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Microstructural Analysis: Tools and Techniques
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During recent years, people involved in developing new metals
and materials for use in some of the rather extreme conditions of
stress, temperature, and environment have relied heavily on the
microstructural condition of their materials. In fact, many of
the newer materials, such as dispersion-strengthened alloys, have
been designed almost entirely by first determining the microstructure
desired and then finding the right combination of composition,
heat treatment, and mechanical working that will result in the desired
microstructure. Furthermore, the extremely high reliability
required of materials used today, for example, in aerospace and
nuclear energy systems, requires close control on the microstructural
conditions of materials. This is clearly evident from even
a cursory examination of recently written specifications for materials
where rather precise microstructural parameters are stipulated.
Whereas specifications written several years ago may have
included microstructural requirements for details such as ASTM
grain size or graphite type, today\'s specifications are beginning
to include such things as volume fraction of phases, mean free path
of particles, and grain intercept distances. Rather arbitrary
terms such as "medium pearlite" have been replaced by requirements
such as "interlamella spacing not to exceed 0.1 micron."
Finally, materials users have become increasingly aware that
when a material does fail, the reason for its failure may be found
by examining and "reading" its microstructure. The responsibility
for a particular microstructure and a resulting failure is a
matter of growing importance in current product liability considerations.
Ŀ¼:
Table of contents :
Content:
Front Matter....Pages i-viii
Photographic Techniques for Optical Microscopy and Macroscopy....Pages 1-22
Specimen Preparation Methods for Microstructural Analysis....Pages 23-34
Quantitative Stereology for Microstructural Analysis....Pages 35-66
Devices for Quantitative Analysis....Pages 67-91
Scanning Electron Microscopy for Microstructural Analysis....Pages 93-124
High Voltage Electron Microscopy for Microstructural Analysis....Pages 125-152
Microstructural Analysis and Fractography....Pages 153-168
X-Ray Diffraction Microscopy....Pages 169-219
Computers in Microstructural Analysis....Pages 221-239
Use of Leed, Auger Emission Spectroscopy and Field Ion Microscopy in Microstructural Studies....Pages 241-279
Microstructural Studies Using the Electron Microprobe Analyzer....Pages 281-285
Ion Probe Mass Spectrometry Analysis of Microstructures....Pages 287-313
Ion Scattering Spectroscopy for Microstructural Analysis....Pages 315-329
Back Matter....Pages 331-343
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