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huadong1227木虫 (小有名气)
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[求助]
LY-21-1 微谱数据求助 已有1人参与
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MEOD溶，13C-NMR如下： 16.26,18.00,18.13,18.71,19.89,21.97,27.27,30.90,31.69, 32.79,33.42,36.15,38.24,38.64,39.69,47.46,52.32,58.00, 62.07,69.24,69.94,70.60,72.30,72.53,72.57,73.07,73.10, 74.00,74.09,76.84,78.13,79.43,79.64,81.00,100.64,102.51, 102.78,103.34,22.60,125.74,142.46,156.53,199.55 |
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木虫 (正式写手)
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huadong1227: 金币+5, ★有帮助 2014-11-10 15:33:58
感谢参与，应助指数 +1
huadong1227: 金币+5, ★有帮助 2014-11-10 15:33:58
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???????????鵽1610????????(???????????ο?) 1 . pregna-5,16-diene-3b-ol-20-one 3-O-??-L-rhamnopyranosyl-(1??2)-[??-L-rhamnopyranosyl-(1??4)]-??-L-rhamnopyranosyl-(1??2)-??-D-glucopyranoside C45H70O19 ?????:91.1% Magnetic Resonance in Chemistry 2012 50 813-817 Steroidal saponins and pregnane glycosides from Smilax microphylla Tao Lin, Hui-Lian Huang, Rong-Hua Liu, Ji-Cheng Shu, Gang Ren, Feng Shao and Li-sha Liu Structure 13C NMR ??????? 2 . hypoglaucin H ?????:86.0% China Journal of Chinese Materia Medica 2014 39 2034-2038 Chemical constituents from Solanum rostratum HAO Li-juan, WANG Shan, ZHU Jing-jing, WANG Zhi-min, WEI Shou-hui Structure 13C NMR ??????? 3 . (3??-dihydroxy pregn-5,16-dien-20-one 3-O-??-chacotrioside ?????:83.7% Phytochemistry 1999 50 481-484 Steroidal saponins from Asparagus dumosus Viqar Uddin Ahmad, Syed Muhammad Khaliq-uz-Zaman, Simin Shameel, Shaista Perveen, Zulfiqar Ali Structure 13C NMR ??????? 4 . 1-O-??-D-glucopyranosyl-22-O-methyl-(25R)-furost-5(6)-en-1??,3??,22??,26-tetraol-26-O-??-L-rhamnopyranosyl-(1'''??6'')-O-??-D-galactopyranoside ?????:82.6% Food Chemistry 2005 93 205-214 Furostanol saponins in Allium caepa L. Var. tropeana seeds Irene Dini, Gian Carlo Tenore, Elena Trimarco, Antonio Dini Structure 13C NMR ??????? 5 . 3-O-[bis-??-L-rhamnopyranosyl-(1??4 and 1??2)??-D-glucopyranosyl]-(25R)-furosta-5,2O-dien-3??,26-diol ?????:82.2% Planta Medica 1988 54 344-346 Oligofurostanosides from Asparagus cochinchinensis Zhou Zhong Liang, Rita Aquino, Francesco De Simone, Antonio Dini, Oreste Schettino, and Cosimo Pizza Structure 13C NMR ??????? 6 . 1-O-??-D-glucopyranosyl-(25R)-fur-ost-5(6)-en-1??,3??,22??,26-tetraol-26-O-??-L-rhamnopyranosyl-(1'''??6'')-O-??-D-galactopyranoside ?????:82.2% Food Chemistry 2005 93 205-214 Furostanol saponins in Allium caepa L. Var. tropeana seeds Irene Dini, Gian Carlo Tenore, Elena Trimarco, Antonio Dini Structure 13C NMR ??????? 7 . solamargine C45H73NO15 ?????:81.8% Bioorganic & Medicinal Chemistry Letters 2011 21 2930-2933 Total synthesis of solamargine Guohua Wei, Jing Wang, Yuguo Du Structure 13C NMR ??????? 8 . (25R)-26-O-??-D-glucopyranosyl-22??-methoxy-furost-5-ene-1??,3??,26-triol 1-O-[??-L-rhamnopyranosyl-(1??2)-6-O-acetyl??-D-glucopyranoside and ?????:80.4% Phytochemistry 2011 72 651-661 Steroidal glycosides from Ruscus ponticus Assunta Napolitano, Tamar Muzashvili, Angela Perrone, Cosimo Pizza, Ether Kemertelidze, Sonia Piacente Structure 13C NMR ??????? 