical & Pharmaceutical Bulletin 2011 59(5) 676-679 Oplopanphesides A—C, Three New Phenolic Glycosides from the Root Barks of Oplopanax horridus Wei-Hua HUANG, Qing-Wen ZHANG, Lan-Zhen MENG, Chun-Su YUAN, Chong-Zhi WANG, and Shao-Ping LI Structure 13C NMR 碳谱模拟图 9 . 2,6-Dimethoxy-4-(3-hydroxy-propen-1-yl)phenyl-4-O-α-L-rhamnopyranosyl-(1→6)-β-D-glucopyranoside C23H34O13 相似度:69.5% Zeitschrift für Naturforschung B 2007 62b 854-858 Chemical Constituents from the Roots and Rhizomes of Clematis hexapetala Pall. Cai-xia Dong, She-po Shi, Ke-siWu, and Peng-fei Tu Structure 13C NMR 碳谱模拟图 10 . (7R,8R)-threo-Guaiacylglycerol-8-O-4'-sinapyl ether 7-O-β-D-glucopyranoside C27H36O13 相似度:69.2% Journal of Natural Medicines 2009 63 227-231 Two new neolignan glycosides from leaves of Osmanthus heterophyllus Koichi Machida, Shigeaki Sakamoto and Masao Kikuchi Structure 13C NMR 碳谱模拟图 11 . Syringin C17H24O9 相似度:68.1% Acta Botanica Yunnanica 2000 22(2) 214-218 The Chemical Constituents from Toricellia angulata WU Shao-Hua,MA Yun-Bao,LUO Xiao-Dong,WU Da-Gang,LIU Ji-Kai Structure 13C NMR 碳谱模拟图 12 . Syringin C17H24O9 相似度:68.1% Acta Botanica Yunnanica 1997 19(1) 92-96 STUDY ON CHEMICAL CONSTITUENTS OF SAUSSUREA LAPPA Ⅱ Yang Hui, Xie J inlun, Sun Handong Structure 13C NMR 碳谱模拟图 13 . Tinoscorside D C22H32O13 相似度:68.1% Fitoterapia 2010 81 485-489 Aporphine alkaloids, clerodane diterpenes, and other constituents from Tinospora cordifolia Phan Van Kiem, Chau Van Minh, Nguyen Tien Dat, La Van Kinh, Dan Thuy Hang, Nguyen Hoai Nam, Nguyen Xuan Cuong, Hoang Thanh Huong, Trinh Van Lau Structure 13C NMR 碳谱模拟图 14 . Sinapyl alcohol 1,3'-di-O-β-D-glucopyranoside 相似度:68.1% Pharmazie 2002 57 209-211 Two new steroids from Adenophora stenanthina subsp. xifengensis Zhen-Fu Hou - Yong-Qiang Tu - Yu Li Structure 13C NMR 碳谱模拟图 15 . icariol A2-4-O-β-D-glucopyranoside 相似度:68.1% Chinese Pharmaceutical Journal 2010 45 898-902 A New Compound from Dendrobium candidum WANG Fang-fei, LI Yan, DONG Hai-ling, GUO Shun-xing, WANG Chun-lan, YANG Jun-shan Structure 13C NMR 碳谱模拟图 16 . 2-[4-(3-Hydroxy-1-propenyl)-2,6-dimethoxyphenoxy]-3-hydroxy-3-(4-hydroxy-3,5-dimethoxyphenyl)propyl-β-D-glucopyranoside C28H36O14 相似度:68.1% Bioscience, Biotechnology, and Biochemistry 2003 67 376-379 New Phenolic Compounds from Kokuto, Non-centrifuged Cane Sugar Kensaku TAKARA, Daigo MATSUI, Koji WADA, Toshio ICHIBA, Isao CHINEN and Yoko NAKASONE Structure 13C NMR 碳谱模拟图 17 . (7S,8R)-erythro-Guaiacylglycerol-β-O-4'-sinapyl ether 9-O-β-D-glucopyranoside C27H36O13 相似度:66.6% Magnetic Resonance in Chemistry 2008 46 990-994 Structure elucidation and NMR spectral assignments of four neolignan glycosides with enantiometric aglycones from Osmanthus ilicifolius (pages 990–994) Koichi Machida, Shigeaki Sakamoto and Masao Kikuchi Structure 13C NMR 碳谱模拟图 18 . (7R,8S)-erythro-Guaiacylglycerol-β-O-4'-sinapyl ether 9-O-β-D-glucopyranoside C27H36O13 相似度:66.6% Magnetic Resonance in Chemistry 2008 46 990-994 Structure elucidation and NMR spectral assignments of four neolignan glycosides with enantiometric aglycones from Osmanthus ilicifolius (pages 990–994) Koichi Machida, Shigeaki Sakamoto and Masao Kikuchi Structure 13C NMR 碳谱模拟图 19 . 