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quxiaoni1990

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应助: 3 (幼儿园)
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专业: 配位化学

[求助] 求助：叠氮化铅和叠氮化银的晶胞参数已有1人参与

求助：叠氮化铅和叠氮化银的晶胞参数，谢谢

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1楼 2014-10-29 17:55:46

已阅回复此楼关注TA 给TA发消息送TA红花 TA的回帖

xhtangxh

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感谢参与，应助指数 +1

Card Information
Names: alpha-Lead Azide
Formula: Pb ( N3 )2
PDF Number: 24-82
Quality: calculated
Subfiles: inorganic alloy EXP FOR

Cell and Symmetry Information
System: orthorhombic Space Group: Pnma    (no.  62)
a: 6.63 b: 16.25 c: 11.31
Density (Dx): 4.760 Z: 12

Instrument Information
Radiation: CuKa1 Wavelength: 1.5405
Instrument(d): calculated
Instrument(I): calculated I type: unknown

Comments and Additional Information
Lines: Plus 102 additional reflections to 1.1025.
Colour: Colorless
General:    Merck Index , 11  5272.
General: Explodes at 350 C or on percussion.
Pattern: See ICSD 23244 (PDF 01-073-0808).

Literature References
General: Abel, McCauley, Explosives Laboratory,Picatinny Arsenal, Dover, N.J. Private Communication          ( )
Unit Cell: Choi, Boutain. Acta Crystallogr., Sec. B 25 982 (1969)
Colour:    Handbook of Chemistry and Physics          ( )

Peak Data
PeakList
   h    k    l    d    I
   1    0    1 5.7200    2
   1    1    1 5.3950    42
   0    3    1 4.8850    100
   1    2    1 4.6770    33
   1    0    2 4.3035    33
   1    1    2 4.1590    77
   1    3    1 3.9314    18
   1    2    2 3.8020    36
   1    3    2 3.3684    1
   1    4    1 3.3120    12
   0    4    2 3.3035    8
   2    1    0 3.2480    1
   1    1    3 3.2130    16
   2    0    1 3.1810    15
   0    5    1 3.1230    15
   0    3    3 3.0946    44
   2    2    0 3.0700    11
   1    2    3 3.0393    20
   1    4    2 2.9534    22
   2    3    0 2.8280    67
   2    1    2 2.8170    42
   1    3    3 2.8040    20
   0    6    0 2.7090    27
   1    5    2 2.5930    16
   1    1    4 2.5680    9
   1    4    3 2.5500    22
   2    3    2 2.5290    2
   2    0    3 2.4894    21
   2    1    3 2.4610    4
   1    6    1 2.4480    1
   1    3    4 2.3450    1
   2    4    2 2.3390    1
   1    5    3 2.3080    4
   1    6    2 2.2920    12
   0    7    1 2.2740    4
   3    0    1 2.1690    11
   3    1    1 2.1500    8
   1    1    5 2.1224    4
   0    3    5 2.0870    12
   2    2    4 2.0815    9
   1    2    5 2.0700    5
   2    6    1 2.0620    16
   1    7    2 2.0430    12
   0    8    0 2.0316    2
   3    3    1 2.0136    1
   2    3    4 1.9993    22
   3    2    2 1.9954    16
   2    5    3 1.9763    2
   0    6    4 1.9559    13
   3    3    2 1.9240    20
   1    8    1 1.9141    5
   3    0    3 1.9066    7
   2    4    4 1.9012    9
   3    1    3 1.8937    10
   2    7    1 1.8752    3
   2    0    5 1.8689    7
   3    2    3 1.8560    3

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2楼2014-10-30 08:20:53

已阅回复此楼关注TA 给TA发消息送TA红花 TA的回帖

xhtangxh

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【答案】应助回帖

★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★
quxiaoni1990: 金币+50, ★★★★★最佳答案 2014-10-30 15:10:00

Card Information
Names: Silver Azide
Formula: Ag N3
PDF Number: 89-8021
Quality: calculated
Subfiles: inorganic alloy FIZ

Cell and Symmetry Information
System: orthorhombic Space Group: Ibam    (no.  72)
a: 5.600 b: 5.980 c: 5.998
Density (Dx): 4.956 Z: 4

Instrument Information
Radiation: CuKa1 Wavelength: 1.54060
Instrument(d): calculated Cut Off: 17.7
Instrument(I): calculated I type: peak heights
I/Icor: 5.91

Comments and Additional Information
ICSD Number: 088335
Temperature factor: ITF
TI Structure refinement and Raman spectrum of silver azide
WY j c b (IBAM)
AF AX3

Literature References
General:    Calculated from ICSD using POWD-12++          ( )
Structure: Guo, G.-C., Wang, Q.-M., Mak, T.C.W. J. Chem. Crystallogr. 29 561 (1999)

Peak Data
PeakList
   h    k    l    d    I
   1    1    0 4.0875    999
   0    2    0 2.9900    473
   2    0    0 2.8000    286
   1    1    2 2.4180    964
   1    2    1 2.4180    964
   2    1    1 2.3356    16
   0    2    2 2.1174    165
   2    0    2 2.0438    288
   2    2    0 2.0438    288
   1    3    0 1.8779    119
   3    1    0 1.7819    104
   2    2    2 1.6889    122
   1    2    3 1.5916    123
   1    3    2 1.5916    123
   2    1    3 1.5700    3
   2    3    1 1.5674    2
   3    1    2 1.5319    93
   3    2    1 1.5319    93
   0    0    4 1.4995    38
   0    4    0 1.4950    33
   1    1    4 1.4078    45
   1    4    1 1.4043    24
   4    0    0 1.4000    16
   3    3    0 1.3625    16
   0    2    4 1.3404    31
   0    4    2 1.3380    37
   4    1    1 1.3292    1
   2    0    4 1.3219    26
   2    4    0 1.3188    43
   4    0    2 1.2679    34
   4    2    0 1.2679    34
   2    3    3 1.2605    1
   3    2    3 1.2405    50
   3    3    2 1.2405    50
   2    2    4 1.2090    37
   2    4    2 1.2072    26
   1    3    4 1.1718    25
   1    4    3 1.1718    25
   1    5    0 1.1696    20
   4    2    2 1.1678    24
   3    1    4 1.1473    23
   3    4    1 1.1454    12
   4    1    3 1.1263    1
   4    3    1 1.1253    1
   5    1    0 1.1009    7
   1    5    2 1.0897    18

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3楼2014-10-30 08:23:17

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