9 . ??-solamarine ?????:80% Phytochemistry 2002 59 79-84 Bioactive steroidal alkaloid glycosides from Solanum aculeastrum Alphonse W. Wanyonyi, Sumesh C. Chhabra, Gerald Mkoji, Udo Eilert,Wilson M. Njue Structure 13C NMR ??????? 10 . solamargine ?????:80% Phytochemistry 2002 59 79-84 Bioactive steroidal alkaloid glycosides from Solanum aculeastrum Alphonse W. Wanyonyi, Sumesh C. Chhabra, Gerald Mkoji, Udo Eilert,Wilson M. Njue Structure 13C NMR ??????? 11 . dioscin ?????:80% Natural Product Research 2003 17 287-292 A New Steroidal Saponin from Dioscorea Zingiberensis Wright Wenji Sun; Guangzhong Tu; Yongmin Zhang Structure 13C NMR ??????? 12 . dioscin ?????:80% Natural Product Research 2003 17 287-292 A New Steroidal Saponin from Dioscorea Zingiberensis Wright Wenji Sun; Guangzhong Tu; Yongmin Zhang Structure 13C NMR ??????? 13 . tribol ?????:80% Fitoterapia 2004 75 117-122 Anovel furostanol saponin from Tribulus terrestris of Bulgarian origin J. Conrad , D. Dinchev , I. Klaiber , S. Mika , I. Kostova,W. Kraus Structure 13C NMR ??????? 14 . dioscoreanoside C C45H72O19 ?????:80% Phytochemistry 2013 95 341-350 Steroidal saponins from the flowers of Dioscorea bulbifera var. sativa L??on Azefack Tapondjou, Kristina Jenett-Siems, Stefan Böttger, Matthias F. Melzig Structure 13C NMR ??????? 15 . dioscoreanoside E C45H72O19 ?????:80% Phytochemistry 2013 95 341-350 Steroidal saponins from the flowers of Dioscorea bulbifera var. sativa L??on Azefack Tapondjou, Kristina Jenett-Siems, Stefan Böttger, Matthias F. Melzig Structure 13C NMR ??????? 16 . 1-O-??-D-glucopyranosyl-(25R)-furost-5(6)-en-1??,3??,22??,26-tetraol-26-O-??-L-rhamnopyranosyl-(1'''??2'')-O-??-L-arabinopyranoside ?????:79.5% Food Chemistry 2005 93 205-214 Furostanol saponins in Allium caepa L. Var. tropeana seeds Irene Dini, Gian Carlo Tenore, Elena Trimarco, Antonio Dini Structure 13C NMR ??????? 17 . 1-O-??-D-glucopyranosyl-(25R)-furost-5(6)-en-1??,3??,22??,26-tetraol-26-O-??-L-rhamnopyranosyl-(1'''??2'')-O-??-L-arabinopyranoside ?????:79.5% Food Chemistry 2005 93 205-214 Furostanol saponins in Allium caepa L. Var. tropeana seeds Irene Dini, Gian Carlo Tenore, Elena Trimarco, Antonio Dini Structure 13C NMR ??????? 18 . (25R)-26-O-??-D-glucopyranosyl-furost-5-ene-3??,22??,26-triol 3-O-[??-L-arabinopyranosyl-(1??4)-O-??-D-glucopyranoside] ?????:79.5% Phytochemistry 2011 72 651-661 Steroidal glycosides from Ruscus ponticus Assunta Napolitano, Tamar Muzashvili, Angela Perrone, Cosimo Pizza, Ether Kemertelidze, Sonia Piacente Structure 13C NMR ??????? 19 . ???????? ?????:79.0% Chinese Traditional and Herbal Drugs 2001 32 18,38 ????ε???????о? ???,????,???,???????,????? Structure 13C NMR ??????? 20 . 1-O-[??-L-rhamnopyranosyl-(1)-6-O-acetyl-??-D-galactopyranosyl]-1??,3??,22??-26-tetrahydroxyfurost-5(6)-ene-26-O-??-D-glucopyranoside ?????:78.7% Chemistry of Natural Compounds 2009 45 756-758 Analysis and isolation of saponins from Limoniastrum feei by LC-UV N. Belboukhari, A. Cheriti Structure 13C NMR ??????? 21 . (25R,26R)-3??,17??