3-hydroxy-1-(4-hydroxy-3-methoxyphenyl)-2-[4-(3-hydroxy-1-(E)-propenyl)-2,6-dimethoxyphenoxy]propyl-β-D-glucopyranoside 相似度:66.6% Bioscience, Biotechnology, and Biochemistry 2003 66 29-35 New Antioxidative Phenolic Glycosides Isolated from Kokuto Non-centrifuged Cane Sugar Kensaku TAKARA, Daigo MATSUI, Koji WADA, Toshio ICHIBA and Yoko NAKASONE Structure 13C NMR 碳谱模拟图 20 . picraquassioside C 相似度:65.3% China Journal of Chinese Materia Medica 2008 33 269-272 Chemical constituents in roots of Hemerocallis fulva YANG Zhongduo, LI Tao, LI Yuanchao Structure 13C NMR 碳谱模拟图 21 . Picraquassioside C C28H38O14 相似度:65.3% Phytochemistry 1995 40 253-256 Phenylpropanoids and other secondary metabolites from fresh fruits of Picrasma quassioides Kazuko Yoshikawa, Saori Sugawara, Shigenobu Arihara Structure 13C NMR 碳谱模拟图 22 . salvadoraside C34H48O8 相似度:64% Phytochemistry 1992 31 2469-2471 Lignan glycosides from stems of Salvadora persica K. Ohtani, R. Kasai, K. Yamasaki, O. Tanaka, M.S. Kamel, M.H. Assaf, M.A. El-Shanawani, A.A. Ali Structure 13C NMR 碳谱模拟图 23 . syringinoside C23H34O14 相似度:63.6% Chemical & Pharmaceutical Bulletin 1991 39 2440-2442 Phenolic Glycosides from Roots of Adenophora tetraphylla Collected in Heilongjiang, China Hai-Xue KUANG,Chun-Jie SHAO,Ryoji KASAI,Kazuhiro OHTANI,Zhen-Kun TIAN,Jing-Da XU and Osamu TANAKA Structure 13C NMR 碳谱模拟图 24 . methylsyringin C18H26O4 相似度:63.6% Chemical & Pharmaceutical Bulletin 1998 46 1587-1590 Water-Soluble Constituents of Fennel. V. Glycosides of Aromatic Compounds Junichi KITAJIMA,Toru ISHIKAWA,Yasuko TANAKA,Masateru ONO,Yasuyuki ITO and Toshihiro NOHARA Structure 13C NMR 碳谱模拟图 25 . 3-(4-acetoxy-3,5-dimethoxy)-phenyl-2E-propenyl-β-D-glucopyranoside C19H26O10 相似度:63.6% Chemical & Pharmaceutical Bulletin 2010 58 980-982 Characterization and Antiglycation Activity of Phenolic Constituents from Viscum album (European Mistletoe) M. Iqbal Choudhary, Saima Maher, Afshan Begum, Ahmed Abbaskhan, Sajjad Ali, Ambreen Khan, Shafique-ur-Rehman and Atta-ur-Rahman Structure 13C NMR 碳谱模拟图 26 . syringaresinol-4'-O-β-D-glucopyranoside C28H36O13 相似度:63.6% Journal of China Pharmaceutical University 2006 37 487-490 Chemical constituents from Asparagus filicinus WU Jia-jun; WANG Hao; YE Wen-cai; ZUO Xiao-feng; ZHAO Shou-xun Structure 13C NMR 碳谱模拟图 27 . (3Z)-5-[2-(β-D-glucopyranosyl)oxy-5-hydroxy-3-methoxyphenyl]-5-(4-hydroxyphenyl)-penta-1,3-diene C24H28O9 相似度:63.6% Journal of Natural Medicines 2011 65 224-228 Phenolic glycosides from Rhodohypoxis baurii Yukiko