-dihydroxy-26-methoxyspirostan-5-ene-3??-O-??-L-rhamnopyranosyl-(1??2)-[??-D-glucopyranosyl-(1??6)]-??-D-glucopyranoside C47H76O18 ?????:78.2% Chinese Traditional and Herbal Drugs 2011 42 21-24 Steroidal saponins and phenylic constituents from Lilium lancifolium and their anti-oxidant activities ZHOU Zhong-liu, SHI Ren-bing, LIU Bin, ZOU Jie-ming, YIN Wen-qing, XIA Jing-min Structure 13C NMR ??????? 22 . (23S,25R)-23-hydroxyspirost-5-en-3??-yl O-??-L-rhamnopyranosyl-(1??2)-O-[??-D-glucopyranosyl-(1??6)]-??-D-glucopyranoside C45H72O18 ?????:77.7% Phytochemistry 1999 51 567-573 Steroidal saponins from the bulbs of Lilium candidum Yoshihiro Mimaki, Tadaaki Satou, Minpei Kuroda, Yutaka Sashida, Yoshio Hatakeyama Structure 13C NMR ??????? 23 . asparasaponin II ?????:77.7% Chinese Traditional and Herbal Drugs 1999 30(12) 888-890 Studies on the Chemical Constituents of Commmon Asparagus Bark (Asparagus officinalis) Sun Jianhua; Zuo Chunxu; Yang Shangjun Structure 13C NMR ??????? 24 . compound 5 C45H72O ?????:77.7% Zeitschrift f??r Naturforschung C 2002 57 33-38 Two New Sulfated Furostanol Saponins from Tribulus terrestris I. Kostova, D. Dinchev, G. Hopp Rentsch, V. Dimitrov, and A. Ivanova Structure 13C NMR ??????? 25 . 1-O-??-D-glucopyranosyl-22-O-methyl-(25R)-furost-5(6)-en-1??,3??,22??,26-tetraol-26-O-??-L-rhamnopyranosyl-(1'''??2'')-O-??-L-arabinopyranoside ?????:77.7% Food Chemistry 2005 93 205-214 Furostanol saponins in Allium caepa L. Var. tropeana seeds Irene Dini, Gian Carlo Tenore, Elena Trimarco, Antonio Dini Structure 13C NMR ??????? 26 . hauptsaponine S2 ?????:77.7% Pharmazie 1987 42 143-143 Steroidsaponine aus Dioscorea hispida L. Ng. X. Cuong, D. Zeigan, Gabriele Voigt, und K. Hiller Structure 13C NMR ??????? 27 . ascalonicoside A1 C45H74O19 ?????:77.7% Journal of Agricultural and Food Chemistry 2002 50 5686-5690 Chemical Composition of Shallot (Allium ascalonicum Hort.) Ernesto Fattorusso, Maria Iorizzi, Virginia Lanzotti, and Orazio Taglialatela-Scafati Structure 13C NMR ??????? 28 . ascalonicoside A2 C45H74O19 ?????:77.7% Journal of Agricultural and Food Chemistry 2002 50 5686-5690 Chemical Composition of Shallot (Allium ascalonicum Hort.) Ernesto Fattorusso, Maria Iorizzi, Virginia Lanzotti, and Orazio Taglialatela-Scafati Structure 13C NMR ??????? 29 . (3??,5??,6??)-5,6-dihydroxysolanidan-3-yl 6-deoxy-??-l-mannopyranosyl-(1??2)-[6-deoxy-??-l-mannopyranosyl-(1??4)]-??-D-glucopyranoside C45H75NO16 ?????:77.7% Helvetica Chimica Acta 2013 96 931-940 Five New Steroidal Alkaloid Glycosides from Solanum tuberosum Zhi-Qiang Zhang, Jian-Guang Luo, Jun-Song Wang and Ling-Yi Kong Structure 13C NMR ??????? 30 . dioscin ?????:77.7% China Journal of Chinese Materia Medica 2014 39 2034-2038 Chemical constituents from Solanum rostratum HAO Li-juan, WANG Shan, ZHU Jing-jing, WANG Zhi-min, WEI Shou-hui Structure 13C NMR ??????? 31 . (23S,25R)-spirost-5-en-3,23-diol 3-O-??-L-rhamnopyranosyl-(1??2)-O-[??-L-rhamnopyranosyl-(1??4)]-??-D-glucopyranoside C45H72O17 ?????:77.7% Records of Natural Products 2015 9 94-104 Chemical Constituents from Solanum glabratum Dunal var. sepicula Essam Abdel-Sattar, Mohamed A Farag and Engy A Mahrous Structure 13C NMR ??????? 32 . (6S,13S)-13-O[??-L-rhamnopyranosyl-(1??4)-??-D-fucopyranosyl]-6-O-[??-D-glucopyranosyl-(1??4)-??-L-rhamnopyranosyl]cleroda-3,14-diene-6,13-diol ?????:77.2% Phytochemistry 1997 46 839-844 Biologically active clerodane-type diterpene glycosides from the root-stalks of Dicranopteris pedata Tadashi Aoki, Tadashi Ohro, Yoshikazu Hiraga, Takayuki Suga, Mihoko Uno, Shinji Ohta Structure 13C NMR ??????? 33 . Solamargine C45H73NO15 ?????:77.2% Fitoterapia 2010 81 767-771 Evaluation of the biological activity of the molluscicidal fraction of Solanum sisymbriifolium against non target organisms Jean-Jacques M. Bagalwa, Laurence Voutquenne-Nazabadioko, Charlotte Sayagh, Augustin S. Bashwira Structure 13C NMR ??????? 34 . ??-solamarine C45H73NO15 ?????:77.2% Fitoterapia 2010 81 767-771 Evaluation of the biological activity of the molluscicidal fraction of Solanum sisymbriifolium against non target organisms Jean-Jacques M. Bagalwa, Laurence Voutquenne-Nazabadioko, Charlotte Sayagh, Augustin S. Bashwira Structure 13C NMR ??????? 35 . (25S)-26-O-??-D-glucopyranoyl-20(22)-en-furost-1??,3??,5??,26-tetraol-1-O-??-D-arabinopyranoside-3-O-??-L-rhamnopyranoside C44H72O19 ?????:77.2% Natural Product Research 2013 27 85-92 Three new steroidal glycosides from roots of Reineckia carnea Qian Wang, Qune Hou, Zhiyong Guo, Kun Zou, Yanhong Xue, Nianyu Huang, Fan Cheng & Yuan Zhou Structure 13C NMR ??????? 36 . 26-O-??-D-glucopyranosyl-furost??-5,25(27)-diene-3??,22??,26-triol 3-O-[??-L-arabinopyranosyl-(1??4)-O-??-D-glucopyranoside] ?????:77.2% Phytochemistry 2011 72 651-661 Steroidal glycosides from Ruscus ponticus Assunta Napolitano, Tamar Muzashvili, Angela Perrone, Cosimo Pizza, Ether Kemertelidze, Sonia Piacente Structure 13C NMR ??????? 37 . (25R)-26-O-??-D-glucopyranosyl-furost??-5,20(22)-diene-3??,26-diol 3-O-[??-L-arabinopyranosyl-(1??4)-O-??-D-glucopyranoside] ?????:77.2% Phytochemistry 2011 72 651-661 Steroidal glycosides from Ruscus ponticus Assunta Napolitano, Tamar Muzashvili, Angela Perrone, Cosimo Pizza, Ether Kemertelidze, Sonia Piacente Structure 13C NMR ??????? 38 . Ceposide A C44H72O18 ?????:77.2% Phytochemistry 2012 74 133-139 Antifungal saponins from bulbs of white onion, Allium cepa L. Virginia Lanzotti, Adriana Romano, Stefania Lanzuise, Giuliano Bonanomi, Felice Scala Structure 13C NMR ??????? 39 . digitoxigenin 3-O-[O-??-D-glucopyranosyl-(1??6)-O-??-D-glucopyranosyl-(1??4)-2-O-acetyl-??-D-digitalopyranoside] C44H69O19 ?????:77.2% Phytochemistry 2013 88 105-111 Cardenolide glycosides from root of Streptocaulon juventas Rui Xue, Na Han, Chun Ye, Hai-bo Wang, Jun Yin Structure 13C NMR ??????? 40 . 3-O-[??-L-rhamnopyranosyl-(1??2)-??-Dgalactopyranosyl-(1??2)-??-D-glucuronopyranosyl]-3??,16??,22??-trihydroxy-olean-12-ene C48H78O18 ?????:77.0% Journal of Natural Products 2007 70 979-983 Oleanane Saponins from Stylosanthes erecta Marinella De Leo,Rokia Sanogo, Nunziatina De Tommasi, and Alessandra Braca Structure 13C NMR ??????? 