Matsuo ,Fumito Tachikawa ,Yoshihiro Mimaki Structure 13C NMR 碳谱模拟图 28 . salvadoraside 相似度:62.9% Phytochemistry 1997 45 159-166 Lignan, phenylpropanoid and iridoid glycosides from Pedicularis torta Wang Changzeng, Jia Zhongjian Structure 13C NMR 碳谱模拟图 29 . foliachinenosides C C28H38O14 相似度:61.5% Heterocycles 2008 75 1435-1446 New Phenolic Glycosides from the Leaves of Salacia chinensis Seikou Nakamura, Yi Zhang, Tao Wang, Hisashi Matsuda, and Masayuki Yoshikawa Structure 13C NMR 碳谱模拟图 30 . (7S,8R)-5-Methoxydehydrodiconiferyl alcohol 4-O-β-D-glucopyranoside C27H34O12 相似度:61.5% Journal of Natural Medicines 2009 63 227-231 Two new neolignan glycosides from leaves of Osmanthus heterophyllus Koichi Machida, Shigeaki Sakamoto and Masao Kikuchi Structure 13C NMR 碳谱模拟图 31 . 2,6-dimethoxy-4[(1E)-prop-1-enyl]phenyl O-α-L-rhamnopyranosyl-(1→6)-β-D-glucopyranoside C23H34O12 相似度:59.0% Helvetica Chimica Acta 2006 Vol. 89 884 Study on the Chemical Constituents of Daphniphyllum angustifolium Haiyun Bai and Lihong Hu Structure 13C NMR 碳谱模拟图 32 . syringin C17H24O9 相似度:59.0% Acta Botanica Yunnanica 2001 23(3) 352-356 The Chemical Constituents of Parakmeria yunnanensis CHENG Yong-Xian,ZHOU Jun, TAN Ning-Hua Structure 13C NMR 碳谱模拟图 33 . moellenoside A C25H30O12 相似度:59.0% Chinese Chemical Letters 2008 19 76-78 Two new coumarin glucosides biosynthesized by transgenic hairy roots of Polygonum multiflorum Rong Min Yu , Liang Bin Zhou , Chun Yan Yan, Guo Yan Duan, Yu Zhao Structure 13C NMR 碳谱模拟图 34 . erythro-guaiacylglycerol-β-O-4'-sinapyl ether 相似度:59.0% China Journal of Chinese Materia Medica 2009 34 1225-1227 Lignans from stems of Sambucus williamsii OUY ANG Fu, LIU Yuan, XI AO Huihui, YU Haiyang, WANG Naili, YAO Xinsheng Structure 13C NMR 碳谱模拟图 35 . (+)-syringaresinol-O-β-D-glucopyranoside C28H36O13 相似度:59.0% China Journal of Chinese Materia Medica 2000 25 728-730 Studies on Chemical Costituents of Cistanche tubulosa (Schenk)R. Wight SONG Zhihong, MO Shaohong, CHEN Yan, TU Pengfei, ZHAO Yuying, ZHENG Junhua Structure 13C NMR 碳谱模拟图 36 . syringinoside 相似度:59.0% Chemical & Pharmaceutical Bulletin 1999 47 114-115 Phenylpropanoid Glycosides from Daphne oleoides Nisar ULLAH,Saeed AHMAD and Abdul MALIK Structure 13C NMR 碳谱模拟图 37 . syringaresinol-4'-O-D-monoglucopyranoside C28H36O13 相似度:59.0% Phytochemistry 1998 48 711-717 Lignan and acetylenic glycosides from Aster auriculatus Chang Zeng Wang, De Quan Yu Structure 13C NMR 碳谱模拟图 38 . syringaresinol mono-β-D-glucoside 相似度:59.0% Acta Pharmaceutica Sinica 2008 Vol 43 284-290 Phenolic glucosides from the leaves of Pieris japonica YAO Guang-min; WANG Yu-bo; WANG Li-quan; QIN Guo-wei Structure 13C NMR 碳谱模拟图 |
2楼2012-07-10 13:08:33
gyp1271985
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3楼2012-07-10 15:36:20
杨大松
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4楼2012-07-10 16:57:04