41 . incanumine C49H79NO19 ?????:77.0% Journal of Natural Products 1990 Vol 53 513 The Cytotoxic Principles of Solanum incanum Chun-Nan Lin, Chai-Ming Lu, Ming-Kung Cheng, Kim-Hong Gan, Shen-Jeu Won Structure 13C NMR ??????? 42 . ent-14-labden-8??-ol 13??-O-[??-D-quinovopyranosyl-(1??2)-3'-O-acetyl-??-L-rhamnopyranosyl]-19-O-??-L-rhamnopyranoside C40H68O16 ?????:76.7% Journal of Natural Products 2007 70 1837-1845 Diterpenoid Glycosides from the Bitter Fern Gleichenia quadripartita Cecilia Socolsky,Yoshinori Asakawa,and Alicia Bard??n Structure 13C NMR ??????? 43 . macrophyllosaponin C C42H72O14 ?????:76.7% Journal of Natural Products 1996 59 1019-1023 Four Novel Cycloartane Glycosides from Astragalus oleifolius I??hsan Çalış, Murat Zor, İclal Saracoğlu, Aşkın Işımer, and Heinz R??egger Structure 13C NMR ??????? 44 . 26-O-??-D-glucopyranosyl-22-O-methylfurosta-5,25(27)-diene-1??,3??,22??,26-tetrol 1-O-{O-??-L-rhamnopyranosyl-(1??2)-3-O-acetyl-4-O-sulfo-??-L-arabinipyranoside} ?????:76.5% Chemical & Pharmaceutical Bulletin 1998 46 298-303 New Steroidal Constituents of the Underground Parts of Ruscus aculeatus and Their Cytostatic Activity on HL-60 Cells Yoshihiro MIMAKI,Minpei KURODA,Aiko KAMEYAMA,Akihito YOKOSUKA and Yutaka SASHIDA Structure 13C NMR ??????? 45 . Acankoreoside J C47H73O20 ?????:76.5% Planta Medica 2010 76 189-194 Lupane-Type Triterpene Glycosides from the Leaves of Acanthopanax koreanum and Their In Vitro Cytotoxicity Nhiem, Nguyen Xuan; Kiem, Phan Van; Minh, Chau Van; Ha, Do Thi; Tai, Buu Huu; Yen, Pham Hai; Tung, Nguyen Huu; Hyun, Jae-Hee; Kang, Hee-Kyoung; Kim, Young Ho Structure 13C NMR ??????? 46 . Acanthifolioside G C47H80O17 ?????:76.5% Journal of Natural Products 2012 75 2094-2100 Isolation of Steroidal Glycosides from the Caribbean Sponge Pandaros acanthifolium Fabrice Berru??, Malcolm W. B. McCulloch, Patricia Boland, Saskia Hart, Mary Kay Harper, James Johnston, and Russell Kerr Structure 13C NMR ??????? 47 . compound 19 C46H76O22 ?????:76.0% Tetrahedron 2002 58 5837-5848 New pregnane glycosides from Caralluma negevensis Alessandra Braca, Ammar Bader, Ivano Morelli, Roberto Scarpato, Gino Turchi, Cosimo Pizza, Nunziatina De Tommasi Structure 13C NMR ??????? 48 . 26-O-??-D-glucopyranosyl-furost-3??,26-diol-22-methoxy-3-O-??-L-rhamnopyranosy(1??4)-O-??-D-glucopyranoside C46H78O18 ?????:76.0% Academic Journal of Second Military Medical University 2007 28 1241-1244 Studies on chemical constituents of Asparagus cochinchinensis SHEN Yang, CHEN Hai-sheng, WANG Qiong Structure 13C NMR ??????? 49 . solamargine ?????:75.5% Planta Medica 1993 59 483-484 Solamargine: The Main Glycoalkaloid from the Fruits of Solanum paludosum Mich??le Valverde, CatherineLavaud, Joel Boustie,Houriya El Badaoui, BrunoMuguet, and Max Henr Structure 13C NMR ??????? 50 . 3-O-[??-L- rhamnopyranosyl-(1??4)-??-D-glucopyranosyl]-26-O-(??-D-glucopyranosyl)-(25R)-furosta-5,20-dien-3??,26-diol ?????:75.5% Planta Medica 1988 54 344-346 Oligofurostanosides from Asparagus cochinchinensis Zhou Zhong Liang, Rita Aquino, Francesco De Simone, Antonio Dini, Oreste Schettino, and Cosimo Pizza Structure 13C NMR ??????? |
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